UPDATE OF TECHNICAL REQUIREMENTS
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UPDATE OF TECHNICAL REQUIREMENTS
Projekt współfinansowany ze środków Europejskiego Funduszu Rozwoju Regionalnego w ramach Programu Operacyjnego Innowacyjna Gospodarka Oświęcim, 04.02.2015 L.dz. 47/TZ/PM/2015 UPDATE OF TECHNICAL REQUIREMENTS Conc: Inquiry / Contrator selection for DELIVERY AND INSTALLATION OF THE TWO PIECES OF 5 l BATCH GLASS REACTORS WITH TOOLS, INSTRUMENTS AND APPARATUS FOR THE S-SBR PLANT : European Regional Development Fund under the operational Program Innovative Economy Project no POIG.04.05.01-00-003/12 PROJECT: "Implementation of innovative technology of rubbers SSBR X3 production in Synthos Dwory 7 spółka z ograniczoną odpowiedzialnością spółka jawna" POIG.04.05.01-00-003 / 12 „Wdrożenie innowacyjnej technologii wytwarzania kauczuków SSBR X3 w Synthos Dwory 7 spółka z ograniczoną odpowiedzialnością spółka jawna” POIG.04.05.01-00-003/12 CLIENT: SYNTHOS DWORY 7 –Spółka z ograniczoną odpowiedzialnością spółka jawna The change concern Appendix no 2 – below new updated requirements Other terms and conditions of the query 47/TZ/PM/2015 without changes Appendix no 2. Technical requirements 5 l batch glass reactor no 1 ( 1 piece ) Wymagania / Requirements Ciśnienie projektowe / design pressure Temperatura projektowa / design temperature Płaszcz grzewczo/chłodzący - Coats - heating / cooling Czujnik temperatury / temperature sensor Pomiar ciśnienia / Pressure Measurement Mieszadło z napędem / Driven stirrer Przeznaczony do strefy Ex/ Suitable for Ex zone Dokumentacja w j. polskim / Documentation in Polish Pokrywa do reaktora winna być wyposażona w 4 stożkowe szlify żeńskie 3 , stożkowe szlify 14 i króciec do wprowadzania substancji stałych ( proszków) / Reactor cover should be equipped with 4 NS tapered female jonts 32, and 2 NS tapered female jonts 14 and a input for introducing solids (powders) Mieszadła/ stirrer Uwagi / Comments -1 do +1 bar - do C Tak / YES Tak /YES Tak/YES Tak/YES Tak/YES Tak/YES Pt100 manometr Zakres 0-500 obr/min - Range 0-500 rev / min Strefa / Zone II 2B T3 Tak/ YES Tak/YES 1 szt kotwicowe, 3 szt łopatkowe, 3 szt wirnikowe Anchor 1 piece, 3-piece paddle, 3-piece rotary Strona 1 z 3 Projekt współfinansowany ze środków Europejskiego Funduszu Rozwoju Regionalnego w ramach Programu Operacyjnego Innowacyjna Gospodarka Zestaw destylacyjny z chłodnicą zwrotną / The distillation assembly with a reflux condenser Podnoszona pokrywa na stelażu / Lifting lid on the rack Reaktor wyposażony w dolny króciec spustowy / A reactor equipped with a bottom drain adapter Tak/YES Mieszadło mechaniczne wyposażone w suche uszczelnienie. / Mechanical stirrer equipped with a dry seal. Tak/ YES Reaktor powinien posiadać czujniki temperatury umożliwiające kontrolę temperatury płaszcza i mieszaniny reakcyjnej wewnątrz reaktora. / The reactor should have temperature sensors to enable control of the coat temperature and the reaction mixture inside the reactor Tak/ YES Dodatkowy odbieralnik 2L / Additional receiver 2L Tak/YES Tak/ YES 5 l batch glass reactor no 2 ( 1 piece ) Reason: R&D investigations of emulsion polymerization at a laboratory scale to understand dependence among reaction parameters, and provide customers with new polymer samples. Parameters: All equipment must be compatible with EX zone. Reactor: Size: 5 liters (final working volume 70-80% from 5 liters) Min/max pressure: 0,04/+2 bar Min/max temperature: -5/ 1 °C Material of Construction: Must be compatible with styrene, butadiene, organic solvents, amines, water solutions of acids and bases (pH range from 3,5 to 12) Agitator: Capable of mixing viscous polymer dispersion (up to 50 000 cPs) – may need to test – 230/400V, three phase 50 Hz, EEx e ii T4, max speed approximately 0-200 rpm, double helix impeller. The thermocouple must be immersed in the reaction medium. The agitator with a frame at the height min. 70% complete, and must be helical. motor sufficient for highly viscous systems 50000cPs operating system and vacuum system. JULABO (cooling and warming system). EX design. Vessel: Borosilicate glass (or better) stirrer vessel 5 liter, max pressure at least 0,04/+2 bar, with heating and cooling jacket, heating min. to 1 °C, cooling min. oC, bottom drain valve. Vessel body is cylindrical. Cover Plate: Has a center opening for agitator, and 5 openings: Strona 2 z 3 Projekt współfinansowany ze środków Europejskiego Funduszu Rozwoju Regionalnego w ramach Programu Operacyjnego Innowacyjna Gospodarka 1. One for Vacuum vent line 2. One for temperature control 3. One for condenser 4. One for charging hopper or biurette 5. One for future growth – empty at this time Bottom Exit Line: Manual ball valve, must have the ability to take samples of viscous latex through a needle outlet fairly quickly. It has to be easy to clean, even when the undesirable coagulation process takes place in the reactor. Stand: Stainless steel construction Accessories: heating and cooling system sufficient for 5l volume, temperature probes with sufficient cable, additional parts for stirrer equipment, additional bottom drain valve, additional separating valves, spare parts and tools sufficient to keep us running. Condenser Line: Manual open/close valve, condenser with approx. 0.1 m2 (or more) exchange area, manual open/close valve for venting. Vacuum pump line Must be capable of working with 0,04 bar absolute pressure. Consisting of condenser and vacuum pump. All elements must be resistant to styrene, butadiene, amines, organic solvents and water solutions of bases or acids (pH range from 3,5 to 12). Waste vessel – 2,5 L could be made from glass resistant to low pressure (0,04 bar) (optional) All lines must be easily detachable for ease of cleaning. System: Must be computer (automatic) operated: -stirring -temperature (Jacket and reactor interior) - vacuum valve opening -parameters such as: rpm, torque, temperatures (in jacket and reactor), should be displayed on the screen. Strona 3 z 3