PRZEWODNIK PO PRZEDMIOCIE
Transkrypt
PRZEWODNIK PO PRZEDMIOCIE
Alternatywne i odnawialne źródła energii ................................................................................. 2 Basic unit processes in chemical technology ............................................................................. 6 Calculation of technical chemistry ........................................................................................... 12 Catalytic processes in oil industry............................................................................................ 17 Chemical and engineering thermodymics ................................................................................ 21 Chemical Engineering .............................................................................................................. 27 Chemical technology-raw materials and organic industry processes....................................... 33 Chemical technology-raw materials and energy carriers ......................................................... 39 Corrosion protection and industrial electrochemical processes ............................................... 44 Philosophy of Science and Technology ................................................................................... 48 Inorganic Technical Chemistry ................................................................................................ 52 Investment and chemical plants maintenance principles ......................................................... 55 Laboratory of surfactants technology I ................................................................................ 61 Laboratory of surfactants technology II ................................................................................... 64 Materials science ...................................................................................................................... 68 Measurements and Automatics ................................................................................................ 72 Optimization of chemical processes and electrochemical production processes ..................... 76 Physicochemistry of coal and carbon materials ....................................................................... 79 Physicochemistry of petroleum and derived materials ............................................................ 82 Quality control of raw materials and products ......................................................................... 86 Quality Management ................................................................................................................ 90 Small volume chemical production .......................................................................................... 94 Strategies of sustainable development ................................................................................... 100 Systems of management of the technological process and quality ........................................ 104 Technical organic chemistry .................................................................................................. 107 Technical safety...................................................................................................................... 111 Technological project ............................................................................................................. 116 Technology of Coal and Carbon Materials ............................................................................ 121 Technology of Fine Chemicals .............................................................................................. 124 Technology of disperse systems ............................................................................................. 128 The Polish chemical industry .............................................................................................. 132 The industrial laboratory of crude oil and coal technology I ................................................. 136 The industrial laboratory of crude oil and coal technology II ................................................ 140 Water in technology ............................................................................................................. 143 1 Zał. nr 4 do ZW 64/2012 Wroclaw University of Technology Faculty of Chemistry SUBJECT CARD Name in Polish Alternatywne i odnawialne źródła energii Name in English Alternative and renewable energy sources Main field of study (if applicable): Chemical Technology Specialization (if applicable): …………………….. Level and form of studies: 1st level, full-time* Kind of subject: optional* Subject code TCC010031 Group of courses NO* Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 30 60 crediting with grade* For group of courses mark (X) final course Number of ECTS points 2 including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 1.0 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 1. \ SUBJECT OBJECTIVES C1 Getting knowledge of the possibility of obtaining energy from alternative sources C2 Getting knowledge about impact of alternative and renewable energy production on environment SUBJECT EDUCATIONAL EFFECTS relating to knowledge: PEK_W01 able to define alternative and renewable energy sources and determine their importance in modern energy systems PEK_W02 able to critically evaluate renewable energy sources PEK_W03 know the future possibilities of renewable energy production PEK_W04 is capable to evaluate essentially the renewable sources of energy from an economic point of view PEK_W05 has the basic knowledge about an environmental risks, associated with alternative PROGRAMME CONTENT Form of classes - lecture Lec 1 Alternative energy sources. Introduction and basic concepts. The 2 Number of hours 1 Lec 2 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 Lec 9 Lec 10 Lec 11 Lec 12 Lec 13 Lec 14 Lec 15 Lec 16 importance of alternative energy for the economy. Classification of conventional and alternative methods of energy production Fuel cells. Basic concepts, principle of operations. Classification of fuel cells in view of: fuel, electrolyte, the work temperature. Fuel cell applications Hydrogen as fuel in future. Production of hydrogen. Hydrogen storage. Hydrogen safety. Magnetohydrodynamic power plants. Conventional fossil fuels power plants, thermodynamic limits. Energy efficiency improvements. Solar energy. Conversion of solar radiation into useful energy using various technologies. Solar thermal energy. Solar photovoltaics (PV). Basic principles and a brief history of PV. Efficiency of photovoltaics. Innovative PV technologies. The application of photovoltaic cells Geothermal energy. The source of heat and its availability. Technologies for geothermal resource exploitation. Resources of high-enthalpy stem fields, dry steam power plant, resources for direct use of geothermal energy. Environmental impact and safety of geothermal energy. Geothermal energy in Poland. Wind energy. Wind energy sources Wind energy potential. A brief history of wind energy. Environmental impact. Non-conventional hydroelectricity. Small-scale hydroelectricity as elements in a power system. Hydrological effect. Types of hydroturbines. Tidal power. Wave energy resources. The energy of ocean currents. Ocean thermal energy conversion. Biomass as a fuel. Main bioenergy conversion routes. Combustion of solid biomass: wood and crop residues, municipal solid wastes. Environmental benefits and impact. Gaseous and liquid fuels from biomass. Anaerobic digestion. Large scale anaerobic digestion plants. Fermentation to produce ethanol. From wood to liquid fuel. History and development of nuclear energy. Natural radioactivity. The interaction of neutrons with matter. Nuclear fission. Fissile isotopes. Nuclear weapons. The discovery and proliferation of nuclear weapons. Development of nuclear weapons. Nuclear weapons, a threat to humanity Non-conventional nuclear energy. Safety of nuclear techniques. Natural nuclear reactors. Radionuclides as an energy source. Nuclear fusion. Physical fundamentals of fusion. Attempts to peaceful use of nuclear fusion. Nuclear fusion in stars. Energy storage problems. Lec 17 Summary and conclusion. Test. 2 2 1 2 2 2 2 2 2 2 2 2 2 2 1 1 30 Total hours TEACHING TOOLS USED N1. Lecture with multimedia presentation EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT 3 Evaluation (F – forming (during semester), P – concluding (at semester end) P (Lecture) Educational effect number Way of evaluating educational effect achievement PEK_W01-PEK_W05 Test PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [1] W. M. Lewandowski. Proekologiczne źródła energii odnawialnej. WNT, Warszawa 2001. [2] Red. J. Szlachta. Niekonwencjonalne źródła energii. WAR, Wrocław 1999. [3] A. J. Rotter. Bomba atomowa, Świat wobec zagrożenia. PWN, Warszawa 2011. [4] J. Kubowski. Broń jądrowa. WNT, Warszawa 2005. [5] H. Drulis, J. Hanuza, D. Hreniak, M. Miller, G. Paściak, W. Stręk. Ogniwa paliwowe, nowe kierunki rozwoju. Wiadomości chemiczne, biblioteka. Wrocław, 2005. SECONDARY LITERATURE: [1] G. Charpak, R. L. Garwin. Błędne ogniki i grzyby atomowe. WNT, Warszawa 1999. [2] J. Taubman. Węgiel i alternatywne źródła energii. Prognozy na przyszłość. PWN, Warszawa 2011. [3] G. Jastrzębska. Ogniwa słoneczne. WKŁ, Warszawa 2013. [4] K. Hoffmann. Wina i odpowiedzialność, Otto Hahn, Konflikty uczonego. WNT, Warszawa, 1997. [5] B. Burczyk. Biomasa. Oficyna Wyd. Politechniki Wr. Wrocław 2011. SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Dr hab. inż. Stanisław Gryglewicz, stanisł[email protected] 4 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Alternative and renewable energy sources AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical technology Subject educational effect Correlation between subject Subject Programme content*** educational effect and objectives*** educational effects defined for main field of study and specialization (if applicable)** PEK_W01 (knowledge) Teaching tool number*** PEK_W02 C1, C2 C2 Lec1 Lec1, Lec17 N1 N1 PEK_W03 C1 Lec2-16 N1 PEK_W04 C2 Lec2-16 N1 PEK_W05 C2 Lec2-16 N1 5 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Podstawowe procesy jednostkowe w technologii chemicznej Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Basic unit processes in chemical technology Chemical technology 1st level obligatory TCC015003 No *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory 30 30 90 60 Examination Examination / crediting with grade* Crediting with grade* Project Seminar Examination / crediting with grade* Examination / crediting with grade* For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 3 3 2 1 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 1. 2. 3. Competence in the field of general and physical chemistry Competence in the field of base mathematics SUBJECT OBJECTIVES C1 C2 C3 C4 Introduce students to conception of process and unit operations Understanding the basic principles of operation of apparatus and reactors for unit processes and operations in a variety of layouts phase Introduce students to conception of realization of chemical processes in the continuous systems Introduce students to principles of technological systems structure as combination of chemical unit processes and operations 6 C5 C6 C7 Acquainting students with the selected processes of chemical technology, noncatalytic and catalytic processes in a fluidized and stationary beds, Introduce students to the specific features of biotechnological processes Introduce students to the modern operations of chemical substances operations SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – student is able to make the correct characterization of the unit processes and operations applied in chemical technology, PEK_W02 – student is able to work up the correct technological scheme of the plant and select the proper apparatuses and reactors, to indicate the suitable unit processes and operations, PEK_W03 – student is able to characterize the flow of chemical substances in various phase systems PEK_W04 – student knows the principles of operation of catalytic and non-catalytic processes and is able to describe and characterize, PEK_W05 – student obtained the fundamental knowledge on separation technics, PEK_W06 – student obtained the fundamental knowledge on the methods of biofuels production, PEK_W07 – student obtained the fundamental knowledge on polymerization processes and physicochemical properties the obtained materials, PEK_W08 – student understands the principles of biotechnological processes. Relating to skills: PEK_U01 – student is able to practically work up technological scheme of the process and define the indispensable unit processes and operations PEK_U02 – student is able to practically describe the base unit operations and processes for the selected chemical technologies from the various chemistry branches, PEK_U03 – student is able to practically realize the simple chemical laboratory as unit processes and to make the base calculations connected with their realization, PEK_U04 – student is able to plane and realize the simple separation operation with application of membrane technics, PEK_U05 – student is able to determine process effectiveness, PEK_U06 – student is able to determine physicochemical properties of the obtained reaction products, PEK_U07 – student is able to plane and realize the process of chemical modification of raw materials. Relating to social competences: PEK_K01 PEK_K02 … change PROGRAMME CONTENT Form of classes - lecture Lec 1 Lec 2 The base concepts, unit process, unit operation, definition, characteristics, Scheme of technological process, unit operations and unit processes as 7 Number of hours 2 2 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 Lec 9 Lec 10 Lec 11 Lec 12 Lec 13 Lec 14 Lec 15 components of chemical technology process. Raw materials, products and side products of unit operations and processes. Regime and parameters of unit processes and operations. Mixing and mass and energy exchange. Equilibrium in chemical processes. Yields and reagent conversions in unit chemical processes. Concept of driving reaction force in various flowing systems, methods of increasing of reaction rate in unit processes. Examples of apparatuses systems for unit processes and operations in gassolid, gas-liquids, liquid solids systems, catalytic and non-catalytic threephase systems, reactor concepts for various catalyst forms. Examples of chemical technology processes, fluidized bed catalytic processes, solid bed catalytic processes, Non-catalytic thermal processes, high temperature in heterogeneous systems, electrolysis processes. Enzymes. Kinetics. Enzymatic processes with native and immobilized enzyme. Microorganisms, microbiological processes. Kinetics. Products separation. Separation operations: extraction, distillation, chromatography, sedimentation, flocculation. Ordinary membrane operations, microfiltration, ultrafiltration, nanofiltration, reversed osmosis, electro-dialysis. Advanced membrane processes, pervaporation, membrane distillation, membrane pertractors, hybrid processes. Addition polymerization: reaction mechanisms, initiators, inhibitors, condensation polymerization. Molecular weight. Distribution of molecular weights. Polymer solutions. Condensed phases. Mixtures. Crystallinity. Phase transformation temperatures. Total hours Form of classes - class 2 2 2 2 2 2 2 2 2 2 2 2 30 Number of hours Cl 1 Cl 2 Cl 3 Cl 4 Total hours Form of classes - laboratory Lab 1 Lab 2 Lab 3 Lab 4 Lab 5 Lab 6 Lab 7 Lab 8 Introductory classes. Catalytic cracking. Rape oil transesterification in flow system. Photodegradation of organic compounds in water. Block polymerization of methyl methacrylate. Membrane separation – isolation of products from reaction mixture. Sulfonation reaction - obtaining of p-toluenesulphonic acid. Alkylation reaction – obtaining of quaternary ammonium salts. 8 Number of hours 2 4 4 4 4 4 4 4 Lab 9 or Ions exchange in basic technological processes Total hours N1 N2 N3 N4 4 30 TEACHING TOOLS USED Lecture with multimedia presentation Realization of experimental tasks Reports from the realized exercises Consultation EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) C (lecture) PEK_W01PEK_W08 Final exam Mark 2.0: 0-50 % Mark 3.0: 51-60 % Mark 3.5: 61-70 % Mark 4.0: 71-80 % Mark 4.5: 81-90 % Mark 5.0: 91-98 % Mark 5.5: >98 % F1 Laboratory exercises, preliminary test F2 Laboratory exercises, report PEK_U02 – PEK_U08 Partial oral preliminary test (max. 30 points) PEK_U02 – PEK_U07 Evaluation of report level (max. 30 points) C (laboratory exercises) = 3.0 if (F1 + F2)/2= 18.0 – 20 pkt. 3.5 if (F1 + F2)/2 = 20 – 22 pkt. 4.0 if (F1 + F2)/2 = 22 – 24pkt. 4.5 if (F1 + F2)/2 = 24 – 26 pkt. 5.0 if (F1 + F2)/2 = 26 – 28 pkt. 5.5 if (F1 + F2)/2 > 28 pkt. 9 PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [1] I. Mukhlyonov et al. The Theoretical Foundations of Chemical Technology, Part 1 and Part 2. Mir Publishers, Moscow. 1977. [2] M. Bodzek, J. Bohodziewicz, K. Konieczny, Techniki membranowe w ochronie środowiska, Wydawnictwo Politechniki Śląskiej, Gliwice 1997 [3] Praca zbiorowa pod red. Z. Florjańczyka, S. Penczka, Chemia polimerów t. III, Oficyna Wydawnicza Politechniki Warszawskiej, Warszawa 1998 [4] Szlachta Z., „Zasilanie silników wysokoprężnych paliwami rzepakowymi”, WKŁ Warszawa 2002. [5] Baczewski K., Kałdoński T. „Paliwa do silników o zapłonie samoczynnym”, WKŁ Warszawa 2008 [6] Morrison R.T., Boyd R.N. „Chemia organiczna T.1” Wydawnictwo Naukowe PWN, Warszawa 2010 SECONDARY LITERATURE: [6] T. Winnicki, Polimery w ochronie środowiska, Arkady, Warszawa 1978 [7] [8] SUBJECT SUPERVISOR (Prof. dr hab. inż. Jerzy Walendziewski, [email protected]) MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY ……………………………………. Subject educational effect (knowledge) PEK_W01 PEK_W02 PEK_W03 PEK_W04 PEK_W05 PEK_W06 PEK_W07 PEK_W08 (skills) PEK_U01 PEK_U02 PEK_U03 Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** Programme content*** Teaching tool number*** K1Atc_W17 C1 Wy1, Wy2, W3 N1, N4 K1Atc_W17 K1Atc_W17 K1Atc_W17 K1Atc_W17 K1Atc_W17 K1Atc_W17 K1Atc_W17 C4, C5 C2, C3, C4 C4, C5 C7 C6 C4 C6 Wy3, Wy4, Wy5 Wy3 - Wy7 Wy3 - Wy7 Wy10 –Wy12 Cw3 Wy2, Wy3 Wy13, Wy14 N1, N4 N1, N4 N1, N4 N1, N4 N1, N4 N1, N4 N1, N4 K1Atc_U25 C2, C4 Wy1, Wy2, N3, N4 K1Atc_U25 K1Atc_U25 C2, C4 C7 Wy6, Wy7 Cw6 N3, N4 N3, N4 10 PEK_U04 K1Atc_U25 C1, C4 PEK_U05 K1Atc_U25 C3, C5, C7 PEK_U06 K1Atc_U25 C5, C6, C7 … (competences) PEK_K01 PEK_K02 PEK_K03 … ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 11 Cw2, Cw3, Cw7 Cw4, Cw6, Cw8, Cw9 Cw3, Cw6, Cw7, Cw8, Cw9 N3, N4 N3, N4 N3, N4 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Obliczenia w chemii technicznej Calculation of technical chemistry Chemical Technology 1st/full-time obligatory CHC012004 NO *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar Examination / crediting with grade* Examination / crediting with grade* Examination / crediting with grade* 30 60 Examination / crediting with grade* crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 2 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 1. Knowledge of chemistry at the high school level. 2. Knowledge of physics at the high school level. 3. Knowledge of elementary mathematics. SUBJECT OBJECTIVES C1 Can a practical use chemical calculations in the following technological processes: combustion processes, water softening, fluid dynamics, diffusion processes, processes catalytic and non-catalytic, technical analysis of gases and water, electrochemistry. C2 C3 C4 12 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – ... Relating to skills: PEK_U01 – Knows how to describe quantitatively the functions of state for basic change ideal and non-ideal gases. PEK_U02 – Knows how to perform calculations for simply diffusion processes. PEK_U03 - Can a practical use chemical calculations in the combustion processes. PEK_U04 - Knows how to perform calculations of fluid dynamics. PEK_U05 - Can identify, formulate and solve simple tasks of the technical analysis of gases and water. PEK_U06 - Can a practical use chemical calculations in the catalytic and non-catalytic ……………processes. PEK_U07 - Can a practical use chemical calculations in electrochemistry . Relating to social competences: PEK_K01 PEK_K02 … PROGRAMME CONTENT Form of classes - lecture Number of hours Lec 1 Lec 2 Lec 3 Lec 4 … Total hours Form of classes - class Cl 1 Cl 2 Cl 3 Cl 4 Cl5 How to conduct classes, conditions for obtaining credit. The accuracy of the calculations. The dynamics of fluids. The equation of continuity, Bernoulli's equation, Stokes law, number of Reynolds'a, laminar flow and turbulent, Diffusion processes. Diffusion of gases. Ficke'a law. I law of thermodynamics, The properties of gases and vapours. Van der Waalls equation. Dalton's Law. The relative humidity. Clausius-Clapeyron equation. The properties of gases and vapours. Van der Waalls equation. Dalton's 13 Number of hours 2 2 2 2 2 Cl6 Cl7 Cl8 Cl9 Cl10 Cl11 Cl12 Cl13 Cl14 Cl15 Law. The relative humidity. Clausius-Clapeyron equation cd. Technical analysis of gases and water. Technical analysis of gases and water cd. Repetition of the material and I Test. Electrochemistry. Galvanic cells, electrode potential, electromotive force, Faraday law. Electrochemistry. Galvanic cells, electrode potential, electromotive force, Faraday law, cd. Thermochemistry. Heat and his unit. Dulonga and Petita rule. Termochemical equilibrium. Hess's Law. Heat phase transformations of substances and the heat of chemical reactions. Heat, combustion, neutralized, dissolving, hydration. Thermochemistry. Heat and his unit. Dulonga and Petita rule. Termochemical equilibrium. Hess's Law. Heat phase transformations of substances and the heat of chemical reactions. Heat, combustion, neutralized, dissolving, hydration. Cd. Fuel combustion processes. Water softening. Repetition of the material and II Test. Total hours Form of classes - laboratory 2 2 2 2 2 2 2 2 2 2 30 Number of hours Lab 1 Lab 2 Lab 3 Lab 4 … Total hours Form of classes - project Number of hours Proj 1 Proj 2 Proj 3 Proj 4 … Total hours Form of classes - seminar Number of hours Sem 1 Sem 2 Sem 3 Sem 4 … Total hours 14 TEACHING TOOLS USED N1 N2 … Troubleshooting tasks EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) F1(Class) F2(Class) PEK_U01 – PEK_U03 PEK_U03 – PEK_U05 Test I (max. 20 points) Test II (max. 20 points) … C (Class) = 3,0 (F1 + F2) = 12,0 – 12,0 pkt. 3,5 (F1 + F2) = 14,0 – 14,0 pkt. 4,0 (F1 + F2) = 16,0 – 16,0 pkt. 4,5 (F1 + F2) = 18,0 – 18,0 pkt. 5,0 (F1 + F2) = 19,0 – 19,0 pkt. 5,5 (F1 + F2) = 40,0 pkt. PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [6] Ufnalski W., Podstawy obliczeń chemicznych z programami komputerowymi, WN-T, Warszawa, 1999 [7] Bielański A., Podstawy chemii nieorganicznej, PWN, Warszawa, 2003 [8] Praca zbiorowa, Obliczenia w chemii nieorganicznej, Wyd. PWr., 2002 [9] Walker J., Podstawy fizyki - zbiór zadań, PWN, Warszawa, 2005 SECONDARY LITERATURE: [9] [10] [11] SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Magdalena Klakočar-Ciepacz, [email protected] 15 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT ……………………………………. AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY ……………………………………. Subject educational effect (knowledge) PEK_W01 PEK_W02 PEK_W03 … (skills) PEK_U01 PEK_U02 PEK_U03 PEK_U04 PEK_U05 PEK_U06 PEK_U07 … Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** Programme content*** Teaching tool number*** K1Atc_U10 K1Atc_U10 K1Atc_U10 C1 Cl3, Cl4, Cl5 N2 C1 N2 K1Atc_U10 K1Atc_U10 K1Atc_U10 K1Atc_U10 C1 C1 C1 C1 Cl2 Cl6, Cl7,Cl11, Cl12, Cl13 Cl4 Cl6, Cl7 Cl6, Cl7 Cl9, Cl10 C1 (competences) PEK_K01 PEK_K02 PEK_K03 … ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 16 N2 N2 N2 N2 N2 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Technologie przemysłu rafineryjnego Catalytic processes in oil industry Chemical Technology Processes and chemical products 1st level, full-time optional TCC010015 NO *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 30 60 crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 4. 5. Basic Organic Chemistry Basic Chemical Engineering SUBJECT OBJECTIVES C1 C2 C3 To provide students with the basic processes of oil processing To provide students with the directions of the development of liquid fuels technologies. To provide students with ways of reducing of the risks associated with the production and use of petroleum products C4 17 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – knows the basic schemes of refinery PEK_W02 - knows methods of oil treatment PEK_W03 - knows methods of liquid fuels producing PEK_W04 - knows methods of hydrogen production PEK_W05 - knows methods of oxygenates production PEK_W06 - knows the ways to reduce the risks associated with the production and use of petroleum products ... Relating to skills: PEK_U01 – PEK_U02 – … Relating to social competences: PEK_K01 PEK_K02 … PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 Lec 9 Form of classes - lecture Flowsheets of oil refinery. Fractionation Hydrotreating Cracking and hydrocracking Reforming of gasoline Isomerization and alkylation Production of oxygenates (ethers, FAME) Production of hydrogen Production of asphalt and refinery waste disposal Number of hours Total hours TEACHING TOOLS USED N1 N2 … 18 2 2 4 8 4 4 2 2 2 30 EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) F1 F2 F3 C PEK_W01 – PEK_W06 test PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [10] J.G. Speight: The chemistry and technology of petroleum, M. Dekker. [11] E.W. Smidowicz: Przeróbka destrukcyjna ropy naftowej i gazu, WNT. [12] SECONDARY LITERATURE: [12] G.D. Hobson: Modern petroleum technology, J. Wiley & Sons 1984. [13] [14] SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) prof. dr hab. inż. Janusz Trawczyński; [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Catalytic processes in oil industry AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical Technology Subject educational effect (knowledge) PEK_W01 PEK_W02 PEK_W03 … Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Course selectable 19 Subject objectives*** Programme content*** Teaching tool number*** (skills) PEK_U01 PEK_U02 PEK_U03 … (competences) PEK_K01 PEK_K02 PEK_K03 … ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 20 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Termodynamika chemiczna i techniczna Chemical and engineering thermodymics Chemical Technology 1st level, full-time obligatory TCC014005 NO *delete as applicable Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Lecture Classes 15 15 60 30 Crediting with grade Laboratory Project Seminar Crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 1 1 0,5 0,5 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 6. 7. 8. Knowledge fundamentals of physical chemistry Knowledge fundamentals of inorganic chemistry Knowledge of algebra and mathematical analysis SUBJECT OBJECTIVES C1 C2 C3 C4 C5 C6 To familiarize students with the basic dependencies and status functions equations of thermodynamic. To get basic knowledge about the thermodynamic description of change; ideal, nonideal. Learn how to perform basic calculations for thermodynamic cycles, heat engine. To familiarize students with a description of the thermodynamic solutions ideal and non-ideal . To get basic knowledge about the thermodynamic equilibrium. Learn how to perform basic calculations for technological processes. 21 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – Familiar with description of reversible and not reversible thermodynamic process. PEK_W02 – Learns the criteria for chemical equilibrium thermodynamic PEK_W03 - Has basic knowledge to describe the thermodynamic real and non-real solutions PEK_W04 - Knows how to describe qualitatively and quantitatively balance in ideal and non-ideal solutions gas/liquid systems. ... Relating to skills: PEK_U01 – knows how to describe quantitatively the functions of state for basic change ideal and non-ideal gases PEK_U02 – knows how to perform calculations for thermodynamic efficiency of refrigerators engine: cooling and warm, heat pumps PEK_U03 - Can make activity of substance and activity coefficients in gas and liquid solutions and the reaction heat PEK_U04 - Knows how to perform calculations of the equilibrium constants and equilibrium composition PEK_U05 - Can identify, formulate and solve simple tasks of practical engineering … Relating to social competences: PEK_K01 PEK_K02 … PROGRAMME CONTENT Form of classes - lecture Lec 1 Forms of energy, basic concepts of thermodynamics, the types of systems. Determination of thermodynamic system (parameter). The functions of the State; internal energy, enthalpy, free energy. Transformation processes with and without the effects of ideal gas interactions with the environment, reversible and irreversible. The principle of thermodynamics, open system, technical work. The status of reference in thermodynamics. Lec 2 Thermodynamic cycles; Carnot, Diesel and others, Gas turbines; refrigeration, a heat pump. Devices using heat pumps; the furnace, drying, fractionating column. Throttling an ideal gas; adiabaticizoenergy, adiabatic-izoentalpy Lec 3 Real gases. The equation of State of real gases; Virial, compressibility factor, is capacity, van der Waals (reduced), Berthelot's (reduced). The principle of corresponding States. Calculation of thermodynamic function of pure real gases for the specified parameters; an approximate method of Watson-Hougena, using graphs of functions of the universal parameters reduced. 22 Number of hours 2 2 2 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 Throttling of the actual effect Joula-Thomson. The temperature inversion, liquify gases. Thermodynamic description of the condensed phases. Calculate the molar volume, density using the coefficient of expansion. The molar heat capacity, enthalpy, entropy of solids and liquid. Solutions of partial molar volumes, equation Gibsa-Duhema. Thermodynamic potential, molal particle thermodynamic potential. Depending on the chemical potential of temperature, pressure and concentration of the component. Gas solutions, solutions. Amagata Rule. Thermodynamic description of solutions (the principle of corresponding States, parameters, pseudo-critical parameters, reduced parameters, Kaya’s formula of universal reduced parameters. Activity, the activity pressure coefficient, Randall-Lewis rule. Calculation of pressure activity (volatility) using any equation of State. Description of the equilibrium state, the relative number of reaction progress, degree of change. Equilibrium state (pressure, activity pressure). Calculation of thermodynamic potential of standard for a chemical reaction with specific parameters (T, p). Depending on the pressure and temperature of equilibrium states. The influence of intertów on the State of equilibrium in the gas phase. Calculation of the equilibrium constant and the equilibrium composition. Phase equilibrium. Enthalpy and entropy changes. Phase transition of the first and second-order transition. Thermodynamics and kinetics of electrochemical processes. The termochemical calculations. Thermal balance of chemical process. Exam Total hours Form of classes - class Cl 1 Cl 2 Cl 3 Cl 4 Cl 5 Cl 6 How to conduct classes, conditions for obtaining credit. Calculation of thermodynamic function changes and heat, work and work volume for ideal gas reversible transformations. Chemical calculations for the reverse transformation of politropic ideal gas. Engineering calculations for simple devices (theoretical power, stream water cooling for perfect izotermic compressors). Carnot cycle, thermodynamic factor value calculations in the cycle, heat and work volume for each changes, the efficiency of circulation. Calculation for heat pumps, refrigerators, freezers, power cooling. Thermodynamic description of the condensed phases. Calculate the molar volume, density using the coefficient of expansion. The molar heat capacity, enthalpy, entropy of solids and liquid. Application of the equation of State of ideal gas, universal reduced parameters. Perfect gases and their mixtures: calculation of activity and activity coefficients. Calculation of standard chemical reaction energy with specific characteristics and thermodynamic constants and composition of równowagowego. Calculation of activity coefficients for real gases activity and their mixtures. Calculation of standard chemical reaction energy with specific parameters, the equilibrium constant and the equilibrium 23 2 2 2 2 1 15 Number of hours 2 2 2 2 2 2 composition. Cl 7 Cl 8 The calculation of termo-chemical. Thermal balance of chemical processes. Repetition of the material. Test Total hours Form of classes - laboratory 2 1 15 Number of hours Lab 1 Lab 2 Lab 3 Lab 4 … Total hours Form of classes - project Number of hours Proj 1 Proj 2 Proj 3 Proj 4 … Total hours Form of classes - seminar Number of hours Sem 1 Sem 2 Sem 3 Sem 4 … Total hours N1 N2 … TEACHING TOOLS USED Lecture with mulimedial presentation Troubleshooting tasks EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) P (lecture) PEK_W01 – PEK_W04 Exam (max. 15 points) 24 P (classes) PEK_U01 – PEK_U05 Test (max. 15 points) … P (lecture, classes) = 3,0=7,5-9,0 3,5=9,5-11,0 4,0=11,5-12,5 4,5=13,0-13,5 5,0=14,0-14,5 5,5=15,0 PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [13] J. Szarawara, Termodynamika chemiczna stosowana, WNT, Warszawa 1997 [14] S. Michałowski, K. Wańkowicz, Termodynamika procesowa, WNT, Warszawa 1999 SECONDARY LITERATURE: [15] W. Ufnalski, Wprowadzenie do termodynamiki chemicznej, Oficyna Wydawnicza Politechniki Warszawskiej, 2004 [16] K. Annamalai, Advance Thermodynamics Engineering, CRC Press, 2002 SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Dr. hab. inż. Piotr Falewicz, [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT ……………………………………. AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY ……………………………………. Subject educational effect (knowledge) PEK_W01 PEK_W02 PEK_W03 … Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** Programme content*** Teaching tool number*** K1Atc_W16 C1 Lec1 N1 KlAtc_W16 KlAtc_W16 KlAtc_W16 C2 C4 C5 Lec2, Lec3 Lec4, Lec5 Lec6, Lec7 N1 N1 N1,N2 25 (skills) PEK_U01 PEK_U02 PEK_U03 PEK_U04 PEK_U05 KlAtc_U26 C3 Cl1 N1,N2 KlAtc_U26 KlAtc_U26 KlAtc_U26 KlAtc_U26 C3 C6 C6 C6 Cl2 Cl3, Cl4 Cl5, Cl6 Cl7 N2 N2 N2 N2 (competences) PEK_K01 PEK_K02 PEK_K03 … ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 26 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Inżynieria Chemiczna Chemical Engineering Chemical Technology 1st level, full-time obligatory ICC015005 NO *delete as applicable Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Lecture Classes Laboratory 30 30 30 60 60 60 Examination Crediting with grade Crediting with grade Project Seminar Examination / crediting with grade* Examination / crediting with grade* For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 1 2 2 2 2 1 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 9. 10. Completion physics Completion mathematics SUBJECT OBJECTIVES C1 C2 C3 C4 C5 C6 C7 Introduce with chemical and physical basis of basic chemical engineering processes Cognition of form rules of heat and mass balances in the steady state and unsteady state conditions. Cognition of mathematical modeling and design rules of processes and apparatus used in chemical engineering and processing Cognition of scale-up rules Usage of hydrostatics and hydrodynamics rules for description of apparatus occur in industrial installations Cognition of rules choice of pumps and other flow apparatus Cognition of rules of apparatus calculation with two phases flow 27 C8 C9 C10 C11 C12 C13 Cognition of mathematical methods of heat exchangers description and design Introduction to balancing and operation parameters calculation for selected mass transfer apparatus Carrying out of pressure drops measurements in order to determine flow velocity. Carrying out of stream volume measurement Experimental determining of heat and mass transfer coefficients Experimental determining of reflux ratio in rectification column and graphical interpretation of column operation SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – Know chemical and physical basis of selected processes and oparations occur in chemical engineering PEK_W02 – Can define heat and mass balances in steady state and unsteady state conditions. PEK_W03 – Can describe with the use of mathematical model and design selected processes and apparatus used in chemical engineering PEK_W04 – Know rules of scale-up Relating to skills: PEK_U01 – Can describe apparatus operation used in industrial plants using rules of hydrostatics and hydrodynamics PEK_U02 – Can choice pumps and other apparatus cooperating with pipeline PEK_U03 – Can calculate heat exchangers area and determine heat exchanger operation parameter PEK_U04 – Can form mass balances and determine operation parameters of selected mass exchangers PEK_U05 – Can use appropriate metering equipment for determination of pressure drop and can calculate fluid flow velocity PEK_U06 – Can carry out of volume stream of gas or liquid PEK_U07 – Can experimentally measure heat and mass transfer coefficients PEK_U08 – Can experimentally determine reflux ratio and use to calculation of operating lines of rectification process PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Form of classes - lecture Field of interest of chemical engineering and rules of mass and energy balancing in chemical engineering processes Fluid flow in apparatus, Bernoulli law, flow resistances in pipelines (Darcy Weisbach equation) and in selected apparatus for one- and two phase flows Pumps – pump and pipeline characteristics. Rules of pumps and pipelines connecting. Calculation of pump operating pump in selected configurations pump – pipeline. Flow single particle in fluids. Calculation of particle diameter, flow velocity, coefficient of flow resistance, swarm falling, fluidization, pneumatic transport, sedimentation 28 Number of hours 2 2 2 2 Lec 5 Filtration. Filters construction, classification of filtration processes, Lec 6 Lec 7 Lec 8 Lec 9 Lec 10 Lec 11 Lec 12 Lec 13 Lec 14 Lec 15 filtration with constant pressure difference, filtration with constant filtrate stream two stage filtration, application of filtration in selected technologies Mixers, construction of stirrers and mixers, definition of Reynolds number, power consumption, scale-up Heat transfer processes, calculation of heat transfer through multilayer flat and cylindrical walls, dimensions analysis, rules of heat transfer exchangers design Classification of mass transfer apparatus, mass transfer and overall mass transfer coefficients, conception of process operation line, concurrent and countercurrent flow of streams, diffusional and thermo-diffusional apparatus Absorption processes. Absorption apparatus, methods of description of interphase mass transfer process, calculation of column diameter and column high. Methods of process realization. Distillation processes. Equilibrium distillation, batch distillation, distillation with steam, thin layer distillation, molecular distillation. Preparation of balance equations for continuous and periodic processes. Rectification of two components systems, construction of rectification column, heat and mass balance of the process, determination of minimal reflux ratio, determination of minimal number of theoretical stages (plates). Aparaty ekstrakcyjne o działaniu okresowym i ciągłym. Sposoby obliczania z wykorzystaniem trójkąta składu. Obliczanie stopnia zatrzymania fazy rozdrobnionej, średnicy kropel, średnicy kolumny, współczynników wnikania masy oraz wysokości kolumny ekstrakcyjnej. Procesy adsorpcyjne, właściwości adsorbentów stałych, adsorbery o działaniu okresowym, pojęcie frontu adsorpcji, metody obliczania czasu adsorpcji, łączenie adsorberów. Procesy suszarnicze. Obliczanie właściwości medium suszącego (powietrza) na podstawie wykresu Moliera. Pierwszy i drugi okres suszenia, bilansowanie procesów suszarniczych, obliczanie zużycia ciepła i czasu suszenia. Podział reaktorów i zasady bilansowania. Obszar zainteresowań inżynierii chemicznej oraz zasady bilansowania masy i energii w procesach inżynierii chemicznej Total hours Cl 1 Cl 2 Cl 3 Form of classes - class Presentation of subject program. Discuss to meet the completion requirements. Basic concepts and parameters. Used units and conversions. Hydrostatics. Calculation of pressure arrangement in the chemical plants. Hydrodynamics. Phenomena connected with fluids flow. Calculation 29 2 2 2 2 2 2 2 2 2 2 2 30 Number of hours 2 2 2 Cl 4 Cl 5 Cl 6 Cl 7 Cl 8 Cl 9 Cl 10 Cl 11 Cl 12 Cl 13 Cl 14 Cl 15 of pressure drops. Bernoulli law and application. Pumps and calculation of pumps installations. Rules of pumps choice. Verification colloquium I. Sedimentation of particles. Forces act on the single particle. Fall of single particle. Stokes law. Fall of particle swarm . Calculation of sedimentation tank, dust chamber, cyclone. Filtration. Filtration equation and usage for filter design. Heat conduction in the flat and cylindrical wall. Calculation of temperature profile in the solid. Heat transfer in the natural convection, forced convection, liquid boiling and steam condensation. Calculations of heat transfer coefficients. Two phase heat transfer. Heat exchangers calculations. Basic mass transfer processes. Rectification, absorption, extraction. Calculation of mass balances. Calculation of rectification column for separation of two component solution. Verification colloquium II. Total hours Form of classes - laboratory Organizational activities. Becoming acquainted with rules of health and safety at work in research laboratory. Discuss to meet the completion requirements. Take knowledge of apparatus used in laboratory. Lab 2 Determination of fluid flow profile in the pipeline with circular cross – section. Lab 3 Pump characteristics. Lab 4 Determination of flow coefficient in flow narrow for liquids. Lab 5 Heat exchanger pipe in pipe type. Lab 6 Heat transfer during liquid boiling Lab 7 Efficiency of mixing energy on the mass transfer coefficient in the solid – liquid system. Lab 8 Determination of HETP in packed bed rectification column. Lab 9 Distillation with the steam. Lab 10 Heat transfer in fluidized bed. Lab 1 Total hours TEACHING TOOLS USED N1 N2 N3 N4 N5 N6 Informational lecture Multimedia presentation Solution of problems Application of Excel for specialist calculations. Realization of experiments. Report description. 30 2 2 2 2 2 2 2 2 2 2 2 2 30 Number of hours 3 3 3 3 3 3 3 3 3 3 30 EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) PEK_W01 – Exam PEK_W04 F1 PEK_U01 – Verification colloquium I – class PEK_U02 F2 PEK_U03 Verification colloquium II – class PEK_U04 Cl(ćwiczenia) = (F1+F2)/2 F3 PEK_U05 – Appraise a student's reports and colloquium PEK_U08 after each laboratory exercise. C (laboratory) = mean of reports and colloquium marks C(lecture) PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [15] J. Ciborowski, Podstawy inżynierii chemicznej, WNT, Warszawa1982 [16] M. Serwiński, Zasady inżynierii chemicznej i procesowej, WNT, Warszawa 1982 [17] Koch Roman, Noworyta Andrzej: Procesy mechaniczne w inżynierii chemicznej. Warszawa : WNT, 1992. [18] Koch Roman, Kozioł Antoni: Dyfuzyjno-cieplny rozdział substancji. Warszawa : WNT, 1994. [19] Zadania rachunkowe z inżynierii chemicznej, (pr. zbiorowa pod red. R.Zarzyckiego), PWN W-wa 1980. [20] Z. Kawala, A. Kołek, M. Pająk, J. Szust, Zbiór zadań z podstawowych procesów inżynierii chemicznej cz. I – III. Skrypty PWr. [21] Laboratorium Inżynierii Procesowej cz.I. Przenoszenie pędu i procesy mechaniczne oraz cz.II. Przenoszenie ciepła i masy – praca zbiorowa pod redakcją Danuty BelinyFreundlich, Wrocław 1981. [22] [2] Instrukcje do ćwiczeń, dostępne na stronie Wydziału Chemicznego PWr. SECONDARY LITERATURE: [17] K.F.Pawłow, P.G.Romankow, A.A.Noskow. Przykłady i zadania z zakresu aparatury i inżynierii chemicznej, WNT W-wa 1988 [18] Selecki A., Gradoń L., Podstawowe procesy przemysłu chemicznego, WNT, Warszawa1985. [19] Kembłowski Z., Podstawy teoretyczne inżynierii chemicznej i procesowej, WNT, Warszawa 1985 [20] Hobler T., Ruch ciepła i wymienniki, WNT, Warszawa1986. SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Dr inż. Wojciech Skrzypiński, [email protected] 31 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Chemical Engineering AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical Technology Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** Programme content*** Teaching tool number*** K1Atc_W12 C1 Wy1 N1, N2 PEK_W02 K1Atc_W12 C2, C3, C8,C9 PEK_W03 PEK_W04 (skills) PEK_U01 PEK_U02 PEK_U03 K1Atc_W12 K1Atc_W12 C3, C4 K1Atc_U09 C5 K1Atc_U09 K1Atc_U09 C6, C7 C8 PEK_U04 K1Atc_U09 C9 PEK_U05 K1Atc_U14 C10 PEK_U06 K1Atc_U14 C11 PEK_U07 K1Atc_U14 C12 (knowledge) PEK_W01 (knowledge) PEK_W01 K1Atc_U14 C13 PEK_U08 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 32 Lec 1, Lec 5, Lec 7, Lec 8, Lec 15 Lec 2 – Lec 15 Lec 2 – Lec 15 Cl 1 – Cl 4, Cl 7 – Cl 9 Cl 5, Cl 10, Cl 11 Cl 4, Cl 5, Cl 7 – Cl 14 Lab2, Lab4 Lab2, - Lab5, Lab7, - Lab10 Lab5, - Lab7, Lab10 Lab8 N1, N2 N1, N2 N1, N2 N3, N4 N3, N4 N3, N4 N3, N4 N5, N6 N5, N6 N5, N6 N5, N6 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Technologia chemiczna-surowce i procesy przemysłu organicznego Name in English Chemical technology-raw materials and organic industry processes Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Chemical Technology 1st level, full-time / part-time* obligatory TCC015006 YES *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 45 60 30 120 90 60 Examination crediting with grade crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 4 1,5 3 2 2 1 PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 11. Principles of organic chemistry SUBJECT OBJECTIVES C1 C2 C3 C4 C5 C6 Gaining of basic knowledge on technology of petroleum, coal and natural gas and the manufacture of chemicals from petroleum and natural gas hydrocarbons Gaining of basic knowledge on the large scale manufacture of organic chemicals Gaining of basic knowledge on polymeric materials: classification, structure, preparation, processing methods, properties and application Gaining of basic knowledge on fine chemicals manufacturing Gaining of knowledge on fabrication technologies of polymer materials Gaining of knowledge on classification and application of surfactants and pesticides including the green chemistry products 33 C7 Acquaintance with synthesis methods of selected chemical compounds and selected technological processes in laboratory- scale SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: Student, who has completed the course: PEK_W01 – has a knowledge on technology of petroleum PEK_W02 – has a knowledge on processing of petroleum hydrocarbons for chemical industries PEK_W03 –has a knowledge on coal conversion processes PEK_W04 – has knowledge on the processing natural gas to pipeline dry gas quality levels PEK_ W05 – has knowledge on production of chemicals from natural gas PEK_ W06 – knowing basic unit processes (e.g., oxidation, alkylation, hydrogenation, halogenation) in chemical organic technology PEK_ W07 – knowing basic isolation and fabrication methods of the most important reagents for syntheses in the large and small volume scale PEK_W08 – has knowledge on the basic chemical and technological principles PEK_W09 – has knowledge on the catalysts importance in chemical technology and green chemistry PEK_W0Y1 – has knowledge on basic synthesis methods of polymers PEK_W0Y2 – has knowledge on main polymers and their applications PEK_W0Y3 – has knowledge on features of chemical and physical structure of polymeric materials with connection to their properties PEK_W0Y4 – knows the basic preparation and molding methods of polymeric materials along with examples of typical products PEK_W0Y5 –knows the main methods of property determination of polymeric materials PEK_W0Y6 –knows the ways of disposal and management of polymer waste Relating to skills: Student, who has completed the course: PEK_U01 – can discuss the fundamental aspects of technological process PEK_U02 – can discuss the process course in industrial plant PEK_U03 – can define the requirements with respect to raw materials for organic syntheses and their gaining methods PEK_U04 – can evaluate the process with respect to by-products PEK_U05 – can diversify integrated processes with respect to raw materials and products PEK_U06 – can prepare the multimedia and oral presentations PEK_U07 – can prepare the case study from the seminar subject area PEK_U08 –is able to conduct synthesis of selected chemical compounds in laboratory-scale PEK_U09 – is able to perform selected operations of technological process in laboratory conditions … 34 PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 Lec 9 Lec 10 Lec 11 Lec 12 Lec 13 Lec 14 Lec 15 Form of classes - lecture Criteria for petroleum technology evaluation . Hydroprocessing technologies in petroleum industry Processes for converting high-boiling petroleum fractions (catalytic cracking, hydrocracking). The interrelationship of the refinery processes Sources of petrochemical intermediates (aromatics, olefins): reforming, cracking processes Chemical processing of coal: coking coal process, coal gasification Processes for natural gas purification and hydrocarbons separation. Natural gas use Technological principles of manufacturing/chemical processing. Manufacturing of hydrogen and synthetic gas Hydrogenation and dehydrogenation processes. Catalysts in organic technology Syntheses of organic compounds from cabon dioxide and hydrogen Oxidation processes in gaseous and liquid phases Technological processes in green chemistry. Catalysts in green chemistry Basic definitions and concepts connected with polymer technology Mechanisms and technological polymerization methods Chemical and physical structure and properties of polymers Polymer additives and methods of polymer molding Methods of property evaluation, disposal and recycling of polymers Total hours Lab 1 Lab 2 Lab 3 Lab 4 Lab 5 Lab 6 Lab 7 Lab 8 Lab 9 Lab 10 Lab 11 Lab 12 Form of classes - laboratory Introduction. Presentation of laboratory room. Acquaintance with health and safety (HS) regulations. Division into groups. Processes for base oil production. Hydrogenation of aromatics in oil fractions. Methylnaphtalene hydrogenation Process of coal coking Hydrochlorination of organic compounds Oxidation processes. Oxidation of xylenes Synthesis of esters. Methyl esters of higher fatty acids Oxyalkylenated processes. Oxyalkylenation of alcohols Oxyalkylenated processes. Reaction of epichlorohydrin with alcohols Polymer processing Copolymerization of styrene and maleic anhydride Suspension polymerization. Preparation of poly(methyl 35 Number of hours 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 45 Number of hours 4 4 4 4 4 4 4 4 4 4 4 4 Lab 13 Lab 14 Lab 15 metacrylate) Polycondensation - preparation of phenol-formaldehyde resin Evaluation methods of physico-chemical properties of polymers Additional laboratory class 4 4 4 60 Total hours Sem 1 Sem 2 Sem 3 Sem 4 Sem 5 Sem 6 Sem 7 Sem 8 Sem 9 Sem 10 Sem 11 Sem 12 Sem 13 Sem 14 Sem 15 N1 N2 N3 N4 Form of classes - seminar Alkylation; isobutane alkylation with olefins C3-C4, benzene alkylation with ethylene/propylene Alkylation processes; isobutylene o-alkylation with methanol Halogenation; methane chlorination, benzene chlorination Chemicals from ethylene: ethanol, vinyl chloride, acetic acid and acetic anhydride Chemicals from ethylene: ethylene oxide – ethylene glycol Chemicals from propylene: allyl chloride, epichlorohydrin, glycerol Propylene oxidation to acrolein, production of acrylic acid Chemicals from propylene: acrylonitrile, propylene oxide – propylene glycol. Technical ways of polymer preparation: polyethylene, polypropylene Preparation of organic polymers: poly(vinyl chloride), polystyrene, rubbers Preparation of organic polymers: phenoplastics and aminoplastics polyesters, polyamides, epoxide resins Preparation of organic polymers: polyurethanes, silicones Pesticides: classification, herbicides, fungicides Pesticides: zoocides Surface active compounds: ionic surfactants Surface active compounds: nonionic surfactants Renewable starting materials; characteristics of biomass, cellulose, plants Principles of green chemistry in chemical technology Progress directions of chemical technology - examples Natural and synthetic biodegradable materials Disposal and management of organic post-fabrication and postconsumer waste Completion seminar Total hours Number of hours TEACHING TOOLS USED Lecture with multimedia presentation Laboratory workplaces with equipment for product fabrication (synthesis or molding) and determination of product properties Workplaces for conducting of technological processes in laboratory-scale Multimedia presentation of selected problems from the course subject area 36 2 2 2 2 2 2 2 2 2 2 2 2 2 2 30 EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect number Way of evaluating educational effect Evaluation F – forming (during achievement semester), C – concluding (at semester end) P1 (lecture) F1 F2 F3 P2 (seminar) F1 F2 P2 (laboratory) PEK_W01-PEK_W15 PEK_W01-PEK_W05 PEK_W06 – PEK_W09 PEK_W10 – PEK_W15 Final grade = (0,7 F1 + 0,3 F2) PEK_U01-PEK_U02…… PEK_U01-PEK_U02…… Final grade = (0,7 F1 + 0,3 F2) Final examination Multimedia presentation report PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [23] E. Grzywa, J. Molenda, Technologia podstawowych syntez organicznych, tom I i II, WNT, Warszawa, 2000 [24] J. Pielichowski, A. Puszyński A., Technologia polimerów, W N-T, Warszawa, 2003 [25] Koksownictwo, pod red. H. Zielińskiego, Wydawnictwo Śląsk, Katowice 1986. [26] M. Taniewski, Przemysłowa synteza organiczna, 1991 [27] Podstawy recyklingu tworzyw sztucznych (red. M. Kozłowski), Wyd. Politechniki Wrocławskiej, 1998 [28] B. Burczyk, „Zielona chemia. Zarys”, Oficyna Wydawnicza Politechniki Wrocławskiej, 2006 SECONDARY LITERATURE: [21] J. A. Moulijn, M. Makkee, A van Dioepen, Chemical Process Technology, Ed. John Wiley & Sons Ltd, 2001 [22] J. Molenda Technologia Chemiczna, Wyd. Szkolne i Pedagogiczne, W-wa 1997 [23] Chemia polimerów T. 1-3 (red. Z. Floriańczyk, S. Penczek), Wyd. Politechniki Warszawskiej 1997 [24] T. Paryjczak, A. Lewicki, M. Zaborski, „Zielona chemia”, PAN Łódź, 2005 SUBJECT SUPERVISORS prof. dr hab. inż. Jolanta Grzechowiak, prof. dr hab. inż. Kazimiera A. Wilk, prof. dr hab. inż. Ryszard Steller 37 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Chemical technology-raw materials and organic industry processes AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical Technology Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** Programme content*** Teaching tool number*** K1Atc_W14, T1A_W03 C1 Lec1,2 N1 K1Atc_W14, T1A_W03 K1Atc_W14, T1A_W03 K1Atc_W14, T1A_W03 C1 C1 C1 Lec 3 Lec 4 Lec 5 N1 N1 N1 K1Atc_W14, T1A_W03 C1 Lec 5 N1 PEK_U02 K1Atc_W14, T1A_W03 C2 PEK_U03 K1Atc_W14, T1A_W03 C2, C4 … K1Atc_W14, T1A_W03 C4 Lec 6, Lec 7, Lec 8 Lec 7, Lec 8, Lec 9 Lec 6, Lec 9 K1Atc_W14, T1A_W03 C6 Lec 6, Lec 10 N1 Lec 11 Lec 12 Lec 13 Lec 14 Lec 15 N1 N1 N1 N1 N1 Sem1-15 N4 Se1-15 N4 Se1-15 N4 Se1-15 N4 Se1-15 N4 Se1-15 N4 Se1-15 N4 Lab5-15 N2, N3 La1-4 N2, N3 (knowledge) PEK_W01 PEK_W02 PEK_W03 … (skills) PEK_U01 (competences) PEK_K01 PEK_K02 PEK_K03 … K1Atc_W14, T1A_W03 C3 K1Atc_W14, T1A_W03 C3 K1Atc_W14, T1A_W03 C3 K1Atc_W14, T1A_W03 C5 K1Atc_W14, T1A_W03 C5 K1Atc_U21, T1A_U04 T1A_U05 C4-C6 InzA_W05 K1Atc_U21, T1A_U04 T1A_U05 C4-C6 InzA_W05 K1Atc_U21, T1A_U04 T1A_U05 C4-C6 InzA_W05 K1Atc_U21, T1A_U04 T1A_U05 C4-C6 InzA_W05 K1Atc_U21, T1A_U04 T1A_U05 C4-C6 InzA_W05 K1Atc_U21, T1A_U04 T1A_U05 C4-C6 InzA_W05 K1Atc_U21, T1A_U04 T1A_U05 C4-C6 InzA_W05 K1Atc_U20, T1A_U08, InzA_U01 C7 T1A_U12, InzA_U04 K1Atc_U20, T1A_U08, InzA_U01 C7 T1A_U12, InzA_U04 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 38 N1 N1 N1 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Technologia chemiczna-surowce i nośniki energii Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Chemical technology Chemical technology-raw materials and energy carriers 1st level, full-time obligatory TCC014004 YES *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 15 45 15 30 60 60 Examination Crediting with grade Crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 1 2 2 0,5 1,5 0,5 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 12. 13. Introduction to organic chemistry Technical organic chemistry SUBJECT OBJECTIVES C1 C2 C3 C4 C5 Introduction to the constitution and properties of coal and coke making. Getting knowledge of methods and principles of determining composition and coking properties of coal according to the standards. Getting the elements of knowledge of group and fraction composition of petroleum and technology of hydrocarbon fuel production Getting knowledge of using natural gas. Getting knowledge of determining physicochemical properties of hydrocarbon fuels. 39 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – has the elements of knowledge about resources and production of fossil fuels and their processing PEK_W02 – knows the chemical constitution of coal PEK_W02 – has knowledge of technological properties of coal PEK_W04 – knows the elements of knowledge about of coke production PEK_W05 – has the knowledge of crude oil classification and related crude oil processing PEK_W06 – knows the elements of knowledge about technology of hydrocarbon fuel production PEK_W07 – has the knowledge of natural gas processing Relating to skills: PEK_U01 – has capability for determining basic physicochemical and technological properties of coal according to the ISO standards PEK_U02 – has skills of calculating the parameters characterizing of coal on different basis of coal (as received, dry, dry and ash free basis) PEK_U03 – has capability for evaluating coal type and coal as energy source PEK_U04 – has capability of determining the basic physicochemical properties of petroleum and hydrocarbon fuels PEK_U05 - has capability of evaluating utilizable properties of fuels based on their physicochemical properties PEK_U06 – has capability of preparing PowerPoin presentation and giving oral presentation PEK_U07 – has capability of preparing elaboration on the topic related with the subject of seminar. PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 Lec 9 Lec 10 Lec 11 Form of classes - lecture Occurrence, reserves and exploitation of lignites and hard coals Coal processing as chemical and energy source The components of coal: moisture and mineral matter. Types of moisture. Composition of mineral matter occurring in coal. Determination of moisture and mineral matter of coal. Influence of moisture and mineral matter on the coal processing. The components of coal: organic substance. The elemental composition of fossil fuels. Functional groups of C, H, N, S and O in the coal structure. The Wiser’s chemical model of coal structure. Technological properties of coal as energy source. Calorific value and heating value. Classification of coals for energy production. Behavior of coal during devolatilization. Coking properties of coal. Influence of coal rank on the coking properties. Coal classification according to the types. Coke making technology. Processing of crude coking gas and tar. Occurrence and reserves of petroleum and natural gas. Chemical and technological classification of petroleum. Technological processes related with gasoline production. 40 Number of hours 1 1 1 1 1 1 1 1 1 1 1 Lec 12 Lec 13 Lec 14 Lec 15 Technological processes related with diesel oil production. Technological processes related with fuel oil production. Composition of natural gas. Installations for natural gas processing. Natural gas – energy source, engine fuel and raw material for chemical industry Total hours Lab 1 Lab 2 Lab 3 Lab 4 Lab 5 Lab 6 Lab 7 Lab 8 Form of classes - laboratory Introduction to laboratory. Getting knowledge of safety according to the rules of BHP. Division into the laboratory groups. Proximate analysis of coal and biomass. Determination of moisture, ash and volatile matter. Determination of sulfur in coal and biomass by combustion method at high temperature with acid-base titration. Determination of caking ability by Roga method (RI) and swelling index (SI) Properties of fuel fraction. Properties and classification of petroleum. Composition of petroleum and natural gas. Supplementary laboratory classes. Total hours Form of classes - seminar Sem 1 Sem 2 Sem 3 Sem 4 Sem 5 Sem 6 Sem 7 Sem 8 N1 N2 N3 N4 Biomass. Composition, properties and processing. Methods of determining the composition and technological properties of coal. Coking process. Properties and application of coke. Occurrence, resources and exploration of petroleum. Primary and secondary petroleum processing. Fuels for transport and oil fuels. Methods for examining physicochemical properties of petroleum and hydrocarbon fuels. Total hours 1 1 1 1 15 Number of hours 3 6 6 6 6 6 6 6 45 Number of hours 2 2 2 2 2 2 2 15 TEACHING TOOLS USED Lecture with PowerPoint presentation. Laboratory equipment for determining the physicochemical properties of coal according to the standards. Laboratory equipment for determining the physicochemical properties of hydrocarbon fuels according to the standards. Standards for testing and standards for products. PowerPoint presentation concerning the topics of the subject. 41 EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect number Way of evaluating educational effect Evaluation F – forming (during achievement semester), C – concluding (at semester end) P1 (lecture) F1 F2 P2 (laboratory) F1 F2 P3 (seminar) PEK_W01-PEK_W07 examination PEK_U01-PEK_U05 test, report PEK_U01-PEK_U05 grade for experiment performance Final grade = (0.7 F1 + 0.3 F2) PEK_U01-PEK_U07 presentation PEK_U01-PEK_U07 elaboration Final grade = (0.5 F1 + 0.5 F2) PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [29] B.Roga, K.Tomków, Chemiczna technologia węgla, WNT, Warszawa 1971 [30] Koksownictwo, pod red. H. Zielińskiego, Wydawnictwo Śląsk, Katowice 1986. [31] J.R.Grzechowiak, Fizykochemia ropy naftowej, Wyd. PWr, Wrocław 1987 [32] J.Molenda, Gaz ziemny, WNT, Warszawa 1993. SECONDARY LITERATURE: [25] Chemia i fizyka węgla, red. S. Jasieńko, Wyd. PWr, Wrocław 1995. [26] Edward Grzywa, Jacek Molenda, Technologia podstawowych syntez organicznych, t.2 WNT, Warszawa 2000. SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Prof. Grażyna Grylewicz, [email protected] 42 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Chemical technology – Raw materials and energy carriers AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical technology Subject educational effect (knowledge) PEK_W01 PEK_W02 PEK_W03 PEK_W04 PEK_W05 PEK_W06 PEK_W07 Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** Programme content*** Teaching tool number*** K1Atc_W15, T1A_W03 C1 Lec1-8 N1 K1Atc_W15, T1A_W03 K1Atc_W15, T1A_W03 K1Atc_W15, T1A_W03 K1Atc_W15, T1A_W03 K1Atc_W15, T1A_W03 K1Atc_W15, T1A_W03 C1 C1 C1 C3, C4 C3, C4 C3, C4 Lec1-8 Lec1-8 Lec1-8 Lec9-15 Lec9-15 Lec9-15 N1 N1 N1 N1 N1 N1 Lab2-4 N2 Lab2-4 N2 Lab2-4 N2 Lab5-8 N3 Lab5-8 N3 Sem1-8 Sem1-8 N4 N4 K1Atc_U22, T1A_U08, InzA_U01, C2 T1A_U13, InzA_U05 K1Atc_U22, T1A_U08, InzA_U01, C2 PEK_U02 T1A_U13, InzA_U05 K1Atc_U22, T1A_U08, InzA_U01, C2 PEK_U03 T1A_U13, InzA_U05 K1Atc_U22, T1A_U08, InzA_U01, C5 PEK_U04 T1A_U13, InzA_U05 K1Atc_U22, T1A_U08, InzA_U01, C5 PEK_U05 T1A_U13, InzA_U05 K1Atc_U23, T1A_U04, T1A_U05 C1, C3, C4 PEK_U06 K1Atc_U23, T1A_U04, T1A_U05 C1, C3, C4 PEK_U07 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above (skills) PEK_U01 43 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Ochrona przed korozją i elektrochemiczne procesy produkcyjne Name in English Corrosion protection and industrial electrochemical processes Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Chemical technology 1st/ 2nd* level, full-time / part-time* obligatory / optional / university-wide* TCC010007 YES / NO* *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 30 60 Examination / crediting with grade* For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 14. 15. Chemical technology - basic Physical chemistry - basic SUBJECT OBJECTIVES C1 C2 C3 C4 Delivering knowledge of the basics of corrosion processes and corrosion types. Introducing the students to the corrosion prevention methods from the aspect of environment, metal, and appliance of interest. Delivering information about the specificity of electrochemical processes performed on a laboratory and industrial scale. Discussion of the basic processes of industrial electrolysis and metal production by the electrochemical method. 44 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: Any person who has got a credit of the subject: PEK_W01 – knows the basics of corrosion processes, including the main types of corrosion; PEK_W02 – is able to propose a pertinent type of corrosion protection in definite conditions of metal exploitation; PEK_W03 – understands specificity of the electrochemical processes performed on a laboratory and industrial scale; PEK_W04 – knows the basic chemical technologies using electrolysis processes. PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 Lec 9 Lec 10 Lec 11 Lec 12 Lec 13 Lec 14 Lec 15 Lec 16 Lec 17 Form of classes - lecture The basics of corrosion processes. Economic aspect and safety issues related to metal corrosion. General criteria of corrosion prevention. The protection in the stage of designing – selection of materials, the shape of a construction. Modification of corrosion environment. Electrochemical protection – cathodic and anodic ways. Protection by means of coating. Organic coatings, including lacquer ones, and inorganic coatings. Metal protective coatings – the cathodic and anodic ones. Corrosion inhibitors in water media. Volatile inhibitors of corrosion. Temporary protection. Partial test. Basics of the electrochemical techniques of production. Electrolysis of chloride water solutions. Other electrolytic processes performed on an industrial scale. Production of metallic coatings on a laboratory scale. Galvanizing plants. Electrolysis in molten salts. Metal electrorefining. Electrochemical and electropolishing working of metals. Electrodialysis processes, electrophoresis and electrorefining. Partial test. Total hours TEACHING TOOLS USED N1 N2 Informative lecture Monographic lecture 45 Number of hours 2 2 2 2 2 2 2 1 1 2 2 2 2 2 2 1 1 30 EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) PEK_W01 – Part test-colloquium PEK_W02 F2 (lecture) PEK_W03 – Part test-colloquium PEK_W04 C (lecture) = Condition to be credited: positive grades from both partial tests. 3,0 if (F1 +F2) = 6,0 – 6,5 3,5 if (F1 +F2) = 7,0 – 7,5 4,0 if (F1 +F2) = 8,0 4,5 if (F1 +F2) = 8,5 – 9,0 5,0 if (F1 +F2) = 9,5 – 10,0 5,5 if (F1 +F2) = 10,5 – 11,0 F1 (lecture) PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [33] Ciszewski A., Technologia chemiczna. Procesy elektrochemiczne, Wydawnictwo Politechniki Poznańskiej, Poznań, 2008. [34] Revie R.W., Uhlig’s corrosion handbook, J. Wiley & Sons, New York, 2000. [35] Dylewski R., Gnot W., Gonet M., Elektrochemia przemysłowa, Wydawnictwo Politechniki Śląskiej, Gliwice, 1999. [36] Bala H., Korozja materiałów –teoria i praktyka, Wydawnictwo Politechniki Częstochowskiej, Częstochowa, 2002. SECONDARY LITERATURE: [27] Ciszewski A., Podstawy inżynierii elektrochemicznej, Wydawnictwo Politechniki Poznańskiej, Poznań, 2004. [28] Fontana M.G., Greene N.D., Corrosion Engineering, McGraw-Hill Book Company, New York, 1986. [29] Wranglen G., Podstawy korozji i ochrony metali, WNT, Warszawa, 1985. SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Prof. dr hab. inż. Bogdan Szczygieł, [email protected] 46 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Corrosion protection and industrial electrochemical processes AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical technology Subject educational effect (knowledge) PEK_W01 PEK_W02 PEK_W03 Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** Programme content*** Teaching tool number*** optional C1 Lec1, Lec 8 N1 C2 C3 Lec 2- Lec 8 Lec 9, Lec 17 Lec 10 – Lec 17 N1, N2 N1 C4 PEK_W04 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 47 N1, N2 Zał. nr1a do ZW 4/2015 DEPARTMENT OF HUMANITIES AND SOCIAL SCIENCES FACULTY OF CHEMISTRY SUBJECT CARD Filozofia nauki i techniki Name in Polish Name in English Philosophy of Science and Technology Main field of study (if applicable): Chemical Technology Specialization (if applicable): …………………….. Level and form of studies: 1st/ 2nd* level, full-time / part-time* Kind of subject: obligatory / optional / university-wide* Subject code FLC028002 Group of courses YES / NO* Lecture Classes Number of hours of 10 organized classes in University (ZZU) Number of hours of total 60 student workload (CNPS) Crediting Form of crediting Examination / with grade crediting with grade* Laboratory Project Seminar Examination / crediting with grade* Examination / crediting with grade* Examination / crediting with grade* For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 0,5 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES Basic knowledge from the field of humanities and social sciences. \ SUBJECT OBJECTIVES C1 Introducing the students to main issues of philosophy of science and technology, including methods of inference and different types of rationalities. C2 Identification and analysis of the problem of relations between science and technology and their mutual development. C3 Expounding non-technical aspects of engineering activity and elucidating the problem of social responsibility of science and technology. 48 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_ HUM W07 – The student obtains knowledge on recognized methods of inference (inductive, deductive, abductive) and on main philosophical issues related to science and technology. PEK_ HUM W08 – The student obtains knowledge essential to understanding and interpreting social and philosophical aspects of engineering activity. Relating to social competences: PEK_ HUM K02: The student is aware of the importance of non-technical aspects of engineering of a chosen specialty and understands the consequences of engineering activity in terms of its environmental and social impact as well as their responsibility for making decisions; the student understands the need for constant learning; the student is capable of inspiring and organizing the process of learning others; the student correctly identifies and analyzes dilemmas related to their profession; the student is aware of a social role of technical university graduates, with a special focus on the need to inform society and the media on developments of science and technology; the student is able to undertake efforts to communicate such informations and opinions in a clear way and give justifications to different points of view; the student is able to think critically and give arguments for their opinions. PROGRAMME CONTENT Number of hours Form of classes - lecture Lec 1 Introduction: philosophy of science and technology in a wider context of philosophical disciplines. Lec 2 Recognized methods of inference. 2 Lec 3 The problem of a definition of science, criteria of scientific knowledge and classification of sciences. Lec 4 Development of science: the problem of empirical data and other chosen issues. Lec 5 Types of rationality and definitions of technology. 2 Relations between technology and science; chosen issues of non-technical aspects of technology. 2 Lec 6,7 2 1 1 Total hours 10 Form of classes - class Cl 1 Cl 2 Cl 3 Cl 4 .. Total hours 49 Number of hours Form of classes - laboratory Number of hours Lab1 Lab2 Lab3 Lab4 Lab5 … Total hours Number of hours Form of classes - project Proj1 Proj2 Proj3 Proj4 … Total hours Form of classes - seminar Number of hours Sem1 Sem2 Sem3 … Total hours TEACHING TOOLS USED N1. Multimedial presentation. N2. Informative lecture. N3. Interactive lecture. EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Way of evaluating educational effect achievement Evaluation(F – Educational forming (during effect number semester), P – concluding (at semester end) F1 PEK_ HUM W07 PEK_ HUM W08 PEK_ HUM K01 Written essay prepared on the basis of the lecture and selected literature or a test written in class. P=F1 PRIMARY AND SECONDARY LITERATURE 50 PRIMARY LITERATURE: [37] V. Dusek, Wprowadzenie do filozofii techniki, tłum. Zbigniew Kasprzyk, Kraków 2011 [38] M. Heller, Filozofia nauki. Wprowadzenie, Kraków 2009 [39] J. Woleński, Epistemologia, Warszawa 2005. SECONDARY LITERATURE: [30] J.M. Bocheński, Współczesne metody myślenia, Poznań 1993 [31] A. Grobler, Metodologia nauk, Kraków 2008 SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Łukasz Mścisławski, [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Philosophy of Science and Technology AND EDUCATIONAL EFFECTS FOR TECHNICAL SCIENCES Subjecteducationaleffect Correlation between Subjectobjectives*** Programmecontent*** Teachingtoolnumber*** (knowledge) PEK_ HUM W07 PEK_ HUM W08 (competences) PEK_ HUM K01 subject educational effect and educational effects defined for main field of study and specialization (if applicable)** T2A_W07 C1, T2A_W08 T2A_K01, T2A_K02, T2A_K05, T2A_K07 C2, C3 Lec 1- Lec 7 N1, N2, N3 C1, C2, C3 Lec 1- Lec 7 N1, N2, N3 ** - enter symbols for main-field-of-study/specialization educational effects *** - from tableabove 51 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Chemia Techniczna Nieorganiczna Inorganic Technical Chemistry Chemical Technology 1st level, full-time obligatory CHC013007 NO *delete as applicable Lecture Classes Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Laboratory Project Seminar 30 60 Crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 2 2 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 16. 17. Basic knowledge in the field of inorganic chemistry Knowledge of the subject realized during the laboratory exercises SUBJECT OBJECTIVES C1 C2 C3 Knowledge of industrial processes for the production of basic chemicals in inorganic chemical technology Knowledge of raw materials and products of inorganic chemistry Gain knowledge and skills related to analytical aspects of technological processes 52 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: The person who passed the object: PEK_W01 - has knowledge in the field of the structures and properties of the chemicals and chemical reactions which are used in the technological process PEK_W02 - knows the selected processes and unit operations used in chemical technology under laboratory conditions Relating to skills: The person who passed the object: PEK_U01 - has the ability of assess the quality of raw materials and industrial products PEK_U02 - can use in the practice various analytical techniques PEK_U03 - can perform chemical experiments PEK_U04 - can describe the chemical experiments in the form of report PROGRAMME CONTENT Form of classes - laboratory Number of hours Lab 1 General working instructions in the laboratory, training (Occupational safety and health). Knowledge of basic equipment and reagents in the laboratory. Learning basic laboratory activities. 2 Lab 2 Obtaining of acids and bases – obtaining of boric acid and sodium hydroxide 4 Lab 3 Obtaining of double salts – obtaining of aluminum potassium sulfate 4 Lab 4 Batch culture of yeast 4 Lab 5 Taking of gaseous samples and gas chromatography analysis of composition of those samples 4 Lab 6 Practical electrochemical chain and corrosion’s macrocells 4 Lab 7 Preparation of soda using Solvay method 4 Lab 8 Determination of density and porosity of ceramic materials 4 Total hours 30 TEACHING TOOLS USED N1 N2 Performing experience Preparation of reports EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect number Way of evaluating educational effect Evaluation F – forming (during achievement semester), C – concluding (at semester end) 53 F1(laboratory) PEK_W01 - PEK_W02 preliminary small exam (max. 14 points) F2(laboratory) PEK_U01 - PEK_U04 laboratory report (max. 14 points) P (laboratory) = 3.0 if (F1+F2/2) = 11.0 – 12.5 points 3.5 if (F1+F2/2) = 13.0 – 14.5 points 4.0 if (F1+F2/2) = 15.0 – 16.5 points 4.5 if (F1+F2/2) = 17.0 – 18.5 points 5.0 if (F1+F2/2) = 19.0 – 20.5 points 5.5 if (F1+F2/2) = 21.0 points PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [1] Instructions for exercises [2] J. Barycka, K. Skudlarski, Podstawy chemii, Wyd.PWr, Wrocław, 2001, [3] L. Jones, P. Atkins, Chemia ogólna, PWN, Warszawa, 2004 SECONDARY LITERATURE: [1] T. Lipiec, Z. S. Szmal, Chemia analityczna z elementami analizy instrumentalnej, PZWL, Warszawa, 1996 [2] B. Bartkiewicz, Oczyszczanie ścieków przemysłowych, PWN, Warszawa, 2006 SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Ph.D. Eng. Krystyna Hoffmann, [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Inorganic Technical Chemistry AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical Technology Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** (knowledge) K1Atc_U15 C1, C2 PEK_W01 K1Atc_U15 C1, C2, C3 PEK_W02 (skills K1Atc_U15 C1-C3 )PEK_U01 K1Atc_U15 C1-C3 PEK_U02 K1Atc_U15 C1-C3 PEK_U03 K1Atc_U15 C1-C3 PEK_U04 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 54 Programme content*** Teaching tool number*** La2-La8 N1, N2 La1-La8 N1, N2 La1-La8 N1, N2 La1-La8 La2-La8 La2-La8 N1, N2 N1, N2 N1, N2 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Zasady inwestowania i eksploatacji instalacji chemicznych Name in English Investment and chemical plants maintenance principles Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses 1st/ level, full-time optional ZMC010007 NO *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 30 60 crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 2 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 1 Basic knowledge of chemical technology 2 Basic knowledge of chemical engineering SUBJECT OBJECTIVES C1 familiarize students with the problem of the competitiveness of the chemical industry C2 Understanding the principles of C2 organization of the market of raw materials and chemical products, as well as the sectoral distribution of production tasks in a "business to business" C3 familiarize students with legal, organizational investment and chemical production 55 C4 C5 C6 and waste products and the industry Gaining knowledge about the most important manufacturing sectors in the chemical industry, the raw material base and cooperative relationship with the chemical processing industries, the impact of the chemical on the environment belief students about the essential role of research and development and innovation in the chemical industry. familiarize students with the organization of the investment process and management systems, linkages with other industries co-operation partners, the organization of industry infrastructure for the storage, transport and distribution of SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 - Know the task of production and the role of the chemical industry in the global economy, the European Union and the domestic industry PEK_W02 Student knows the problems organizational, economic, technological and basic regulations for the operation of the chemical industry PEK_W03t Can be made for investment, operation system in accordance with the requirements of environmental protection and the principles of the IPPCIntegrated Pollution Prevention Control PEK_W04-Student knows responsibility for maintaining a healthy and environmentally friendly production, the existing emission standards, the principles of waste management PEK_W05- Students have basic knowledge of the certification procedure, the conditions of authorization of commercial and broadcasting of the CE mark, knows the principle of life-cycle analysis of the product / life cycle analysis / PEK_W06-Student has a general understanding of the terms and conditions of the competitive chemical production and development trends and the problems of energy, waste management rules, knows the rules of rational water management, attention to air quality, as well as on the principles of innovation. Relating to skills: PEK_U01 – PEK_U02 – … Relating to social competences: PEK_K01 PEK_K02 … 56 PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Form of classes – lecture Condition of the world chemical industry,chemical industry in the European Union and Polish: the level of technologies, BAT/ best available technology/, material resources, conditions of raw materials and energy developments, the competitiveness of chemical sector . Market of the chemical raw materials and chemical products: the competitiveness of the industry, the market, the export of raw materials and products, the problems of political, environmental and social issues in the chemical industry Relation-chemical industry/ environment: basic definitions related to the protection and shaping of the environment, the evolution of relations industry-environment, natural resources and their rational use, renewable resources, basic instruments of environmental protection, environmental policy elements Chemicals Policy of the European Union: the historical evolution of the industry, modern methods of investment and operation of industrial, product innovations and environmental technologies to protect the environment from pollution, closed circulation systems, waste-free method, the characteristics of the issue of the European chemical industry and biotechnology principle of BAT / The Best Available Technology '/ and the implementation of the IPPC Directive / Integrated Pollution Prevention Control / in the development of industry, the REACH program for the safe use of chemicals, the role of integrated permits Energy problems in the chemical industry: the world's energy resources, the impact of energy and consumption of fossil fuels on the competitiveness of the industry, the possibility of reducing energy consumption in industry, promising ways of generating energy, the use of biomass for energy and fuel, the European energy and climate policy, the European Emissions Trading System ECTS Efficient water management in the chemical industry: global resources, global sourcing and water balance, the rational management of water resources, pollution of surface water, protection of water resources, waste water in a chemical plant, point and diffuse sources of water pollution, water treatment, water purification, renewal water, closed water circuits, technological safeguards water resources from contamination by substances eluted from landfills Waste management in the chemical industry: the definition of waste types and legal classification of the wastes, the evolution of methods of disposal and treatment of wastes, the problem of hazardous waste, the safe storage of the waste, hierarchy of waste management methods, principles of "green chemistry" in waste disposal, treatment, waste-free method waste, chemical industry and biotechnology, chemical technology used for the disposal and treatment of waste, the cost of waste management 57 Number of hours 2 2 2 2 2 2 2 Lec 8 Lec 9 Lec10 Lec11 Lec12 Lec13 Lec14 Lec15 Greenhouse gases and dust in the manufacture of chemicals: chemical plant emitter characteristics, the characteristics of gaseous pollutants emission standards and a study of the protection of the atmosphere, methods and devices for purification of gases, transport of gases including changes secondary air protection for indoor / indoor pollution control /, emission standards for selected technologies / BAT / Specific regulations in the chemical industry, with particular emphasis on the impact of the industry and its products on the environment: a system of environmental law, legal instruments for the protection of the environment, environmental impact assessment, the role of regulating the rights of the use of the environment, protection of the environment in international law, Community law, Agenda 21 program, the Global Programme of Action / Rio de Janeiro /, emission standards, regulations governing the working conditions Investing in the chemical industry: the phase of the investment process, local agreements, process design and technical design study of the protection of air, water-sewage system, the principle of the "best available techniques" / BAT / environmental assessment, an integrated maintainence permission Operation chemical systems: decisions on emissions, water permits and legal process management system, ISO 9000, ISO 14000 environmental management system, HACCP principles of process safety, safety at work, exposure limits on workplaces, the cost of environment impact Principles of authorization of market product, the procedure starts production for the market, compliance with Polish standards, CE marking, product certification, quality testing of chemical products, the organization of the quality control system, the analysis of the product life cycle in direction, the analysis of the product life cycle in the environment " life cycle analysis " Infrastructure chemical industry: the organization of the system storage, transportation and distribution of products, technical solutions, packaging products, packaging, labeling system of chemicals, REACH on the market and use of chemicals Innovations basis for the development of the chemical industry: innovation process and raw materials, the role of research and development in the process of innovation, financing innovation, the company's image-trademarks, utility models, industrial designs, the protection of industrial and intellectual property, licenses, know-how lecture summary and final test 2 Total hours Form of classes – class Cl 1 Cl 2 Cl 3 58 2 2 2 2 2 2 2 30 Number of hours Cl 4 … Total hours Form of classes – laboratory Number of hours Lab 1 Lab 2 Lab 3 Lab 4 … Total hours Form of classes – project Number of hours Proj 1 Proj 2 Proj 3 Proj 4 … Total hours Form of classes – seminar Number of hours Sem 1 Sem 2 Sem 3 Sem 4 … Total hours TEACHING TOOLS USED N1 N2 … EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) F1 lecture PEK-W01PEKW06 Final test F2 59 … C PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [1]CEFIC Chemical Reports ,internet [2]M.Górski, Prawo ochrony środowiska,Wolter Kluwer Polska,2009 [3]K.Małachowski, Gospodarka a środowisko i ekologia, wyd.CeDeWu,2011 [4]Raporty Polskiej Izby Przemysłu Chemicznego, internet SECONDARY LITERATURE: [32] Czasopismo PRZEMYSŁ CHEMICZNY [33] Czasopismo CHEMIK SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Prof. dr hab. inż. Henryk Górecki [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT … Investment and chemical plants maintenance principles AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical Technology Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** (wiedza) PEK_W01 K1 Atc W10 C1,C6 PEK_W02 K1 Atc W10 C2,C3,C5,C6, C7 PEK_W03 K1 Atc W10, K1 Atc W12, K1 Atc W15 C5,C6,C7,C8, C9 PEK_W04 K1 Atc W12 C9,C10,C11 PEK_W05 K1 Atc W10 C12 Le 12 N1 PEK_W06 K1 Atc W10, K1 Atc W12, K1 Atc W15 C1,C13,C14 Le1,Le13, Le 14 N1 60 Programme kontent*** Le1, Le 4, Le Le 6 Le 2, Le 3, Le 4, Le 5, Le 6, Le 7 Le 5 Le 6, Le 7, Le 8, Le 9 Le 9 Le 10, Le 11 Teaching tool number*** N1 N1 N1 N1 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Lecture Laboratorium technologii surfaktantów I Laboratory of surfactants technology I Chemical Technology 1st level, full-time obligatory TCC016008 NO Classes Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Laboratory Project Seminar 15 30 crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 1 1 0.5 PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 18. Basic knowledge about the surfactants. 19. Basic knowledge of the surfactants synthesis. 20. Basic knowledge of surfactants practical applications. SUBJECT OBJECTIVES C1 C2 C3 C4 C5 Obtaining knowledge about the types of surfactants. Obtaining detailed knowledge about the methods of synthesis of different groups of surfactants. Gaining knowledge on the analysis of the composition of produced surfactants. Gaining knowledge on how to assess the performance of produced surfactants. To gain knowledge on how to prepare a composition containing surfactants. 61 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – PEK_W02 – ... Relating to skills: PEK_U01 – PEK_U02 – … Relating to social competences: PEK_K01 PEK_K02 … Lab 1 Lab 2 Lab 3 Lab 4 Form of classes - laboratory Synthesis of anionic and nonionic surfactant Determination of properties of synthesized compounds Assessment of the performance of the synthesized surfactants Crediting test Number of hours Total hours N1 N2 N3 N4 TEACHING TOOLS USED Discussion of surfactant types Implementation of a wide range of chemical analyzes in accordance with the instructions Learning the methods for assessing the performance of surfactants Preparation of reports EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) PEK_U01 Crediting test F1 (laboratory) PEK_U06 Max. 11 pts Min. 6 pts PEK_U01 F2 (laboratory) Report PEK_U06 Max. 11 pts Min. 6 pts P (laboratorium) = F1 + F2 3.0 if 12-13 3.5 if 14-15 4.0 if 16-17 4.5 if 18-19 62 6 6 2 1 15 5.0 if 20-21 5.5 if 22 PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [40] Przondo J., Związki powierzchniowo czynne i ich zastosowania w produktach chemii gospodarczej, Radom 2007 [41] Laboratory manual SECONDARY LITERATURE: [34] Anastasiu S., Jelescu E., Związki powierzchniowo czynne, Warszawa 1973 [35] Zieliński, R., Surfaktanty, budowa, właściwości, zastosowania, Poznań 2013 SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Dr inż. Jacek Łuczyński, [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT LABORATORY OF SURFACTANT TECHNOLOGY I AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY CHEMICAL TECHNOLOGY Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** (skills) K1Atc_U34 C1 –C5 PEK_U01 K1Atc_U34 C1 –C5 PEK_U02 K1Atc_U34 C1 –C5 PEK_U03 K1Atc_U34 C1 –C5 PEK_U04 K1Atc_U34 C1 –C5 PEK_U05 K1Atc_U34 C1 –C5 PEK_U06 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 63 Programme content*** Teaching tool number*** Lab1-Lab4 N1 – N4 Lab1-Lab4 Lab1-Lab4 Lab1-Lab4 Lab1-Lab4 Lab1-Lab4 N1 – N4 N1 – N4 N1 – N4 N1 – N4 N1 – N4 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology Faculty of Chemistry SUBJECT CARD Laboratorium technologii surfaktantów II Name in Polish Name in English Laboratory of surfactants technology II Main field of study (if applicable): Chemical technology Specialization (if applicable): Level and form of studies: 1st, full-time Kind of subject: obligatory Subject code TCC017006 Group of courses NO Lecture Classes Laboratory 15 Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Project Seminar 30 Crediting with grade For group of courses mark (X) final course Number of ECTS points 1 1 including number of ECTS points for practical (P) classes including number of ECTS points for direct teacher-student contact (BK) classes 0,5 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 1. Basic knowledge about surfactants 2. General knowledge about surfactants synthesis 3. Basic knowledge about practical aspects of surfactants use \ SUBJECT OBJECTIVES C1 Conquest the knowledge about surfactants applications C2 Conquest the particular knowledge about additives to surfactants compositions C3 Conquest the knowledge about commercial products containing surfactants ingredients analysis C4 Conquest the knowledge about methods of detergents application properties determination C5 Conquest the knowledge about composing applicable mixtures containing surfactants 64 SUBJECT EDUCATIONAL EFFECTS relating to knowledge: PEK_W01 PEK_W02 … relating to skills: PEK_U01 PEK_U02 … relating to social competences: PEK_K01 PEK_K02 Lab 1 Lab 2 Lab 3 Lab 4 PROGRAMME CONTENT Form of classes - laboratory Ingredients analysis of particular commercial products containing detergents (laundry detergents) Application properties determination of commercial products containing dtergents Composing and analysis of own applicable mixtures containing surfactants Test Total hours 8 2 4 1 15 TEACHING TOOLS USED N1. Review of commercial product types containing surfactants N2. Conducting chemical analysis of commercial products according to given instructions N3. Composing own applicable mixtures containing surfactants from proposed ingredients N4. Report preparation EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Evaluation (F – forming Educational effect Way of evaluating educational effect (during semester), P – number achievement concluding (at semester end) F1 PEK_U01 Test PEK_U06 Maks. 11 pkt. Min. 6 pkt F2 PEK_U01 Report PEK_U06 Maks. 11 pkt. Min. 6 pkt F3 C P (laboratory) = F1 + F2 3,0 if 12-13 3,5 if 14-15 4,0 if 16-17 4,5 if 18-19 5,0 if 20-21 5,5 if 22 PRIMARY AND SECONDARY LITERATURE 65 PRIMARY LITERATURE: [1] Przondo J., Związki powierzchniowo czynne i ich zastosowania w produktach chemii gospodarczej, Radom 2007 [2] Laboratory instructions SECONDARY LITERATURE: [1] Anastasiu S., Jelescu E., Związki powierzchniowo czynne, Warszawa 1973 [2] Zieliński, R., Surfaktanty, budowa, właściwości, zastosowania, Poznań 2013 SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Dr Jacek Łuczyński, [email protected] 66 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT …………………………… AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY ……………………….. AND SPECIALIZATION …………………………….. Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** Programme content*** Teaching tool number*** PEK_U01 (skills) K1Atc_U34 C1 –C5 La1-La4 N1 – N4 PEK_U02 PEK_U03 PEK_U04 PEK_U05 PEK_U06 K1Atc_U34 K1Atc_U34 K1Atc_U34 K1Atc_U34 K1Atc_U34 C1 –C5 C1 –C5 C1 –C5 C1 –C5 C1 –C5 La1-La4 La1-La4 La1-La4 La1-La4 La1-La4 N1 – N4 N1 – N4 N1 – N4 N1 – N4 N1 – N4 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 67 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Materiałoznawstwo Materials science Chemical technology Chemical and processing engineering 1st/ 2nd* level, full-time / part-time* obligatory / optional / university-wide* IMC012002 YES / NO* *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 30 60 Examination / crediting with grade* For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 21. Chemistry and physics - basic SUBJECT OBJECTIVES C1 C2 C3 C4 Introducing the students to the repartition of engineering materials Learning the selection rules for a material to a definite application Acquisition of information about usable properties of engineering materials Understanding the relationship material/structure/production method 68 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: Any person who has got a credit of the subject: PEK_W01 – knows basic sorts of engineering materials, bad and good sides of these; PEK_W02 – understands the selection rules for a material to a definite application; PEK_W03 – knows the definitions, importance and means of determination of the main mechanical properties of the materials as the deciding factors for applications in practice; PEK_W04 – has acquired basic information about correlations between materials' properties, structure and production method; PEK_W05 – has acquired basic knowledge about metallic material structure, phase equilibria and transformations; PEK_W06 – knows the basics of rheology in the linear viscoelasticity of polymer materials; PEK_W07 – knows the basics of polymer processing methods. PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 Lec 9 Lec 10 Lec 11 Form of classes - lecture Types of engineering materials: basic advantages and disadvantages of metals, ceramics and plastics. Composites. Types of crystalline materials through the ages. Recent achievements and trends in production of new materials: nanomaterials, shape memory materials etc. Atom structure in light of present-day studies. Types and energies of chemical bonding. Importance of binding energy in properties of materials. Chemical bonds dominating throughout the respective types of engineering materials. Basic information about the crystal structure of materials. Crystal structure of metals. Unit cell. Correlations between the production process, crystal structure and properties of materials. Crystalline and amorphous materials. Mechanical properties of engineering materials. Stress and strain. Elastic and plastic deformations. Static tensile test. Hardness. Impact strength. Cracking resistance. Fatigue. Creep. Crystal structure defects. Substitution and interstitial solid solutions. The crystallographic structure of iron and steel. Metals and alloys. Homogenous and heterogenous alloys. Gibbs phase rule. Phase diagrams for binary systems with a perfect-, partial-, and completely lacking intersolubility. Alloy- and non-alloy steels: obtaining, properties, and applications. Systems of marking the steels. Constructional and tool steels. Cast irons. The system iron-carbon. Non-ferrous metal alloys. Basic information about corrosion of metals. Methods of corrosion protection. Partial test Synthetic engineering materials; historical outline, milestones in discoveries. 69 Number of hours 2 2 2 2 2 2 2 2 1 1 2 Lec 12 Conception of the macroparticle (synthesis methods, radical polymerization, degree of polymerization, polycondensation). Lec 13 Amorphous and semicrystalline polymers, crosslinked polymers (structural models, glass transition temperature, melting point). Lec 14 Rheological models (the Maxwell model, Kelvin-Voigt model, Maxwell three-parameter model; creep, tension relaxation, plastic deformation recovery). Lec 15 Typical machinery to process polymer materials. The operating principle of: injection molding machine; extruder; two-high rolling mill; calender roller; hydraulic press. Rotomolding. Lec 16 PCW example of polymer modification (relationship between structure, composition, and functional properties). Lec 17 Partial test Total hours N1 TEACHING TOOLS USED Informative lecture including a multimedia presentation EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) PEK_W01 – Part test-colloquium PEK_W05 F2 (lecture) PEK_W02, Part test-colloquium PEK_W04, PEK_W06, PEK_W07 C (lecture) - condition to be credited: positive grades from both partial tests. 3,0 if (F1 +F2) = 6,0 – 6,5 3,5 if (F1 +F2) = 7,0 – 7,5 4,0 if (F1 +F2) = 8,0 4,5 if (F1 +F2) = 8,5 – 9,0 5,0 if (F1 +F2) = 9,5 – 10,0 5,5 if (F1 +F2) = 10,5 – 11,0 F1 (lecture) 70 2 2 2 2 1 1 30 PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [42] M. Blicharski, Wstęp do inżynierii materiałowej, WNT, Warszawa, 2003. [43] W.D. Callister Jr, Materials Science and Engineering, Jihn Willey & Sons Inc., New York, 1991. [44] D. Żuchowska, Polimery konstrukcyjne, WNT, Warszawa, 1995. [45] W. Szlezyngier, Tworzywa sztuczne, Oficyna Wydawnicza Politechniki Rzeszowskiej, Rzeszów, 1996. SECONDARY LITERATURE: [36] L.A. Dobrzański, Podstawy nauki o materiałach i metaloznawstwo, WNT, Gliwice, Warszawa, 2002. [37] M. Blicharski, Inżynieria materiałowa. Stal, WNT, Warszawa, 2004. [38] W. Królikiewicz, Polimerowe materiały specjalne, Wydawnictwo Politechniki Szczecińskiej, Szczecin, 1998. SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Prof. dr hab. inż. Bogdan Szczygieł; [email protected] Prof. dr hab. inż. Jacek Pigłowski; [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Materials science AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical technology Chemical and processing engineering Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** (wiedza) PEK_W01 K1Atc_W19, K1Aic_W15 C1 PEK_W02 K1Atc_W19, K1Aic_W15 C2 PEK_W03 PEK_W04 K1Atc_W19, K1Aic_W15 K1Atc_W19, K1Aic_W15 PEK_W05 K1Atc_W19, K1Aic_W15 Teaching tool number*** N1, N2 C3 C4 Lec1, Lec 2, Lec 11 Lec 3, Lec 8, Lec 9, Lec 16 Lec 5, Lec 13 Lec 4, Lec 12 C4 Lec 6, Lec 7 N1, N2 Lec 14 Lec 15 N1 N1 K1Atc_W19, K1Aic_W15 PEK_W06 K1Atc_W19, K1Aic_W15 PEK_W07 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 71 Programme content*** N1 N1 N1 Zał. nr 4 do ZW 33/2012 WYDZIAŁ Chemiczny Nazwa w języku polskim: Nazwa w języku angielskim: KARTA PRZEDMIOTU Miernictwo i Automatyka Measurements and Automatics Kierunek studiów (jeśli dotyczy): Specjalność (jeśli dotyczy): Stopień studiów i forma: Rodzaj przedmiotu: Kod przedmiotu Grupa kursów Wykład Liczba godzin zajęć zorganizowanych w Uczelni (ZZU) Liczba godzin całkowitego nakładu pracy studenta (CNPS) Forma zaliczenia Technologia Chemiczna I stopień, stacjonarna obowiązkowy ETP001002 NIE Ćwiczenia Laboratorium Projekt 15 30 30 60 zaliczenie na ocenę Seminarium zaliczenie na ocenę Dla grupy kursów zaznaczyć kurs końcowy (X) Liczba punktów ECTS w tym liczba punktów odpowiadająca zajęciom o charakterze praktycznym (P) w tym liczba punktów ECTS odpowiadająca zajęciom wymagającym bezpośredniego kontaktu (BK) 1 2 2 0,5 1 *niepotrzebne skreślić 22. WYMAGANIA WSTĘPNE W ZAKRESIE WIEDZY, UMIEJĘTNOŚCI I INNYCH KOMPETENCJI Zaliczony kurs: Fizyka 2 (wyk,cw) i Fizyka 2 (lab.). \ CELE PRZEDMIOTU C1: Uzyskanie podstawowej wiedzy w zakresie pomiarów podstawowych wielkości nieelektrycznych i regulacji automatycznej procesów i obiektów. C2: Nabycie praktycznych umiejętności w zakresie pomiaru podstawowych wielkości nieelektrycznych metodami elektrycznymi oraz obsługi i komputerowego symulowania prostych układów automatyki. 72 PRZEDMIOTOWE EFEKTY KSZTAŁCENIA Z zakresu wiedzy: PEK_W01 – Ma pogłębioną wiedzę w zakresie pomiarów podstawowych wielkości fizycznych oraz automatycznego sterowania procesami i obiektami w przemyśle. PEK_W02 – Zna czujniki i urządzenia do pomiarów podstawowych wielkości fizycznych oraz struktury i działanie układów sterowania i automatycznej regulacji. Z zakresu umiejętności: PEK_U01 - Potrafi mierzyć podstawowe wielkości fizyczne i obsługiwać prosty układ automatycznej regulacji. PEK_U02 - Potrafi stosować praktycznie oprogramowanie komputerowe w zakresie pracy wirtualnych przyrządów pomiarowych oraz symulowania struktur sterowania i regulacji automatycznej. Z zakresu kompetencji społecznych: PEK_K01 - Zna ograniczenia własnej wiedzy w zakresie pomiarów oraz automatyki i rozumie potrzebę dalszego kształcenia. TREŚCI PROGRAMOWE Forma zajęć - wykład W1 W2 W3 W4 W5 W6 W7 W8 Cele i zakres tematyczny przedmiotu, warunki zaliczenia. Pojęcie sprzężenia zwrotnego. Schematy blokowe. Struktury układów regulacji i sterowania automatycznego. Podstawowe człony dynamiczne układów regulacji automatycznej, badanie odpowiedzi na pobudzenie skokowe. Identyfikacja obiektów sterowania. Czujniki pomiarowe temperatury, ciśnienia, natężenia przepływu, poziomu, itp.: właściwości, podstawowe parametry, zastosowanie. Czujniki inteligentne wielkości nieelektrycznych, przetworniki pomiarowe, karty normalizujące ich współpraca z komputerem, interfejsy cyfrowe. Regulacja dwupołożeniowa, ciągła i krokowo-impulsowa. Stabilność i jakość regulacji automatycznej. Elementy wykonawcze. Zasady doboru regulatorów oraz doboru nastaw regulatorów. Symulacja komputerowa w procesie projektowania układów regulacji automatycznej. Przykłady mikrokomputerowych systemów regulacji. Kolokwium zaliczeniowe. Suma godzin Liczba godzin 2 2 2 2 2 2 2 1 15 Forma zajęć - ćwiczenia Liczba godzin Forma zajęć - laboratorium Termin organizacyjny, szkolenie BHP, podział na grupy, regulamin. Prezentacja tematyki ćwiczeń. Liczba godzin Ćw1 Ćw2 Ćw3 Ćw4 .. Suma godzin L1 L2 L3 Czujniki pomiarowe, modele, właściwości zastosowanie. Czujniki temperatury- charakterystyki statyczne. 73 2 2 2 L4 L5 L6 L7 L8 L9 L10 L11 L12 L13 L14 L15 Czujniki temperatury – charakterystyki dynamiczne. Czujniki ciśnienia. Pomiary przepływu. Pomiary przemieszczeń. Waga prądowa. Przyrządy wirtualne – rezystometr. Przyrządy wirtualne – termometr. Człony dynamiczne. Symulacja właściwości dynamicznych obiektówprogram Simulink. Identyfikacja właściwości dynamicznych obiektu cieplnego, regulacja temperatury. Regulacja dwupołożeniowa. Regulacja ciągła. Termin poprawkowy-zaliczenia. Suma godzin Forma zajęć - projekt 2 2 2 2 2 2 2 2 2 2 2 2 30 Liczba godzin Pr1 Pr2 Pr3 Pr4 … Suma godzin Forma zajęć - seminarium Liczba godzin Se1 Se2 Se3 … Suma godzin STOSOWANE NARZĘDZIA DYDAKTYCZNE N1. Tablica i pisaki do wykładu prowadzonego metodą tradycyjną. N2. Elementy prezentacji multimedialnej ilustrujące zagadnienia omawiane na wykładzie. N3. Komputer i oprogramowanie dedykowane do ćwiczeń laboratoryjnych. N4. Testy sprawdzające - krótkie prace pisemne stosowane na zajęciach laboratoryjnych. N5. Sprawozdania z ćwiczeń laboratoryjnych. OCENA OSIĄGNIĘCIA PRZEDMIOTOWYCH EFEKTÓW KSZTAŁCENIA Oceny (F – formująca (w trakcie semestru), P – podsumowująca (na koniec semestru) P F1 Numer efektu kształcenia Sposób oceny osiągnięcia efektu kształcenia PEK_W01 PEK_W02 PEK_U01 PEK_U02 Ocena z kolokwium. 1. 1. Krótkie prace pisemne – testy sprawdzające. 2.Oceny ze sprawozdań z zajęć laboratoryjnych opracowywanych poza zajęciami zorganizowanymi. P – wykład – ocena z kolokwium. 74 F1– zajęcia laboratoryjne – średnia ocen z testów sprawdzających i sprawozdań. LITERATURA PODSTAWOWA I UZUPEŁNIAJĄCA LITERATURA PODSTAWOWA: [1] J. Zakrzewski, Czujniki i przetworniki pomiarowe. Podręcznik problemowy. Wydawnictwo Politechniki Sląskiej, Gliwice 2004. [2] T. Mikulczyński, Podstawy automatyki, WPW Wrocław 1998. [3] A. Markowski, J. Kostro, A. Lewandowski, automatyka w pytaniach i odpowiedziach. WNT Warszawa 1995. [4] Instrukcje do ćwiczeń laboratoryjnych http://www.ibp.pwr.wroc.pl LITERATURA UZUPEŁNIAJĄCA: [1] E. Romer, Miernictwo przemysłowe, W-wa PWN 1970. [2] W. Nawrocki, Rozproszone systemy pomiarowe, WKŁ Warszawa 2006. [3] B. Mrozek, Z. Mrozek, Matlab i Simulink – Poradnik użytkownika. Helion 2006. OPIEKUN PRZEDMIOTU (IMIĘ, NAZWISKO, ADRES E-MAIL) Stefan Giżewski, [email protected] MACIERZ POWIĄZANIA EFEKTÓW KSZTAŁCENIA DLA PRZEDMIOTU Miernictwo i Automatyka Z EFEKTAMI KSZTAŁCENIA NA KIERUNKU Technologia Chemiczna I SPECJALNOŚCI …………………………….. Przedmiotowy efekt kształcenia PEK_W01 (wiedza) PEK_W02 PEK_U01 (umiejętności) PEK_U02 PEK_K01 Cele przedmiotu*** Treści programowe*** Numer narzędzia dydaktycznego*** K1Atc_W21 C1 W1 do W7 N1 do N5 K1Atc_W21 K1Atc_U41 C1 C2 W1 do W7 L1 do L15 N1 do N5 N1 do N5 K1Atc_U41 C2 C1,C2 L9 do L14 W8,L15 N1 do N5 N4,N5 Odniesienie przedmiotowego efektu do efektów kształcenia zdefiniowanych dla kierunku studiów i specjalności (o ile dotyczy)** (kompetencje) ** - wpisać symbole kierunkowych/specjalnościowych efektów kształcenia *** - z tabeli powyżej 75 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Optymalizacja procesów chemicznych i elektrochemiczne procesy produkcyjne Name in English Optimization of chemical processes and electrochemical production processes Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses CHEMICAL TECHNOLOGY 1st level, full-time optional TCC017003l NO *delete as applicable Lecture Classes Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Laboratory Project Seminar 30 60 Crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 2 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 23. Knowledge of chemistry at 1-st degree studies 24. Knowledge of mathematics at the middle school level 25. Knowledge of basic concept of mathematical statistics SUBJECT OBJECTIVES C1 To familiarize students with the way of experiment performing and with interpretation of results. C2 To familiarize students with methods of statistical quality control serving to check validity of technological process. C3 Learning methods for validation of quantitative analysis. 76 C4 Teaching students methods of optimization of chemical and electrochemical processes. SUBJECT EDUCATIONAL EFFECTS Relating to skills: Person who has complited the course: PEK_U01 - is able to describe the chemical and electrochemical processes by regression equations and apply statistical control for process quality, PEK_U02 – can use statistical methods for quality control of chemical process occurring, PEK_U03 – is able to perform statistical analysis of regression equation (Snedecor F-test and Student’s t-test), PEK_U04 – is able to carry out and control chemical and electrochemical processes. PROGRAMME CONTENT Number of hours Form of classes - laboratory Lab 1 Lab 2 Lab 3 Lab 4 Lab 5 Lab 6 Work out of measured results, control charts for statistical control of chemical process. Determination and preparation of calibration curve. Validation of measuring methods. Electrorefining of nickel Electroplating of metallic coatings Production of o-aminophenol by cathodic reduction of o-nitrophenol Total hours N1 N2 N3 5 5 5 5 5 5 30 TEACHING TOOLS USED Performance of chemical and electrochemical experiments Interpretation of test results Performance of mathematical calculation. EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) F1 (laboratory) PEK_U01PEK_U04 Test and report for each laboratory (max 30 points. Up to 3 points for test and 2 points for report) F2 77 … C (laboratory) = 3.0 if F1/6=3.0-3.4 =3.5 if F1/6=3.41-3.9 =4.0 if F1/6= 3.91-4.4 =4.5 if F1/6= 4.41-4.74 =5.0 if F1/6= 4.75-5.0 =5.5 if F1/6> 5.0 PRIMARY AND SECONDARY LITERATURE Primary literature: [1] J. Arendarski, Niepewność pomiarów, Oficyna wydawnicza P.W., Warszawa 2003 [2] J.R. Thompson, J. Koronacki, Statystyczne sterowanie procesem, Akademicka Oficyna Wydawnicza PLJ, Warszawa 1994 [3] O. Hryniewicz, Nowoczesne metody statystycznego sterowania jakością, Instytut Badań Systemowych PAN, Warszawa 1996 [4] P. Konieczko, J. Namieśnik, Ocena i kontrola jakości wyników pomiarów analitycznych, WNT, Warszawa 2007 [5] J. R. Thomson, J. Kornacki Statystyczne sterowanie procesem, Akademicka Oficyna Wydawnicza PLI, Warszawa 1994. [6] R. Dylewski, W. Gnot, M. Gonet, Elektrochemia Przemysłowa, Wyd. Politechniki Śląskiej, Gliwice 1999 Secondary literature: [1] PN EN-ISO/IEC 17025/2001 [2] A.T. Kuhn, Industrial electrochemical processes, Els. Pub. Co., New York 1991. SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Barbara Kucharczyk, [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Optimization of chemical processes and electrochemical production processes AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY CHEMICAL TECHNOLOGY Subject educational effect (skills) PEK_U01 PEK_U02 PEK_U03 PEK_U04 Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** Programme content*** Teaching tool number*** K1Atc_U34 C1, C3 Lab1-Lab6 N1, N2, N3 K1Atc_U34 K1Atc_U34 K1Atc_U34 C2 C1, C3 C4 Lab1- Lab3 Lab2 Lab1 – Lab6 N1, N2, N3 N1, N2, N3 N1, N2, N3 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 78 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Fizykochemia węgla i materiałów węglowych Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Chemical Technology Physicochemistry of coal and carbon materials 1st level, full-time optional TCC010028 NO *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 30 60 Crediting in grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 26. Fundamentals in organic chemistry SUBJECT OBJECTIVES C1 C2 C3 Getting knowledge of composition, structure and physicochemical properties of fossil fuels. Getting fundamental knowledge of carbon materials and physicochemical processes occurring during their production. Getting fundamental knowledge of instrumental analytical techniques for examination of properties and structure of coal and carbon materials. 79 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – has knowledge of genesis of fossil fuels and coal petrology PEK_W02 – knows the structure of coals of different rank PEK_W03 – has the elements of knowledge of physical and chemical models of coal structure PEK_W04 – has knowledge of porosity and density of coal and extraction methods of coal organic substance PEK_W05 – has knowledge of interpreting the results obtained by instrumental analytical techniques (XRD, FTIR, 1H NMR, SEM-EDX, TGA/DTG, ASA, AES/ICP) for characterization of coal and carbon materials PEK_W06 – gets knowledge of different carbon materials, knows the relationships between structure and texture and properties PEK_W07 – has knowledge of pyrolysis and carbonization processes of organic substances and of basic methods for examination of carbon materials PEK_W08 – has knowledge of methods for determining porosity; gets the fundamental knowledge of synthesis and structure of fullerenes, carbon nanotubes/nanofibers and graphene PROGRAMME CONTENT Form of classes - lecture Lec 1 Genesis of coal. Petrographic composition of coal. Properties of petrographic constituents of coal. Lec 2 Coalification degree. Elemental composition of fossil fuels of different coalification degree. Constitution of coal organic matrix. Carbon and hydrogen functional groups. Lec 3 Constitution of coal organic matrix. Oxygen, sulfur and nitrogen functional groups. Lec 4 Physical and chemical models of coal structure. Porous structure of coal. Extraction of coal. Types of extraction Lec 5 processes and their application. Analysis of extracts. Examination methods of coal organic matrix and mineral Lec 6 substance. Definitions and classification of carbon materials. Structure vs. Lec 7 texture. Carbonization and graphitization processes. Optical microscopy Lec 8 and XRD for characterization of carbon materials. Porous carbon materials. Determination of porosity by gas sorption Lec 9 and porosimetry. Nanostructured carbon. Lec 10 Evaluation educational effect achievement. Total hours N1 TEACHING TOOLS USED Lecture with PowerPoint presentations 80 Number of hours 3 3 3 3 3 3 3 3 3 3 30 EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect number Way of evaluating educational effect Evaluation F – forming (during achievement semester), C – concluding (at semester end) P PEK_W01-PEK_W10 Crediting with grade PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [1] D.V. Van Krevelen, Węgiel, WNT, Warszawa 1954. [2] Chemia i fizyka węgla, pod red. S. Jasieńki, Wyd. PWr, Wrocław 1995. SECONDARY LITERATURE: [3] D.V. Van Krevelen, Coal. Typology-Physics-Chemistry-Constitution, Elsevier, Amsterdam 1993 [4] Introduction to Carbon Science, red. H, Marsh, Butterworth, London 1989 SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Prof. dr hab. inż. Grażyna Gryglewicz, [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Physicochemistry of coal and carbon materials AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** (knowledge) PEK_W01 PEK_W02 PEK_W03 PEK_W04 PEK_W05 PEK_W06 PEK_W07 PEK_W08 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 81 Programme content*** Teaching tool number*** Lec1 N1 Lec2-3 Lec4 Lac5 Lec4, Lec6 Lec7 Lec8 Lec9 N1 N1 N1 N1 N1 N1 N1 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Fizykochemia ropy i produktów naftowych Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Chemical Technology Physicochemistry of petroleum and derived materials 1st level, full-time optional TCC010027 NO *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 30 60 Crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 27. 28. Organic chemistry Organic chemical technology SUBJECT OBJECTIVES C1 C2 C3 C4 C5 C6 Understanding fundamental aspects of origin and evaluation of petroleum and the variation in the character of crude oils which occurs over geological time To familiarize students with the method of petroleum classification To provide a core of knowledge of the chemical composition of crude oil (hydrocarbon and non-hydrocarbon components) To provide the student with understanding of petroleum products manufacture and available product improvement processes To provide an knowledge of properties and uses of main petroleum products To familiarize students with the standard requirements and test methods for 82 C7 marketed petroleum products To familiarize students with the environmental impact cause by petroleum products during their use SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – student has a knowledge about the origin of crude oil and understands how the composition of crude oil is affected by organic fluids and geological environments PEK_W02 – student has a core knowledge about composition and classification of crude oil PEK_W03 – student has a basic knowledge in the field of main refining processes PEK_W04 – student can present examples of schematic flow diagrams for the production of marketable products PEK_W05 – student has a basic knowledge about the petroleum products improvement and their physicochemical properties and performance PEK_W06 – student understands the importance of product standards and testing standards and the reasons for their change PEK_W07 – student has a knowledge about technology for the reduction of the negative impact on the environment of petroleum products PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Lec.5 Lec 6 Lec. 7 Lec. 8 Lec.9 Lec. 10 Lec.11 Lec. 12 Lec. 13 Lec.14 Lec.15 Form of classes - lecture Petroleum geochemistry Crude oil distillation system, fractional composition – crude oil classification Hydrocarbon components. Normal and branched paraffins; structure, concentration and influence on the properties of petroleum fractions Hydrocarbon components. Aromatics compounds; structure, concentration and influence on the properties of petroleum fractions Hydrocarbon components. Cycloparaffis compounds; structure, concentration in the petroleum fractions Nonhydrocarbon components. Sulphur, nitrogen and oxygen compounds Nonhydrocarbon components. Porphyrins, metallic constituents, asphaltenes and resins Composition and physical properties of the primary and refining processes fractions. Preparation of components for transportation fuels Lubricating oils and grases; manufacture, properties and uses Asphalt, waxes and coke; manufacture, properties and uses Petroleum products improvement, physical properties Petroleum products improvement, physical properties Petroleum products specifications and related tests methods Environmental regulations in respect to petroleum products 83 Number of hours 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 Total hours N1 30 TEACHING TOOLS USED Lecture and multimedia presentation EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) C PEK_W01-PEK_W07 toutoriale PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [7] G. Speight, The chemistry and Technology of Petroleum, Marcel Dekker, Inc. 1991 [8] J. R. Grzechowiak, Fizykochemia ropy naftowej, Wyd. PWr, Wrocław, 1987 [9] Alfred Podsiadło. Paliwa oleje i smary w ekologicznej eksploatacji, Wyd. PWN Warszawa 2002 SECONDARY LITERATURE: [5] [6] [7] SUBJECT SUPERVISOR (Prof. dr hab. inż. Jolanta Grzechowiak) 84 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Physicochemistry petroleum and derived materials AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical technology Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** (knowledge) PEK_W01 PEK_W02 PEK_W03 PEK_W04 PEK_W05 PEK_W07 (skills) PEK_U01 PEK_U02 PEK_U03 … Subject objectives*** Programme content*** Teaching tool number*** C1 Wy 1 N1 C2C3 C4 C4 C5 C6 Wy 2-7 Wyk 8-11 Wyk 8-11 Wyk 13, 14 Wyk 14 N1 N1 N1 N1 N1 C7 Wyk 15 N1 (competences) PEK_K01 PEK_K02 PEK_K03 … ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 85 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Kontrola jakości surowców i produktów Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Technologia chemiczna Quality control of raw materials and products 1st level, full-time obligatory TCC015005 NO *delete as applicable Lecture Classes Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Laboratory Project Seminar 60 120 Crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 4 4 2 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 29. Basic knowledge of analytical chemistry SUBJECT OBJECTIVES C1 C2 Learning how to perform basic chemical analysis of raw materials and products Teaching physicochemical measurements for process control 86 SUBJECT EDUCATIONAL EFFECTS Relating to skills: Person who has complited the course: PEK_U01 – is able to determine the composition and quality of water, PEK_U02 – can perform analysis and define the properties of mineral fertilizers, PEK_U03 – can determine the corrosion resistance and thermophysical properties of materials and the quality of galvanic coatings, PEK_U04 – can determine properties of flammable and explosive gases, PEK_U05 – can identify plastics and determine the average molecular weight of the polymers, PEK_U06 – can determine the quality of surface-active agents, PEK_U07 – is able to analyze the properties of petroleum products, catalysts and sorbents, PEK_U08 – can perform chromatographic analysis of gaseous and liquid motor fuels. PROGRAMME CONTENT Number of hours Form of classes - laboratory Lab 1 Lab 2 Lab 3 Lab 4 Lab 5 Lab 6 Lab 7 Lab 8 Lab 9 Lab 10 Lab 11 Lab 12 Lab 13 Lab 14 Lab 15 Method of conducting and completion activities. Health and Safety Training. Quality water control. Chemical composition and properties of mineral fertilizers. Corrosion resistance of construction materials. Flammable and explosive properties of gases. Influence of electrolysis parameters on quality of galvanic coatings. Identification of plastics. Determination of average molecular weight of the polymers. Surface characterization of polymers by means of contact angle measurements. Determination of quaternary ammonium surfactants. Determination of the critical micelle concentration by conductivity method. Analysis of catalysts and sorbents properties. Analysis of properties of petroleum products. Study of thermophysical properties of materials. Chromatographic analysis of the gas and liquid components of motor fuels. Total hours N1 N2 TEACHING TOOLS USED Performance of experiment Results elaboration and preparing of report 87 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 60 EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational Way of evaluating educational effect achievement Evaluation F – forming (during effect semester), number C – concluding (at semester end) F1 (laboratory) PEK_U01 pre-test and report on laboratory exercises F2 (laboratory) PEK_U02 pre-test and report on laboratory exercises F3 (laboratory) PEK_U03 pre-test and report on laboratory exercises F4 (laboratory) PEK_U04 pre-test and report on laboratory exercises F5 (laboratory) PEK_U03 pre-test and report on laboratory exercises F6 (laboratory) PEK_U05 pre-test and report on laboratory exercises F7 (laboratory) PEK_U05 pre-test and report on laboratory exercises F8 (laboratory) PEK_U05 pre-test and report on laboratory exercises F9 (laboratory) PEK_U06 pre-test and report on laboratory exercises F10 (laboratory) PEK_U06 pre-test and report on laboratory exercises F11 (laboratory) PEK_U07 pre-test and report on laboratory exercises F12 (laboratory) PEK_U07 pre-test and report on laboratory exercises F13 (laboratory) PEK_U03 pre-test and report on laboratory exercises F14 (laboratory) PEK_U08 pre-test and report on laboratory exercises C (laboratory) = (F1+F2+F3+F4+F5+F6+F7+F8+F9+F10+F11+F12+F13+F14)/14 PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [10] J. Minczewski, Z. Marczenko, Chemia analityczna, PWN Warzsawa, 1985 [11] J.G. Dick, Analytical Chemistry, Int. Stud. Edition, MC Graw-Hill, Tokyo, 2004 [12] Z. Szmal, T. Lipiec, Chemia analityczna z elementami analizy instrumentalnej, Wyd. Lekarskie PZWL, Warszawa, 1997 [13] B. Bobrański, Analiza Ilościowa związków organicznych, PWN, Warszawa, 1979. SECONDARY LITERATURE: [8] Instructions for exercises [9] National and EU Standarts SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Izydor Drela, [email protected] 88 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT ……………………………………. AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY ……………………………………. Subject educational effect (skills) PEK_U01 PEK_U02 PEK_U03 Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** Programme content*** Teaching tool number*** K1Atc_U24 C1, C2 Lab2 N1, N2 K1Atc_U24 C1, C2 N1, N2 K1Atc_U24 C2 Lab3 Lab4, Lab6, Lab 14 Lab5 Lab7–Lab9 Lab10–Lab11 Lab12, Lab13 Lab15 K1Atc_U24 C2 PEK_U04 K1Atc_U24 C1, C2 PEK_U05 K1Atc_U24 C1, C2 PEK_U06 K1Atc_U24 C1, C2 PEK_U07 K1Atc_U24 C1 PEK_U08 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 89 N1, N2 N1, N2 N1, N2 N1, N2 N1, N2 N1, N2 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Zarządzanie jakością Quality Management Chemical Technology 1st level, full-time obligatory ZMC016001 NO *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 30 60 Crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 *delete as applicable SUBJECT OBJECTIVES C1 C2 C3 Introducing students to the basic terminology concepts and definitions of quality management and tools for its improvement. Presentation of issues concerning the development of sustainable technologies and applied in practice management systems of quality, environment, occupational health and safety and quality management in laboratory / implementation. Introducing students to the documentation in quality management systems and the principles of certification and accreditation of quality systems. 90 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: The person who passed the object: PEK_W01 – knows the key concepts and definitions of quality and have sufficient knowledge of the basic concepts and models of management PEK_W02 – can describe the structure, objectives and goals of Total Quality ManagementTQM, and also has a knowledge of the implementation of the TQM concept in the organization PEK_W03 – has the knowledge and can describe the Quality Management System in accordance with ISO 9000, knows basic documentation in this area and knows how to use the tools of quality improvement PEK_W04 – has knowledge of Sustainable Development and the documents relating to global sustainable development policy PEK_W05 – has a basic knowledge of the improvement cycle in the environmental management system ISO serii14000 PEK_W06 – has a knowledge of Occupational Health and Safety Management Systems in accordance with the ISO 18000 series and knows the process steps in the range of identification and risk assessment PEK_W07 –knows the basic regulations for the management of chemicals PEK_W08 – knows the requirements for the competence of research and calibration laboratories in the field of quality management in the laboratory according to ISO 17025 PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 Lec 9 Lec 10 Lec 11 Lec 12 Lec 13 Lec 14 Form of classes - lecture Quality, origin, basic concepts and definitions The ideas and management models (Deminga, Jurana, Crosby’ego, Feinbauma) Quality Management– TQM Quality Management Systems Standards ISO 9000, 9001, 9004 Techniques and methods for improving the quality Principles of Sustainable Development Environmental management - basic requirements, stages of implementation in accordance with ISO series 14000 Occupational Health and Safety Management Systems - ISO series 18 000 Occupational Health and Safety Management Systems - risk assessment Chemicals Management (Material safety data sheet, recycling, utilization of chemicals) - the programs implemented by the chemical industry in this area Quality management systems in the laboratory according to ISO 17025 Documentation in quality management systems - ISO / TR 10 013 Certification and accreditation of quality systems 91 Number of hours 2 2 2 2 2 2 2 2 2 2 2 2 2 2 Lec 15 Other management systems - a repeat of the material, final test Total hours N1 2 TEACHING TOOLS USED lecture with a multimedia presentation EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) C1 (Lecture) PEK_W01 – PEK_W08 Final test PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [1] Łańcucki J., Podstawy Kompleksowego Zarządzania Jakością TQM, Wyd. AE, Poznań, 2006 [2] Karaszewski R., TQM teoria i praktyka, Toruń 2001 [3] Hamrol A., Mantura W., Zarządzania jakością, teoria i praktyka, PWN, Poznań, 1999 [4] Nowak Z., Zarządzania środowiskiem, cz. I i II, Wyd. Pol. Śl., Gliwice, 2001 SECONDARY LITERATURE: [1] Urbaniak M., Systemy zarządzania w praktyce gospodarczej, Difin, Warszawa, 2006 [2] Wawak S., Zarządzania jakością – teoria i praktyka, Helion, Gliwice, 2002 [3] Żuchowski J., Łagowski E., Narzędzia i metody doskonalenia jakości, Wyd. Pol. Radomskiej, Radom, 2004 [4] Konarzewska-Gubała E., Zarządzania przez jakość, koncepcje, metody, studia przypadków, Wyd. AE Wrocław, 2003 [5] Kubera H., Zachowanie jakości produktu, Wyd. AE Poznań, 2002 SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Professor Jozef Hoffmann PhD, DSc, [email protected] 92 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Quality Management AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical Technology Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** K1Atc_W25 C1 K1Atc_W25 C1 PEK_W03 K1Atc_W25 C1, C2, C3 PEK_W04 K1Atc_W25 C2 Lec1, Lec2, Lec15 Lec3 Lec4-Lec6, Lec13, Lec14 Lec7 PEK_W05 K1Atc_W25 C2 Lec8 N1 Lec9, Lec10 Lec11 Lec12 N1 N1 N1 (knowledge) PEK_W01 PEK_W02 K1Atc_W25 C2 PEK_W06 K1Atc_W25 C2 PEK_W07 K1Atc_W25 C3 PEK_W08 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 93 Programme content*** Teaching tool number*** N1 N1 N1 N1 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Chemiczna produkcja małotonażowa Small volume chemical production 1st level, full-time optional CHC010020 /NO *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 30 crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 1 Basic knowledge of chemical technology 2 Basic knowledge of chemical engineering 3 Basic knowledge of environmental protection SUBJECT OBJECTIVES C1 C2 C3 C4 C5 C6 To familiarize students with the specific production of chemical industry Understanding the principles of organization of the market of chemical products, as well as the sectoral distribution of production tasks To familiarize students with the basic legal requirements and organization of chemical production Basic knowledge about the production of basic chemicals, raw materials base and cooperative relations with the sector of chemical processing Understanding the conditions and characteristics of small capacity production Convincing students about the essential role of research and development and 94 deployment of innovative small and medium-sized enterprises SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 - Know the task of production and the role of small and medium-sized enterprises in the chemical industry PEK_W0 He knows the problems PEK_W02-organizational, economic, technological and basic regulations for the operation of small businesses PEK_W03- Students knows fundamental principles of investing, operation system in accordance with the requirements of environmental protection PEK_W04- Student knows responsibility for maintaining a healthy and environmentally friendly production, the existing emission standards, the principles of waste management PEK_W05- Students have basic knowledge of the conditions of approval of the product for marketing PEK_W06-Student has a general understanding of the problems of market, technology and development trends in the group of small companies producing plastic products, ceramics, agrochemicals, chemical products for agriculture, medical, automotive, construction, municipal,medicine ... Relating to skills: PEK_U01 – PEK_U02 – … Relating to social competences: PEK_K01 PEK_K02 … 95 PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 Lec 9 Lec10 Form of classes - lecture Characteristics of the chemical industry: production structure, sectoral organization, the impact of industry on the environment, chemical production of monomers, manufacture and market finished products, production in the "bussines to bussines" The role of small and medium-sized enterprises in the industry of the European Union: the role of low-volume production and its competitiveness, cooperative relations with large chemical industry, the problems of raw material supply and distribution of products on the market Technical and organizational rules and regulations for the production of low-volume: basic definitions, forms of ownership, the procedure for the preparation of investment projects and investment projects, rules for the implementation of new technologies, regulations on emissions, waste water discharge, waste management Technical conditions of operation of chemical plants: rules and regulations for the use of the environment in the production of lowvolume, cost of use of the environment, methods of efficiency of water, energy and raw materials The raw material base of small -tonnage production : competitiveness, and the costs of raw materials, including energy, use of renewable materials and biomass as a new source of raw materials, raw material trends worldwide Economic Policy, Energy and Climate on the chemical and chemicals: Integrating the principles of sustainable development, the principle of BAT / The Best Available Technique / in investing, an integrated permit, the European Emissions Trading, the REACH program in the handling and use of chemicals Technological innovation in low-volume production: the role of research, systems of innovation, the organization of the R & D cycle, examples of product innovation and resource The tasks of small and medium-sized enterprises in waste management: the use of recycled materials as feedstock and energy, the recovery of valuable components from waste, recycling and disposal of waste, chemical waste disposal methods in agriculture and food economy Transport, storage and distribution of chemical products in small and medium-sized enterprises: the organization of the system of supply of raw materials and distribution of finished products, storage, transportation, packaging, distribution, transport requirements ARD, packaging products Policy and funding of innovative projects: a system of funding for research and development as a basis in the implementation of innovation, research support from structural funds, the European Union and the budget allocated for education, organization of research and development facilities in Poland 96 Number of hours 2 2 2 2 2 2 2 2 2 2 Lec11 Lec12 Lec13 Lec14 Lec15 Small volume production in the "bussines to bussines": products of the "specialties" and "fine chemicals" made to order such industries and fields as agriculture, automotive, health care, construction, electronics, energy, environment, Chemical Services in different sectors of the economy, chemical technologies used in various industries and in various applications, including disinfection processes, sterilization, protection against corrosion, detoxification, the introduction of micro-food products, animal feed, Princeples of certyification of products on the market: the development of occupational standards, product certification, obtaining the CE mark, quality management systems, life cycle analysis of products, trademarks, accredited role of qualitative research, product certification system Small volume production and chemical services industry as an example: will present the form of technological and organizational support agricultural production in the fertilizer and animal feed, as well as chemical waste by low-volume production Summary of the lecture and the final test Total hours Form of classes - class 2 2 2 2 2 30 Number of hours Cl 1 Cl 2 Cl 3 Cl 4 … Total hours Form of classes - laboratory Number of hours Lab 1 Lab 2 Lab 3 Lab 4 … Total hours Form of classes - project Number of hours Proj 1 Proj 2 Proj 3 Proj 4 … Total hours 97 Form of classes - seminar Number of hours Sem 1 Sem 2 Sem 3 Sem 4 … Total hours N1 N2 … TEACHING TOOLS USED Lecture and multimedia presentation EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), Final test PEK_W01 – C – concluding (at PEK_W06 semester end) F1 F2 … C PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [1].K.Małachowski, Gospodarka a środowisko i ekologia, wyd.CeDeWu,2011 [2].J.Boć j,K. Nowacki Ochrona Środowiska, Kolonia Ltd, 2008 [3].B.Dobrzańska, G.Dobrzański,D.Kiełczewski, Ochrona środowiska przyrodniczego,wyd.PWN, 2010 [4]M.Górski, Prawo ochrony środowiska,Wolter Kluwer Polska,2009 [5]CEFIC Chemical Reports internet SECONDARY LITERATURE: [10] czasopismo Chemik [11] czasopismo Przemysł Chemiczny [12] raporty środowiskowe Polskiej Izby Przemysłu Chemicznego SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Prof.dr.hab.inż.Henryk Górecki e-mail. [email protected] 98 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT …… Small volume chemical production ………………………………. AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY …Chemical technology…………………………………. Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** knowlege PEK_W01 Subject objectives*** Programme content*** Teaching tool number*** K1 Atc W13, K1 Atc W14, K1 Atc W15 C1,C6 Le1. Le2, Le 12 N1 PEK_W02 K1 Atc W10 C2,C3 PEK_W03 K1 Atc W09, K1 Atc W13 K1 Atc W10. K1 Atc W12, K1 Atc W14 K1 Atc W10. K1 Atc W12, K1 Atc W14 K1 Atc W10. K1 Atc W12, K1 Atc W14 C2,C3,C4,C6 PEK_W04 PEK_W05 PEK_W06 C3,C5 N1 N1 N1 C2,C3,C5,C6 Le 8, Le 9, N1 C6 Le 6, Le 10 N1 … ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 99 Le 3, Le 4, Le, Le 6, Le 11 Le 3, Le 4, Le 5 Le 6, Le 7, Le8, Le 9 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Strategie zrównoważonego rozwoju Strategies of sustainable development Chemical technology 1st level, full-time optional TCC010038 NO* *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar Examination / crediting with grade* Examination / crediting with grade* Examination / crediting with grade* Examination / crediting with grade* 2 30 crediting with grade* For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 0.5 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 30. 31. Basic Chemistry SUBJECT OBJECTIVES C1 C2 To provide students with the basic determinants of sustainable development. To provide students with examples of practical application of the concept of sustainable development in chemical technology C3 C4 100 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – knows determinants of sustainable development and its principles PEK_W02 – knows examples of practical application of the principles of sustainable development in chemical technology PEK_W03 - knows the directions of the development of sustainable energy production PEK_W04 - known examples of recycled materials in chemical technology ... Relating to skills: PEK_U01 – PEK_U02 – … Relating to social competences: PEK_K01 PEK_K02 … PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Lec 5 Lec 6 … Form of classes - lecture What is sustainable development (SD), strategies of SD. Economic and social conditions of SD. Monitoring systems SD in chemical technology: the production of hydrogen, CO2 sequestration, waste water treatment, extraction under supercritical conditions, combustion and selective oxidation, liquid phase oxidation with H2O2; renewable raw materials (ethanol, glycerol, biomass) LCA techniques in the evaluation of products, processes and waste management. Energy production and SD Recycling (spent catalysts and oils) Total hours TEACHING TOOLS USED N1 N2 … Problem lecture 101 Number of hours 2 3 2 15 5 3 30 EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) F1 F2 F3 C PEK_W01 – PEK_W04 assignments PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [14] J.A. Moulijn, M. Makkee, A. Van Diepen. Chemical Process Technology. J. Wiley & Sons, Ltd. [15] B. Burczyk. Zielona Chemia. Oficyna Wydawnicz PWr. Wrocław 2006 [16] B. Grzybowska-Świerkosz. Elementy katalizy heterogenicznej. PWN 1992 [17] Praca zbiorowa pod redakcją J. Ryczkowskiego: Adsorbenty i katalizatory. Wybrane technologie a środowisko. SECONDARY LITERATURE: [13] M.B. Hocking; Chemical technology and pollution control. AP 1993 [14] [15] SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) prof. dr hab. inż. Janusz Trawczyński; [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Strategies of sustainable development AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical technology Subject educational effect (knowledge) PEK_W01 PEK_W02 PEK_W03 Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Optional course 102 Subject objectives*** Programme content*** Teaching tool number*** … (skills) PEK_U01 PEK_U02 PEK_U03 … (competences) PEK_K01 PEK_K02 PEK_K03 … ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 103 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Systemy zarządzania procesem technologicznym i jakością Name in English Systems of management of the technological process and quality Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Chemical Technology 1st level, full-time optional ZMC010007 NO *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 30 60 Crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 *delete as applicable SUBJECT OBJECTIVES C1 C2 C3 C4 Introducing students to the basic terminology, concepts and definitions of quality management and process technology and its improvement tools. Presentation of issues concerning Sustainability Principles, standards of quality management, including subject of quality industry standards Introducing students to the issues of aquire, implementation and development of technology Understanding the nature and role of formation and management of quality in the production process 104 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: The person who passed subject: PEK_W01 – knows the key concepts and issues in the field of quality management and process technology that meets the requirements of quality and environmental PEK_W02 – has the knowledge and can describe the quality management systems in the industry, the environment and knows quality improvement tools and basic techniques PEK_W03 – has knowledge of the organization and methodology of the process realization, knows the principles of technology strategy as well as principles of technology selection and its implementation PEK_W04 – knows the scope of producer responsibility for the product life cycle and has a information about the continuous improvement of product quality and productivity of manufacturing processes PEK_W05 – has knowledge of the marketing aspects of the product quality formation PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 Lec 9 Lec 10 Form of classes - lecture Introduction, terminology, basic terms, definitions Introduction to management in the chemical company and laboratory Kaizen Qualitative industry standards Concept of Sustainable Development, EMAS, environmental programs, "Responsible and Care", Cleaner Production, Cleaner Technology, Green Chemistry Life Cycle Analysis The essence, the principle of selection, acquisition and implementation of technology - from plan to action Lean Manufacturing, Benchmarking, Controlling Brand and its position on the market Marketing aspects of product quality Total hours N1 TEACHING TOOLS USED lecture with a multimedia presentation 105 Number of hours 3 3 3 3 3 3 3 3 3 3 30 EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) C1 (Lecture) PEK_W01 – PEK_W05 Final test PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [1] Zarządzanie technologią, UNIDO (Organizacja ds. Rozwoju Przemysłowego Narodów Zjednoczonych, Wiedeń, 2003 [2] Draft reference document on economics and cross-media effects, European IPPC Bureau, Sevilla, 2003, ([email protected]) [3] Jyż G., Prawo do wynagradzania za projekty wynalazcze, Wyd. U. Śl., Gliwice, 2003 [4] Nowosielski S., Zarządzanie produkcją, Wyd. AE, Wrocław, 2001 [5] Safin K., Zarządzanie małą firmą, Wyd. AE, Wrocław, 2003 SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Professor Jozef Hoffmann PhD, DSc, [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Systems of management the technological process and quality AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical Technology Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** (knowledge) C1 PEK_W01 C1, C2 PEK_W02 C3 PEK_W03 C4 PEK_W04 C4 PEK_W05 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 106 Programme content*** Teaching tool number*** Lec1, Lec2 N1 Lec3-5 Lec6-7 Lec8 Lec9-10 N1 N1 N1 N1 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology Faculty of Chemistry CARD OF SUBJECT Name in Polish Name in English Main field of study (if applicable): Specialization (if applicable): Level and form of studies: Kind of subject: Subject code Group of courses Chemia techniczna organiczna Technical organic chemistry Chemical Technology 1st level, full-time obligatory CHC013008 NO Lecture Classes Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of course crediting Laboratory Project Seminar 30 60 credit with grade For a group of courses mark (X) if final course Number of ECTS points 2 including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes *delete as applicable PREREQUISITES RELATED WITH KNOWLEDGE, SKILLS AND OTHER COMPETENCIES 1. Basic knowledge of the chemical reagents. 2. Knowledge of the basic of chemical reactions. 3. Knowledge of the basic glassware and laboratory equipment. \ AIM OF THE SUBJECT C1 Acquiring the basic knowledge of purification of the mixture of compounds with distillation and crystallization, separation of the mixture’s compounds with distillation, gravity and vacuum filtration, as well as the modification of polymers. C2 Acquainting with the basic chemical experiments performed in the scope of individual actions. C3 Acquainting with the chemical measurements techniques: refractive index determination, melting point determination. EDUCATIONAL EFFECTS OF COURSE Related with knowledge: Student who graduates the course, has the knowledge concerning: PEK_W01 – basic techniques of chemical compounds purification PEK_W02 – simple methods of polymers modification – nitration, aminolysis PEK_W03 – methods of examination of properties of chemical substances PEK_W04 – basic laboratory techniques: distillation, crystallization, gravity and vacuum filtration, drying, two-phase extraction Related with skills: 107 Student who graduates the course should be able to: PEK_U01 – devise a simple chemical experiment PEK_U02 – separate a mixture of chemical compounds PEK_U03 – modify polymers – cellulose and polyacrylonitrile PEK_U04 – assemble a complex equipement to perform a chemical reaction PEK_U05 – determine properties and purity of chemical reaction products PEK_U06 – perform test of positive control PEK_U07 – to runs correctly laboratory notes PROGRAMME CONTENT Number of hours Form of classes - laboratory Lab 1 Lab 2 Lab 3 Lab 4 Lab 5 Lab 6 Lab 7 Lab 8 Introduction and safety rules. Determination of the composition of mixture of liquid organic compounds. Nitration of cellulose Aminolysis of polyacrylonitryle Aminoesteres of fatty acids Coupling of diazonium salts Synthesis of cycloheksanone Additional classes 2 4 4 4 4 4 4 4 Total hours 30 TEACHING TOOLS USED N1. A set of prepared manuals for experiments. N2. Verification of student’s preparation to perform the experiment – a test. N3. Proper execution of the experiment and teachers instructions N4. Reports of performed experiments. EVALUATION OF THE ACHIEVEMENTS OF THE EDUCATIONAL EFFECTS OF THE COURSE Evaluation (F – forming (during Number of semester), P – education effect of Methods of the achievement of the educational effect concluding (at the course the end of semester) F1 (laboratory) PEK_W01-W04 Average of grades of tests verifying student’s preparation to PEK_U01-U07 perform the experiment, as well as of grades of reports of performed experiments. F2 (laboraory) PEK_U01-U07 Proper performance of six exercises and providing the teacher 6 reports. P (laboratorr = F1+F2 BASIC AND SUPPLEMENTARY LITERATURE 108 BASIC LITERATURE: [18] L. Achremowicz. M. Soroka, Chemia organiczna Laboratorium, Skrypt Politechniki Wrocławskiej, Wrocław 1980 [19] A. I. Vogel, Preparatyka organiczna, WNT, Warszawa 1984 [20] J. Pielichowski, A. Puszyński, Technologia tworzyw sztucznych, WNT, Warszawa 2003 [21] Z. Jerzmanowska, Preparatyka organicznych związków chemicznych, PZWL, Warszawa 1972 [22] J. Gaworowski, M. Dziankowski, Pracownia preparatyki organicznej, PWT, Warszawa 1960 [23] D. Żuchowska, Polimery konstrukcyjne, WNT, Warszawa 1995 [24] Z. Florjańczyk, S. Penczek, Chemia polimerów, tom II, III, Wyd. Pol. Warszawska, Warszawa 1997 SUPPLEMENTARY LITERATURE: [16] R. Zieliński, Surfaktanty towaroznawcze i ekologiczne aspekty ich zastosowania, Wyd. Akademii Ekonom. W Poznaniu, Poznań 2000 [17] J. Ogonowski, A. Tomaszewski-Potepa, Związki powierzchniowo czynne, Wyd. Pol. Krakowskiej, Kraków 1999 [18] G.M. Fuller, D. Shield, Podstawy molekularne biologii komórki, aspekty medyczne, PZWL, Warszawa 2000 COURSE SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Prof. dr hab. inż. Kazimiera A. Wilk [email protected] 109 MATRIX OF CORRELATIONS BETWEEN EDUCATIONAL EFFECTS OF THE COURSE Technical organic chemistry AND EDUCATIONAL EFFECTS FOR THE MAIN FIELD OF STUDIES Chemical technology Educational effect of the course Aim of the subject*** Content of the course programme*** Number of teaching tool *** PEK_W01 (knowledge) PEK_W02 PEK_W03 PEK_W04 Correlation between educational effects of the course and educational effects defined for the main field of studies and specialization (if applicable)** K1Atc_U16 K1Atc_U16 K1Atc_U16 K1Atc_U16 C1, C2 C1, C2 C1, C2, C3 C1, C2, C3 La2, La5, La6, La7 La3, La4 La2,La5, La7 La2, La5, La6, La7 N1, N2, N3, N4 N1, N2, N3, N4 N1, N2, N3, N4 N1, N2, N3, N4 PEK_U01 (skills) T1A_U08, InzA_U01 C1, C2, C3 La2-La7 N1, N2, N3, N4 PEK_U02 PEK_U03 PEK_U04 PEK_U05 PEK_U06 PEK_U07 T1A_U08, InzA_U01 T1A_U08, InzA_U01 T1A_U08, InzA_U01 T1A_U08, InzA_U01 T1A_U08, InzA_U01 T1A_U08, InzA_U01 C1, C2 C1, C2 C1, C2, C3 C1, C2, C3 C1 C1, C2, C3 La2, La5, La6, La7 La3, La4 La2,La5, La7 La2, La5, La6, La7 La2-La7 La3, La6 N1, N2, N3, N4 N1, N2, N3, N4 N1, N2, N3, N4 N1, N2, N3, N4 N1, N2, N3, N4 N1, N2, N3, N4 ** - enter symbols for main-field-of-study/specialization educational effects *** - from the table above 110 Zał. nr 4 do ZW 64/2012 FACULTY of CHEMISTRY / DEPARTMENT……………… SUBJECT CARD Name in Polish …… Bezpieczeństwo techniczne Name in English …… Technical safety Main field of study (if applicable): Chemical Technology Specialization (if applicable): …………………….. Level and form of studies: 1st/ 2nd* level, full-time / part-time* Kind of subject: obligatory / optional / university-wide* Subject code TCC014006 Group of courses YES / NO* Lecture 15 Number of hours of organized classes in University (ZZU) Number of hours of 30 total student workload (CNPS) Examination / Form of crediting crediting with grade* Classes Laboratory 15 Project Seminar Examination / crediting with grade* Examination / crediting with grade* 30 Examination / crediting with grade* Examination / crediting with grade* For group of courses mark (X) final course Number of ECTS points 1 including number of ECTS points for practical (P) classes including number of ECTS points for direct teacher-student contact (BK) classes 1 1 1 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 1. Knowledge of chemistry on the secondary school level 2. Fundamental knowledge on the chemical safety 3. Skill in computer operation \ SUBJECT OBJECTIVES C1 To familiarize students with the basics of technical safety C2 National and European law regulations related to the technical safety C3 Learning algorithms for analysis of industrial installations hazards C4 Teach students of the health risk assessment associated with industrial failures C5 Familiarizing students with examples of spreading chemical pollution and with the methodology of calculations of spreading the contaminants in the environment 111 SUBJECT EDUCATIONAL EFFECTS relating to knowledge: PEK_W01 - familiar with basic concepts and definitions of technical safety PEK_W02 - can specify the basic legislative acts governing the national and European technical safety rules PEK_W03 – knows the common elements of industrial operational and emergency response PEK_W04 – familiar with the main provisions of environmental law, Seveso III directive and of the Convention on the transboundary effects of industrial accidents PEK_W05 – able to apply methods of risk analysis to identify possible failure in industrial installations PEK_W06 – knows how to describe the basic methods of analysis of the health risks in areas contaminated as a result of industrial accidents relating to skills: PEK_U01 – can use the databases in order to classify plants in terms of the risks involved PEK_U02 – knows how to carry out an analysis of the hazards in simple industrial installations PEK_U03 – can suggest remedial measures in the event of an industrial accident in simple chemical installations PEK_U04 – can perform simple calculations of exposure to the contamination of the environment after the failure of industrial plant PEK_U05 – can use the tools to model the spreading of chemical contamination relating to social competences: PEK_K01 – able to work in a team PEK_K02 – feels responsible for the results of the tasks entrusted to PROGRAMME CONTENT Form of classes - lecture Number o f h o u r s Lec Basic concepts. The subject of technical safety, safety perception, the essence of 1 enterprise security, basic definitions, security scopes, importance of safety as a guarantee of the existence of an entity, the risk and examples of threats to the elements of the environment. Risks for the environment. The state of insecurity, its social and economic effects. Types of security. Examples of technical failures, the analysis of the causes and effects. Lec Safety-related items. Safety features versus general security companies. 2 Organisation and management, skills, specificity of manufacturing technology, infrastructure condition, emergency planning, internal reviews and analysis of accidents, development of safe work, organisation of operational service posts, striving for as few nuisance work. Analysis of the causes of industrial accidents. Characteristics of chemical companies, dangers, hazardous chemical substances. Lec Polish and the European legislation. Environmental law, Directive 67/548/EEC. 3 Groups of substances and preparations considered dangerous. Explosive substances (E) oxidizing (O), extremely flammable (F+), flammable (F), flammable (R10), very toxic (T+), toxic (T), harmful (Xn), corrosive (C), irritant 112 2 2 2 (Xi), sensitizing (R42 and/or R43), carcinogenic (karc..), mutagenic (Muta.), toxic to reproduction (Repr.), which are dangerous for the environment (N or/and R52, R53, R59), European Council Directive 96/82/EC, the Convention on the transboundary effects of industrial accidents, environmental law, Sevesoenterprises, non-Seveso enterprises, criteria. Lec Toxic industrial agents, industrial accidents, severe crashes, industrial 4 contamination. Process safety. Functional safety, safety assessment map. A comprehensive evaluation of the installation process in the various phases of the realisation of the investment. Lec Risk assessment methods. Identification of potential threats. HAZard and 5 OPerability Study (hazard and operability study), its goals, importance, specialty risks. Keywords, main and auxiliary keywords, installations, design objectives, deviations from design intent, hazards, parameter, operational problems, the experts, the process, pairs of keywords in hazards analysis. Lec Examples of HAZOP analysis. Chemical process, the analysis of installation 6 nodes, HAZOP team of experts, the structure of the team, the team of experts work scheme, the development of HAZOP report, deviation, deviation result, the security, the action. Certification of persons carrying out safety circuits, design and service. Lec The principles of contamination assessment resulted from the industrial 7 accidents, toxicity, carcinogenicity, principles for the risks evaluation in areas contaminated as a result of industrial accidents. Exposure-transmission pathreceptor relationship. Elements of the risk assessment procedures, hazard identification, exposure assessment, dose-response identification, risk assessment, uncertainty analysis. Health risk, the risk quotient, the risk index. Elimination of the effects of industrial accidents, environment remediation Lec methods for the areas contaminated as a result of industrial accidents, examples. 8 Summary. Knowledge check. Total hours 2 2 2 2 1 15 Form of classes - class Number of hours Form of classes - laboratory Number of hours Lab Determination of the limits of flammability and explosion of chemical 1 substances 2 Lab Determination of the effects related to the influence of toxic vapours of volatile 2 substances resulting from industrial accidents 2 Lab Analysis of explosive substances emissions and risks associated with their 3 spread in the environment Lab Calculation of the level limits of toxic substances during outflow from a tank, 4 taking into account different topography and atmospheric conditions 2 Lab Analysis of risks related to the emission of toxic substances during the free 5 evaporation from the open tank 2 Lab Liquefied gas discharge from a pipeline. Hazard analysis and prevention 6 consultation and the development of exercises. 2 Lab Calculation of the migration limits of dangerous substances and their 7 concentrations in areas with dense infrastructure 2 113 2 Lab Consultations and development of laboratory reports. 8 Total hours 1 15 TEACHING TOOLS USED N1. Software EFFECTS 9 to calculate the potential risks arising from industrial accidents N2. ALOHA software to calculate the effects of emissions of hazardous substances into the environment N3. Multimedia presentations N4. The laboratory test stand EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Way of evaluating educational effect achievement Evaluation (F – forming Educational effect number (during semester), P – concluding (at semester end) P (lecture) PEK_W01 – final test PEK_W06 F (laboratory) PEK_U01 – PEK_U05 reports from the laboratory excercises P1 (laboratory) = (F1+F2+F3+F4+F5+F6)/6 PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [25] M.Ryng, Bezpieczenstwo techniczne w przemsle chemicznym , WNT Warszawa 1985 [26] Praca zbiorowa, Zapobieganie stratom w przemyśle, Pol. Łódzka, Łódź 1999 [27] W. Pihowicz, Inżynieria bezpieczeństwa technicznego, Problematyka podstawowa, WNT 2009 SECONDARY LITERATURE: [19] Granice palności zgodnie z normą PN-EN 720-2, wskaźniki wybuchowości zgodnie z normą PN-EN26184-2, temperatury zapłonu w tyglu Clevelanda i Pensky’ego Martnsa [20] Wydawnictwo Ministerstwa Przemysłu Chemicznego pt. "Niebezpieczne materiały chemiczne - charakterystyka, zagrożenia, ratownictwo" - Biuro Wydawnicze "Chemia" Warszawa 1989r. SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Dr hab. inż. Adam Pawełczyk, [email protected] 114 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Technical safety AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical Technology Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** Programme content*** Teaching tool number*** K2Atc_W15 C1 Wy1 N3 K2Atc_W15 K2Atc_W15 K2Atc_W15 C1 C1, C2 C2 Wy2 Wy3- Wy4 Wy4- Wy5 N3 N3 N3 PEK_W05 K2Atc_W15 C3 Wy6- Wy7 N3 PEK_W06 (skills) PEK_U01 PEK_U02 PEK_U03 PEK_U04 PEK_U05 (competences) PEK_K01 K2Atc_W15 C4 Wy8 N3 K2Atc_U17 C3 La1 N4 K2Atc_U17, S2Atc_W05 K2Atc_U17, S2Atc_W05 K2Atc_U17, S2Atc_W05 K2Atc_U17 C3 C3, C4 C3, C4 C4 La1 – La2 La3 – La4 La5 – La6 La2-La8 Wy1 – Wy8, La1 – La7 N1 N1 N1-N2 N1-N2 (knowledge) PEK_W01 PEK_W02 PEK_W03 PEK_W04 K2Atc_K1 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 115 N1-N4 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Projekt technologiczny Technological project Chemical Technology 1st level, full-time obligatory TCC016001 NO Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacher–student contact (BK) classes 32. 33. 34. 35. C1 C2 Classes Laboratory Project 15 45 60 180 examination crediting with grade 2 6 Seminar 6 0.5 1.5 PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES Basic principles of chemical engineering Basic principles of chemical technology Chemical technology Chemical engineering SUBJECT OBJECTIVES Providing the students with the design procedures. Acquiring the fundamental knowledge about technological-equipment solutions 116 C3 C4 C5 C6 C7 concerning the given production process. Providing the students with the rules of process balancing, selection and design of process equipment and apparatuses selection. Providing design algorithms concerning selected apparatuses sizing. Presentation of procedures used in making the technological-equipment schemes of production processes. Acquiring the fundamental knowledge about economical aspects of the designed plant (rules of investment and exploitation costs calculation). Providing the students with the information about computer programs for design – e.g. CAD. SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – Knows the general rules concerning elaboration of new technological plants, PEK_W02 – Knows basic methods and algorithms used in solving of engineering and design problems, PEK_W03 – Has general knowledge in the field of investment feasibility analysis, production process course, as well as processes and unit operations, PEK_W04 – Knows the rules concerning making of mass and energy balances in the designed plant, PEK_W05 – Knows how to select basic equipment items and process apparatuses, as well as knows design algorithms of the basic process apparatuses, PEK_W06 – Knows how to make technological-equipment scheme of the industrial plant, PEK_W07 – Knows the rules of estimation of investment costs and exploitation costs, PEK_W08 – Can use CAD programs in design problems. Relating to skills: PEK_U01 – Can use information and communication techniques, can use CAD programs for design problems and propose specific technological-equipment solution of the production process, PEK_U02 – Can determine productivity of the batch and continuous plant, PEK_U03 – Can make calculations for selected, basic heat and diffusional processes and flow operations, PEK_U04 – Can make material and energy balances, PEK_U05 – Can design basic process equipment and adjust the apparatuses, PEK_U06 – Can elaborate the technological-equipment scheme of the technological plant, PEK_U07 – Can design simple industrial plant according to the given assumptions. PROGRAMME CONTENT Number of hours Form of classes – lecture Lec 1 Design rules. Multistage elaboration of new technologies, technological-equipment assumptions, process project, 2 technological project, investment feasibility analysis. Lec 2 Input data for design. Raw materials, energy, products, wastes, 2 environment protection. Lec 3 Production process course. Processes and unit operations, general 2 117 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 scheme of the production process. Mass and energy balances. Balancing rules. Sankey’s diagram. Indicators of raw materials and energy consumption. Technological-equipment solution. Rules and guidelines in selection of apparatuses and equipment items in industrial plant. Rules of making the technological-equipment schemes. Design rules of process apparatuses. Rules of estimation of the investment and exploitation costs. Application of CAD programs for design. Total hours Proj 1 Proj 2 Proj 3 Proj 4 Proj 5 Proj 6 – Proj 8 Proj 9 Proj 10 Proj 11 Proj 12 Proj 13 Proj 14 Proj 15 2 2 2 2 1 15 Number of hours Form of classes – project Making general schemes of the exemplary production processes – batch and continuous plants for real design 3 assumptions (raw materials, energy). Calculation of productability of the continuous (kg/h) and batch (kg/batch) plant for the assumed annual productability (Mg product/year) and for assumed 3 annual economic capacity (Mg raw material/year). Application of CAD programs for design. Design calculations for the selected unit operations of momentum transfer: flows in pipeline and in selected 6 process apparatuses, selection of pumps, sedimentation, filtration, mixing and mixers. Design calculations for the selected unit operations involved heat transfer, heat conduction and heat 3 transfer, heat exchanger. Design calculations for selected mass transfer operations: absorption, adsorption, extraction, 9 distillation, crystallization, mass exchangers, including continuous reactors and batch stirred reactors. Material balances for the exemplary production 6 processes in continuous and batch plants. Energy balances for exemplary production processes 6 in continuous and batch plants. Calculations of basic process apparatuses in the designed plants: tank, mixer, reactor with mixer; pump 3 selection. Making of technological-equipment scheme of the designed technological plant – in continuous and batch 3 modes. Material revision. Credit test. 3 Total hours 45 118 N1 N2 N3 N4 TEACHING TOOLS USED Lecture with multimedia presentation. Plant design. Solution of specific design tasks. Project consultations. EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect number Way of evaluating Evaluation F – forming (during semester), educational effect C – concluding (at semester end) achievement C (lecture) PEK_W01 – PEK_W08 Examination C(project) PEK_U01 – PEK_U07 Crediting with grade PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [28] J. Ciborowski, Podstawy inżynierii chemicznej, WNT, Warszawa, 1982. [29] R. Koch, A. Noworyta, Procesy mechaniczne w inżynierii chemicznej, WNT, Warszawa, 1992. [30] J. Pikoń, Aparatura chemiczna, PWN, Warszawa, 1978. [31] D.W. Green, R.H. Perry (red.), Perry’s chemical engineers’ handbook, 8th ed., McGraw–Hill, 2007. [32] S. Kucharski, J. Głowiński, Podstawy obliczeń projektowych w inżynierii chemicznej, OWPWr, Wrocław, 2000. [33] Pr. zbiorowa, Zadania projektowe z inżynierii procesowej, OWPW, Warszawa, 1986. [34] K. Szmidt–Szałowski red., Podstawy technologii chemicznej. Bilanse procesów technologicznych, OWPW, Warszawa, 1997. SECONDARY LITERATURE: [21] Himmelblau, Basic principles and calculation in chemical engineering, N. Y., 1986. [22] G.I. Wells, L.M. Rose, The art of chemical process design, Elsevier, 1986. [23] W.D. Seider, Process design principles, J.W.&S., 1999. [24] U. Bröckel, W. Meier, G. Wagner (red.), Product design and engineering. Vol. 1: Basics and technologies, Vol. 2: Raw materials, additives and application, Wiley, 2007. SUBJECT SUPERVISOR (NAME AND SURNAME, E–MAIL ADDRESS) Prof. dr hab. inż. Andrzej Matynia, [email protected] 119 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Technological project AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical technology Subject educational effect (knowledge) PEK_W01 PEK_W02 PEK_W03 PEK_W04 PEK_W05 PEK_W06 PEK_W07 PEK_W08 (skills) PEK_U01 PEK_U02 PEK_U03 PEK_U04 PEK_U05 PEK_U06 PEK_U07 Correlation between subject educational effect and educational effects defined for main field of study and specialization Subject objectives Programme content Teaching tool number K1Atc_W24 K1Atc_W24 K1Atc_W24 K1Atc_W24 K1Atc_W24 K1Atc_W24 K1Atc_W24 K1Atc_W24 C1 C2 C2 C3 C3, C4 C5 C6 C7 Lec1 Lec2 Lec3 Lec4 Lec5 Lec6 Lec7 Lec8 N1 N1 N1 N1 N1 N1 N1 N1 K1Atc_U29 K1Atc_U29 K1Atc_U29 K1Atc_U29 K1Atc_U29 K1Atc_U29 K1Atc_U29 C1, C2 C2, C7 C3 C3 C4 C5 C1 – C7 Proj 1 Proj 2 Proj 3 – Proj 8 Proj 9 – Proj 12 Proj 13 Proj 14 Proj 15 N2 N2 N3 N2, N3 N2, N3 N2, N4 N2 – N4 120 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Technologia Węgla i Materiałów Węglowych Technology of Coal and Carbon Materials Chemical Technology 1st / full-time optional TCC010014 NO *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 30 60 crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 36. General Chemistry SUBJECT OBJECTIVES C1 C2 C3 To gain knowledge on the current technologies of coal processing, resultant products and their application To acquaint with environmental impact of processing and using solid fossil fuels To gain the basic knowledge on the manufacturing technologies and properties of engineering and porous carbon materials 121 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – Possesses the knowledge on the meaning, resources, technological properties and possible use of solid fossil fuels PEK_W02 – Can describe facilities and technologies used for coal coking PEK_W03 – Is familiar with cokery products, their technological properties and utilization PEK_W04 – Has knowledge on the coal gasification technology, raw gas processing and fields of synthesis gas use PEK_W05 – Is familiar with the environment protection related to coal coal processing and combustion PEK_W06 – Knows the technology of carbon and graphite artifact manufacture and understand the relationship between structure, texture and properties PEK_W07 – Is familiar with the methods of activated carbon production PEK_W08 – Has a basic knowledge on the synthesis and properties of nanostructured carbons PROGRAMME CONTENT Number of hours Form of classes - lecture Lec 1 Role of solid fossil fuel as an energy source. Resources and areas of coal utilisation. Classification of solid fossil fuels. Lec 2 Coal beneficiation (grinding, classification, enrichment). Fundamentals of termochemical coal processing. Pyrolysis and hydropyrolysis. Direct coal hydrogenation. Lec 3 Coal blending for coke manufacture. Construction of coking battery. Technology of metalurgical coke production. Lec 4 Raw coking gas processing (condensation, ammonia utilization, benzole separation). Processing of coal-tar. Properties and application of coking products. Lec 5 Technology of coal gasification. Purification and reforming of raw synthetic gas. Fields of synthetic gas utilization. Lec 6 Technologies of coal combustion. Environmental protection in coal processing and energy production. CO2 emission reduction. Lec 7 Raw materials for electrode industry. Conventional technologies of carbon and graphite artifacts production. Properties and application of carbon and graphite artifacts. Lec 8 Raw materials for activated carbons production. Methods of porosity developing. Properties and application of activated carbons. Lec 9 Carbon fibers and composites. Gas-phase pyrolysis – carbon black and pyrolytic carbon. New areas of carbon materials application. Lec 10 Test Total hours N1 TEACHING TOOLS USED Lecture with multimedial presentation 122 3 3 3 3 3 3 3 3 3 3 30 EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect number Way of evaluating educational effect Evaluation F – forming (during achievement semester), C – concluding (at semester end) C PEK_W01-PEK_W08 Test PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [1] A.Karcz, Koksownictwo, Wydawnictwa AGH, Kraków 1991, [2] J.G. Speight, The Chemistry and Technology of Coal, Marcel Dekker, New York 1994. SECONDARY LITERATURE: [1] Praca zbiorowa, Czysta energia, produkty chemiczne i paliwa z węgla – ocena potencjału rozwojowego, Wydawnictwo Instytutu Chemicznej Przeróbki Węgla, Zabrze 2008 [2] H. Marsh, E.A. Heintz, F.Rodriguez-Reinoso, Introduction to Carbon Technologies, Alicante 1997. SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Prof. dr hab. inż. Jacek Machnikowski, [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Carbon Materials AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Materials Engineering Subject educational effect Correlation between subject Subject educational effect and educational objectives*** effects defined for main field of study and specialization (if applicable)** (knowledge) C1 PEK_W01 C1 PEK_W02 C1 PEK_W03 C1 PEK_W04 C2 PEK_W05 C3 PEK_W06 C3 PEK_W07 C3 PEK_W08 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 123 Programme content*** Teaching tool number*** Lec 1, Lec 2 N1 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 Lec 9 N1 N1 N1 N1 N1 N2 N1 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Technologia Lekkiej Syntezy Technology of Fine Chemicals Chemical Technology 1st level, full-time optional TCC010030 NO *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 30 60 Crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 37. 38. 39. C1 C2 C3 Basis knowledge in the field of nonorganic chemistry an of organic chemistry. Principles of technical chemistry. Knowledge in the field of basis of technological chemistry is recommended. SUBJECT OBJECTIVES Gaining of the knowledge on the modern technologies of deep processed chemicals, in the point of view of their chemical structures and of their applications. Acquaintance with the different technological concepts in the field of fine chemicals syntheses, taking the profitability and ecological aspects of the production process into the consideration. Expanding the knowledge in the field of small-scale production of fine chemicals using High-Tech processes. 124 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: Student, who has completed the course: PEK_W01 – has a knowledge on types and application of fine chemicals, PEK_W02 – has a knowledge on types of syntheses of fine chemicals, PEK_W03 – has a knowledge on the popular technologies of fine chemicals production, PEK_W04 – has a knowledge on modern technologies of fine chemicals syntheses, especially High-Tech processes keeping up the ecological aspects, PEK_W05 – has a knowledge on economy of fine chemicals syntheses, in the point of view of profitability of them, PEK_W06 – has a knowledge on marketing principles, as the elements of profitability and demand for the production of fine chemicals. PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 Lec 9 Lec10 Lec11 Lec12 Lec13 Lec14 Form of classes - lecture Fine chemicals – deep processed organic compounds; introduction, definition, manufacturing, products characteristics. Antistatic agents. Cationic surfactants. Manufacturing. Commercially available products – their characteristics.. Ionic liquids; definition, structures and properties. Technologies of manufacturing. Silicones and their meaning - commercially available products in the fine chemicals industry. Products for cosmetics industry as bio-oils, plant oils, waxes, flavors and fragrances (I). Products for cosmetics industry as vitamins, fitohormones, collagen and elastin (II). Organic dyes and pigments - examples of manufacturing. Biocides and plant protection products - examples of manufacturing. The industry of perfumens and olfactory compositions – from isolation to fine chemicals synthesis. The rules of olfactory compositions creation on basis of synthetic and natural products. Pharmaceuticals as the cost-effective branch of production of fine chemicals. Types and manufacturing of accompanying ingredients of drugs formulations. „Espying of nature” – the synthesis of antibiotics, antivirals and anticancer drugs. Examples of syntheses. Medicines on blood circulation system – the examples of manufacturing. The cost of production and the final price of the product. Drugs on nervous system – medicines and para pharmaceutical products – common features and differences of manufacturing technology. Patent protection and implementation of new technologies of fine chemicals. The processes of registration of new products (fine 125 Number of hours 2 2 2 2 2 2 2 2 2 2 2 2 2 2 chemicals) - the technical requirements. Lec15 Marketing i application of fine chemicals. Total hours N1 2 30 TEACHING TOOLS USED Informative lecture with the use of multimedia. EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) C PEK_W01 – PEK_W06 The preparation of a multimedial presentation on the selected topic of a fine chemicals technology of organic compounds. PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [25] Hill RM, Silicone surfactants – new developements Current Opinion in Colloid and Interface Science 2002; 255-261 [26] Przondo J., Związki powierzchniowo czynne i ich zastosowanie w produktach chemii gospodarczej Radom 2007 [27] Current issues of Przemysł Chemiczny [28] Reference Document on Best Available Techniques for the Manufacture of Organic Fine Chemicals August 2006 [29] NIIR Board., Modern technology of perfumes, flavours and essential oils. 2nd Ed. 2004. National Institute of Industrial Research. [30] Lednicer D., The organic chemistry of drug synthesis. Vol. 7. 2008. John Willey and Sons. [31] Johnson D. S., Li J. J., The art of drug synthesis. 2007. John Willey and Sons. [32] The act from 30th of June, 2000. The law on the industrial ownership. [33] The act from 4th February, 1994. Copyright and the related law. SECONDARY LITERATURE: [1] Panda H., Perfumes and flavours technology. 2010. Asia Pacific Business Press Inc. [2] Levin M. Pharmaceutical process scale-up. 2002. Marcel Dekker Inc. SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) 126 prof. dr hab. inż. Kazimiera A. Wilk, [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT TECHNOLOGY OF FINE CHEMICALS AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY CHEMICAL TECHNOLOGY Subject educational effect PEK_W01 Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** C1, C3 selectable course PEK_W02 C1, C2, C3 PEK_W03 C2 PEK_W04 C2, C3 PEK_W05 C2, C3 PEK_W06 C1, C2, C3 127 Programme content*** Lec1, Lec2, Lec3, Lec4, Lec5, Lec6, Lec7, Lec8, Lec9, Lec10, Lec11, Lec12, Lec13 Lec1, Lec2, Lec3, Lec4, Lec5, Lec6, Lec7, Lec8, Lec9, Lec10, Lec11, Lec12, Lec13 Lec1, Lec2, Lec3, Lec4, Lec5, Lec6, Lec7, Lec8, Lec9, Lec10, Lec11, Lec12, Lec13 Lec1, Lec2, Lec3, Lec4, Lec5, Lec6, Lec7, Lec8, Lec9, Lec10, Lec11, Lec12, Lec13 Lec2, Lec3, Lec4, Lec5, Lec6, Lec7, Lec8, Lec9, Lec10, Lec11, Lec12, Lec13, Lec14, Lec15 Lec2, Lec3, Lec4, Lec5, Lec6, Lec7, Lec8, Lec9, Lec10, Lec11, Lec12, Lec13, Lec15 Teaching tool number*** N1 N1 N1 N1 N1 N1 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Technologia układów dyspersyjnych Technology of disperse systems Chemical Technology No applicable 1st/ 2nd* level, full-time / part-time* obligatory / optional / university-wide* TCC010033 YES / NO* *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar 30 60 crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 40. 41. Basic information on physicochemistry of colloid systems of an application and industrial meaning There are necessary the following optional cources: Technology of Fine Chemicals and Additives for Detergents and Polymers SUBJECT OBJECTIVES C1 C2 Opportunities to learn the main fabrication and application methods of disperse systems (cosmetics, pharmacy, metallurgy, polymers) Opportunities to learn the most important feature on disperse systems, their properties and manufacturing C3 C4 128 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – knowing types and designation of forms of disperse systems PEK_W02 – kwowing mechanismsm and efectivity of colloidal stabilization Relating to skills: PEK_U01 – knowing theoretical and thechnological rules for the disperse systems formation PEK_U02 – knowing technical methods of disperse sustems’ performance forms Relating to social competences: PEK_K01 – knowing influence of components on final characteristics of disperse systems PEK_K02 – knowing main attempts to study physicochemical and performance properties of disperse systems PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Lec 8 Lec 9 Lec 10 Form of classes - lecture Disperse systems, definition and propesties. Colloidal systems and their characteristics. Performance forms of disperse systems. Emulsion systems. Liposomes and vesicles. Foams and aerosols. Solid dispersion. Gold and silver bionanotechnology, biosynthesis of silver and gold nanoparticles,gold and silver nanoparticles characterization, application of silver and gold nanoparticles Polymer-surfactant interaction, polymer-surfactant interaction in solution, adsorption of polymer and surfactant on the solid surface, biosurfactants, MEOR technology, coagulation, flocculation Minerals flotation,super- hydrophobic surfaces, physicochemical base of mineral, flotation reagents, sulfide minerals flotation, flotation deinking, paper recycling Suspension polymerization and their potential in polimer technology Emulsion polymerization and their potential in polimer technology Polymers in chemical catalysis. Gels and hydrogels and their uses Disperse systems in current literature Disperse systems in current patent literature Total hours N1 N2 … TEACHING TOOLS USED Informative lecture with the use of multimedia 129 Number of hours 3 3 3 3 3 3 3 3 3 3 30 EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) PEK_W01 – PEK_W06 C Crediting with grade PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [35] Textbook, J. Rosen, Surfactants and Interfacial Phenomena, Wiley, 1989 Wiley, 1989. [36] R. Zieliński, Surfaktanty, Towaroznawcze i ekologiczne aspekty ich stosowania, Wyd. Akad. Ekonom., Poznań, 2000. [37] J. Pielichowski, A. Puszyński, Technologia tworzyw sztucznych, WNT, Warszawa, 1994. SECONDARY LITERATURE: [34] Jan Ogonowski, Anna Tomaszkiewicz-Potępa, Związki Powierzchniowo Czynne, Kraków 1999. [35] Michael S. Showell, Handbook of Detergents, Part D, Formulations, vol. 128. [36] S. Anastasiu, E. Jelescu, Środki powierzchniowo Czynne, WNT, Warszawa 1973. SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) prof. dr hab. inż. Kazimiera A. Wilk, [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Technology of disperse systems AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical Technology Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** Subject objectives*** (knowledge) PEK_W01 C1 PEK_W02 C1, C2 130 Programme content*** Lec1, Lec2, Lec10 Lec1-Lec3, Lec6, Lec8 Teaching tool number*** N1 N1 (skills) PEK_U01 C1, C2 PEK_U02 C1, C2 (competences) C2 PEK_K01 C2 PEK_K02 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 131 Lec1, Lec5, Lec6, Lec7 Lec4, Lec8, Lec9 Lec1-Lec6, Lec8, Lec9 Lec5, Lec7, Lec9, Lec10 N1 N1 N1 N1 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Krajowy przemysł chemiczny The Polish chemical industry TECHNOLOGIA CHEMICZNA 1st level, optional TCC010035 NO* *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar Examination / crediting with grade* Examination / crediting with grade* Examination / crediting with grade* Examination / crediting with grade* 30 60 crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 42. Basic knowledge of chemical technology. 43. SUBJECT OBJECTIVES C1 C2 C3 Knowledge and understanding of the problems of chemical technology. Understanding the dependencies and relationships occurring in chemical technology. To acquaint the student with the modern technologies used in the domestic chemical industry. 132 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – The student knows the source of the raw materials in the chemical technology and ways of obtaining them. PEK_W02 – The student has knowledge of the implementation process in industrial scale and conditions. Relating to skills: PEK_U01 – The student is able to diagnose the correct implementation of the process. … Relating to social competences: PEK_K01 The student can put into practice the theoretical knowledge acquired and apply their skills … PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Form of classes - lecture Information on the national chemical industry. Discussion of selected principles of chemical processes. Discussion of the basic of process systems and their compliance to objectives BAT. Operate of selected chemical technology in industrial scale. Number of hours Total hours TEACHING TOOLS USED N1 N2 N3 Lecture problem Multimedia presentation Own work - self-study and preparation for passing. EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) F1 F2 … C =F1 Lec 1 to Lec 4 written crediting with grade 133 2 6 16 30 PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [37] Józef Kępiński: Technologia chemiczna nieorganiczna. Warszawa: Państwowe Wydawnictwo Naukowe PWN, 1964. [38] A. Wielopolski: Technologia chemiczna organiczna. Warszawa: Państwowe Wydawnictwo Naukowe PWN, 1959. [39] Encyklopedia techniki – Chemia. Warszawa: Wydawnictwa NaukowoTechniczne, 1993. [40] Józef Zawadzki: Technologia chemiczna nieorganiczna. Warszawa: Biblioteka Techniczna, 1949. [41] P.H. Groggins: Procesy jednostkowe w syntezie organicznej (Unit processes in organic synthesis, 1958). Warszawa: Wydawnictwo Naukowo-Techniczne, 1961. [42] Atanazy Boryniec, Stefan Chudzyński, Stanisław Porejko, Stanisław Malinowski: Technologia chemiczna organiczna. T. II. Warszawa: Państwowe Wydawnictwo Naukowe, 1958. [43] Józef Kępiński: Technologia chloru i związków chloru. Warszawa: Wydawnictwo Naukowo-Techniczne, 1963. [44] Atanazy Boryniec: Technologia włókien sztucznych. Warszawa: PWT, 1956. [45] Romuald Klimek: Olejki eteryczne. Warszawa: Wydawnictwo Przemysłu Lekkiego i Spożywczego, 1957. [46] E. Grzywa, J. Molenda: Technologia podstawowych syntez organicznych Tom I i II, WNT Warszawa 1996. SECONDARY LITERATURE: [1] J. Molenda : Gaz ziemnyPWN Warszawa 1996. [2] J.G.Speight: The Chemistry and Technology of Petroleum Marcel Dekker Inc.1991. SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Dr hab. inż. Marek Kułażyński [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT The Polish chemical industry AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY I-st level. Subject educational effect (knowledge) Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** K1Atc_W09, K1Atc_W14 Subject objectives*** Programme content*** Teaching tool number*** C1, C2, C3. Lec 1 to Lec 4 N1, N2, N3. 134 PEK_W01 PEK_W02 PEK_W03 … (skills) PEK_U01 PEK_U02 PEK_U03 … K1Atc_W09, K1Atc_W13, K1Atc_W14 K1Atc_U23 C1, C2, C3. Lec 1 to Lec 4 N1, N2, N3. C1, C2, C3. Lec 1 to Lec 4 N1, N2, N3. K1Atc_K01, K1Atc_K02, C1, C2, C3. Lec 1 PEK_K01 K1Atc_K01 PEK_K02 PEK_K03 … ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above (competences) 135 to Lec 4 N1, N2, N3. Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Przemysłowe laboratorium technologii ropy naftowej i węgla I Name in English The industrial laboratory of crude oil and coal technology I Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Chemical technology 1st level, full-time obligatory TCC016006 NO *delete as applicable Lecture Classes Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Laboratory Project Seminar 30 60 crediting with grade For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 2 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 44. Basic knowledge of organic and inorganic chemistry SUBJECT OBJECTIVES C1 C2 Gaining a knowledge about processing of crude oil and coal The ability to assess the quality of raw materials and products and to define production process efficiency 136 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – Knowledge of crude oil and coal processing Relating to skills: PEK_U01 – The ability to assess the quality of raw materials, petroleum and coal-based products. PEK_U02 – The ability to define production process efficiency. PEK_U03 – The ability to detailed characterization of hydroisomerisation, steam reforming of ethanol, coal gasification, pyrolysis and flotation processes PEK_U04 – Knowledge about activated carbons manufacturing methods PEK_U05 – The ability to define activity and selectivity of catalyst used in the hydroisomerisation and steam reforming of ethanol PROGRAMME CONTENT Form of classes - laboratory Lab 1 Lab 2 Lab 3 Lab 4 Lab 5 Lab 6 Number of hours Hydroisomerysation of n-paraffins Hydrogen from ethanol Coal gasification Pyrolysis of coal and biomass Coal enrichment by flotation method Production of activated carbons Total hours N1 N2 N3 TEACHING TOOLS USED Realisation of experiment Performing of calculation Preparation of report EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) F1 F2 F3 PEK_U01PEK_U03, PEK_U05 PEK_U01PEK_U03, PEK_U05 PEK_U01PEK_U03 Test, laboratory report Test, laboratory report Test, laboratory report 137 4 4 4 4 4 4 24 F4 PEK_U01PEK_U03 F5 PEK_U01PEK_U03 F6 PEK_U01PEK_U04 C=(F1+F2+F3+F4+F5+F6)/6 Test, laboratory report Test, laboratory report Test, laboratory report PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [38] Grzywa E., Molenda J., Technologia podstawowych syntez organicznych, t. I i II, WNT, Warszawa, 2000. [39] Górska K., Górski W., Materiały pędne i smary, Wydawnictwa Komunikacji i Łączności, Warszawa 1986 [40] Kajdas C,. Chemia i fizykochemia ropy naftowej, WNT, Warszawa 1979. [41] Jankowska H., Świątkowski A., Choma J., Węgiel aktywny, WNT, Warszawa 1985. [42] Roga B,, Tomków K, Technologia chemiczna węgla, WNT, Warszawa 1971. SECONDARY LITERATURE: [47] H. Marsh, E.A.Heintz, F. Rodriguez-Reinoso, Introduction to Carbon Technologies, Publicationes, Univesrsity of Alicante, 1997. SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Rafał Łużny, [email protected] 138 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT The industrial laboratory of crude oil and coal technology AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical technology Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** PEK_W01 T1A_U08 InzA_U01 C1, C2 PEK_U01 T1A_U08 InzA_U01 C1, C2 PEK_U02 T1A_U08 InzA_U01 C1, C2 PEK_U03 T1A_U08 InzA_U01 C1, C2 PEK_U04 T1A_U08 InzA_U01 C1, C2 La6 N1, N2, N3 PEK_U05 T1A_U08 InzA_U01 C1, C2 La1, La2 N1, N2, N3 139 Subject objectives*** Programme content*** La1, La2, La3, La4, La5, La6 La1, La2, La3, La4, La5, La6 La1, La2, La3, La4, La5, La6 La1, La2, La3, La4, La5, La6 Teaching tool number*** N1, N2, N3 N1, N2, N3 N1, N2, N3 N1, N2, N3 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology Faculty of Chemistry SUBJECT CARD Name in Polish Przemysłowe laboratorium technologii ropy naftowej I węgla II Name in English The industrial laboratory of crude oil and coal technology II Main field of study (if applicable): Chemical Technology Specialization (if applicable): …………………….. Level and form of studies: 1st level, full-time Kind of subject: obligatory Subject code TCC017004 Group of courses YES Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Examination / Form of crediting crediting with grade* Classes Laboratory Project Seminar Examination / crediting with grade* Examination / crediting with grade* 30 60 Examination / crediting with grade* Examination / crediting with grade* For group of courses mark (X) final course Number of ECTS points 2 2 including number of ECTS points for practical (P) classes including number of ECTS points for direct teacher-student contact (BK) classes 1 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 1. Fundaments of inorganic chemistry 2. Fundaments of organic chemistry \ SUBJECT OBJECTIVES C1- to get the knowledge about the most important technological processes of crude oil processing, evaluation of the quality of raw materials and its products, evaluation of the efficiency of the production process. C2- to get the knowledge about the most important technological processes of coal processing, evaluation of the quality of raw materials and its products, evaluation of the efficiency of the production process. 140 SUBJECT EDUCATIONAL EFFECTS … relating to skills: PEK_U01 student is able to determine the groups of components of fuels fraction, PEK_U02 student is able to evaluate the quality of the products derived from hydrocarbon feedstocks PEK_U03 student is able to determine the groups of components of oil fraction PEK_U04 student is able to evaluate the utility if coal as energy source PEK_U05 student is able to evaluate the technological properties of pitch PEK_U06 student able to assess the property of coal as raw material for the coke production PROGRAMME CONTENT Form of classes - laboratory Lab 1 Lab 2 Lab 3 Number of hours Determination of composition of groups of the fuel fractions by FIA 5 Analysis of the fuels fractions by GC 5 Determination of composition of groups of oil fractions by column chromatography Lab Determination of the heat of combustion and calorific value of solid fuels 4 Lab Technological properties of pitch 5 Lab Determination of plastic properties of carbon 6 Total hours 5 5 5 5 30 TEACHING TOOLS USED N1. Preliminary lecture of the problem N2.Performing the laboratory class in laboratory room supplied with normalized equipment for the determination of the physicochemical and technological properties of coal and its derivatives. N3. Performing the laboratory class in laboratory room supplied with normalized equipment for the determination of physicochemical and technological properties of hydrocarbon fuels. N4. Final report EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Way of evaluating educational effect achievement Evaluation (F – Educational effect number forming (during semester), P – concluding (at semester end) F1 PEK_U01 F2 PEK_U02 F3 PEK_U03 F4 PEK_U04 Preliminary test -70%, active participation in class- 5% -; the final report -25% of the evaluation Preliminary test -70%, active participation in class- 5% -; the final report -25% of the evaluation Preliminary test -70%, active participation in class- 5% -; the final report -25% of the evaluation Preliminary test -70%, active participation in class- 5% -; the 141 F5 PEK_U05 F6 PEK_U06 final report -25% of the evaluation Preliminary test -70%, active participation in class- 5% -; the final report -25% of the evaluation Preliminary test -70%, active participation in class- 5% -; the final report -25% of the evaluation C= (F1+F2+F3+F4+F5+F6)/6 PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [43] [44] [45] [46] [47] Grzywa E., Molenda J., Technologia podstawowych syntez organicznych, t.I i II, WNT, Warszawa, 2000. Schmit-Szałowski K., Podstawy technologii chemicznej, Of.Wyd.PW, Warszawa, 1997. Bortel E., Koneczny H., Zarys technologii chemicznej, PWN, Warszawa, 1992. Jankowska H., Świątkowski A., Choma J., Węgiel aktywny, WNT, Warszawa, 1985. Roga B., Tomków., Technologia chemiczna węgla, WNT, Warszawa, 1971. SECONDARY LITERATURE: [1] Marsh H., Heintz E.A., Rodriguez-Reinoso F., Introdutcion to Carbon Technologies, University of Alicante, 1997. [2] [3] SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS) Dr inż. Ewa Lorenc-Grabowska, [email protected] MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT The industrial laboratory of crude oiland coal technology II AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical Technology Subject educational effect Subject objectives*** Programme content*** Teaching tool number*** C1 C1 C1 C2 C2 La1 La2 La3 La4 PEK_U05 Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** T1A_U08, InzA_U01 T1A_U08, InzA_U01 T1A_U08, InzA_U01 T1A_U08, InzA_U01 T1A_U08, InzA_U01 La5 N1,N3,N4 N1,N3,N4 N1,N3,N4 N1,N2,N4 N1,N2,N4 PEK_U06 T1A_U08, InzA_U01 C2 La6 N1,N2,N4 PEK_K01(competences) PEK_U02 PEK_U03 PEK_U04 PEK_K01 PEK_K02 … ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 142 Zał. nr 4 do ZW 64/2012 Wrocław University of Technology FACULTY OF CHEMISTRY SUBJECT CARD Name in Polish Name in English Main field of study (if applicable) Specialization (if applicable) Level and form of studies: Kind of subject Subject code Group of courses Woda w procesach technologicznych Water in technology Chemical Technology 1st level, full-time optional TCC010037 NO* *delete as applicable Lecture Number of hours of organized classes in University (ZZU) Number of hours of total student workload (CNPS) Form of crediting Classes Laboratory Project Seminar Examination / crediting with grade* Examination / crediting with grade* Examination / crediting with grade* Examination / crediting with grade* 30 60 Examination / crediting with grade* For group of courses mark (X) final course Number of ECTS points including number of ECTS points for practical (P) classes including number of ECTS points for direct teacherstudent contact (BK) classes 2 *delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES 45. 46. Basic knowledge on chem technology Knowledge on inorganic chemistry and organic chemistry SUBJECT OBJECTIVES C1 C2 Introduction to water management Presentation of methods for water and wastewater treatments 143 SUBJECT EDUCATIONAL EFFECTS Relating to knowledge: PEK_W01 – students know the basic processes and operations used in water technology and are familiar with selection of the more efficient parameters PEK_W02 – Students know the general rules in designing new technologies, ... Relating to skills: PEK_U01 – students can shape and solve the problems Relating to social competences: PEK_K01 students understand a need to transfer their knowledge on engineering achievements to communities PROGRAMME CONTENT Lec 1 Lec 2 Lec 3 Lec 4 Lec 5 Lec 6 Lec 7 Lec8 Lec9 Form of classes - lecture Availability of water in the world, in Europe and in Poland, water cycle, water in technology, close cycles Sources of water pollution: natural, industrial, agriculture and domestic Legal regulations of water quality, Polish Water Decree and EU directives Principles of sedimentation and flocculation, chemicals Systems for sedimentation and flocculation Water demineralization by ion-exchange resins, chelating resins, processing Electrolysis and ED demineralization, ion-exchange membranes, EDI systems Reverse osmosis and water desalination, membranes and modules Forward osmosis, recovery of water and energy in salinity gradient systems, Lec10 Desalination of seawater, modern trends in design of SWRO plants, megatone installations, sea-mining Lec11 Dialysis and some exam[ples of its use Lec12 UF and MF, membranes and modules, membrane fouling, module regeneration Lec13 MD and PV in water purification and recovery of valuable components Lec14 Submerged membrane systems in WWTP, bioreactors Lec15 Exam Total, hours 144 Number of hours 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 30 N1 TEACHING TOOLS USED Lecture with PPT presentations EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT Educational effect Way of evaluating educational effect Evaluation F – forming (during number achievement semester), C – concluding (at semester end) C PEK-W01, W02 PEK-U01 PEK-K01 Exam PRIMARY AND SECONDARY LITERATURE PRIMARY LITERATURE: [48] [49] [50] Water and wastewater engineering: design and practice: D.L.Mackenzie, McGraw Hill, 2o1o, Water quality control handbook, E.R.Alley, McGraw Hill 2oo7 Oczyszczanie wody: podstawy teoretyczne i technologiczne, A.L.Kowal PWN 2oo9 SECONDARY LITERATURE: Innovative materials and methods for water treatment, M.Bryjak, CRC 2o16 SUBJECT SUPERVISOR (Prof. Dr. Marek Bryjak, [email protected]) 145 MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT Water for technology AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical Technology Subject educational effect Correlation between subject educational effect and educational effects defined for main field of study and specialization (if applicable)** (knowledge) PEK_W01 PEK_W02 (skills) PEK_U01 (competences) Subject objectives*** Programme content*** Teaching tool number*** C1, C2 Lec4-Lec14 N1 C1, C2 Lec1-Lec3 N1 C1, C2 Lec1-Lec14 N1 Lec4-Lec14 N1 C1, C2 PEK_K01 ** - enter symbols for main-field-of-study/specialization educational effects *** - from table above 146