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MATERIA£Y CERAMICZNE /CERAMIC MATERIALS/, 64, 1, (2012), 22-25 www.ptcer.pl/mccm Birefringence of glass-air photonic crystal ¿bre induced by elliptical microholes of cladding IRENEUSZ KUJAWA1*, RYSZARD BUCZYēSKI1, 2, DARIUSZ PYSZ1, TADEUSZ MARTYNKIEN3, HUGO THIENPONT4 Institute of Electronic Materials Technology, Glass Laboratory, WólczyĔska 133, 01-919 Warsaw, Poland University of Warsaw, Faculty of Physics, Pasteura 7, 02-093 Warsaw, Poland 3 Wroclaw University of Technology, Institute of Physics, WybrzeĪe WyspiaĔskiego 27, 50-370 Wroclaw, Poland 4 Vrije Universiteit Brussel, Department of Applied Physics and Photonics, Pleinlaan 2, 1050 Brussels, Belgium *e-mail: [email protected] 1 2 Abstract In this paper, we report on the fabrication of the birefringent photonic crystal ¿bre with a photonic cladding composed of elliptical holes ordered in a rectangular lattice. Choice of such con¿guration allows obtaining birefringence in photonic crystal ¿bres. In this case two-fold rotational symmetry is achieved and the polarized orthogonal modes (HE11x and HE11y) are not degenerated. We discuss the inÀuence of structural parameters including the ellipticity of the air holes and the aspect ratio of the rectangular lattice on the birefringence and on the modal properties of this glass-air microstructural ¿bre. Keywords: Photonic crystal ¿bres, Microstructured ¿bres, Birefringence, Multicomponent glass DWÓJàOMNOĝû W SZKLANO-POWIETRZNYM ĝWIATàOWODZIE FOTONICZNYM WYWOàANA ELIPTYCZNYMI MIKROOTWORAMI PàASZCZA W artykule przedstawiono uzyskane wáókno dwójáomne o anizotropii optycznej wywoáanej eliptycznym ksztaátem elementów páaszcza fotonicznego i prostokątnym ksztaátem przekroju. WyraĨnie okreĞlona dwuosiowoĞü prowadzi do duĪych róĪnic efektywnych wspóáczynników zaáamania dla dwóch podstawowych i ortogonalnie spolaryzowanych modów HE11x i HE11y. DziĊki temu mody te nie są zdegenerowane. ZaleĪnie od parametrów strukturalnych wáókna moĪliwe jest uzyskanie znacznych wartoĞci dwójáomnoĞci. W artykule przedstawiono zarys technologii wytwarzania szklanych wáókien tego typu, przedyskutowano wpáyw parametrów strukturalnych na wartoĞü dwójáomnoĞci i wáasnoĞci modowe oraz wyniki symulacji i pomiarów dla uzyskanego wáókna. Sáowa kluczowe: Ğwiatáowody fotoniczne, Ğwiatáowody mikrostrukturalne, dwójáomnoĞü, szkáa wieloskáadnikowe 1. Introduction The high birefringence in the photonic crystal ¿bres (PCFs) is a result of large effective index anisotropy possible to achieve only in the two-fold rotational symmetry photonic structure [1]. A typical PCF which has three-fold rotational symmetry (m = 3) with an ideal hexagonal lattice and circular holes is not birefringent [2]. For real samples of such ¿bres, degeneracy of fundamental mode breaks down due to fabrication imperfections and low-birefringence always occurs. However, a photonic crystal ¿bre with global anisotropy can achieve extremely high birefringence of the order of 10-2 when rectangular lattice and elliptical-like air holes are applied [3]. Such PCFs can ¿nd applications in the optical ¿bre directional transverse strain sensors with the bene¿t that their rectangular cross-section allows avoiding twist during mounting and provides straightforward orientation of the polarization axis with respect to the direction of applied force, and in many others applications for example in sensing and in the telecommunication [4, 5]. Unfortunately 22 elliptical holes with controlled dimensions are indeed much more dif¿cult to obtain than circular holes. In this paper we deal with our latest achievements in the fabrication of such rectangular lattice. First, we brieÀy describe the fabrication process. Second, we deal with the measurement set-up and with our experimental results. Finally, we present the results our simulations. 2. Fabrication The lattice geometry used at the PCF preform stage inÀuences the shape of the air holes formed during the ¿bre drawing process [6, 7]. One typically observes the tendency to form air holes with a shape that matches the lattice geometry. This effect can be controlled for structures with a high air-¿lling factor. Choosing a rectangular lattice at the preform stage therefore results in elliptical air holes during drawing of the subpreform (Fig. 1). However, during ¿bre drawing, the subpreform air holes tend to become circular, which renders controlling the ellipti- BIREFRINGENCE OF GLASS-AIR PHOTONIC CRYSTAL FIBRE INDUCED BY ELLIPTICAL MICROHOLES OF CLADDING a) b) c) Fig. 1. Subpreform with rectangular air holes: a) general view, b) core, c) single hole. Rys. 1. Szklana subpreforma o prostokątnych otworach: a) widok ogólny, b) obszar rdzenia, c) pojedynczy otwór. Fig. 2. The photos of obtained PCF. Rys. 2. ZdjĊcia wytworzonego wáókna. cal hole features very dif¿cult (Fig. 2). To specify the obtained structure, we rely on the following de¿nitions: the lattice constant along the X-axis ȁx; the lattice constant along the Y - axis ȁy; the lattice constant ratio ȡ = ȁy /ȁx; the ellipticity of the air holes Ș = dx/dy (where dx and dy represent the minor and major axis of the air-¿lled ellipse) and the linear ¿lling factors fx and fy given by fa = da /ȁa , when a is X or Y. The lattice constants of our ¿bre are ȁx = 1.35 ȝm and ȁy = 2.25 Pm. The size of the elliptical holes varies slightly depending on the location in the structure (Fig. 2). The holes have a minor and major axes dx = 735 nm and dy = 960 nm, respectively, yielding linear ¿lling factors of fx = 0.54 and fy = 0.43 and Ș = 0.76. The base material for our PCF is a borosilicate glass labelled NC-21A. This multicomponent glass is synthesized in-house at the ITME and has an oxide composition detailed in Table 1. This glass is selected to verify our stack and draw technology for elliptical holes fabrication. The main physical properties of NC21A are: – refractive index nD = 1.533, – density ȡ = 2.50 g/cm3, – coef¿cient of thermal expansion Į20–300 = 82·10í7 Kí1, – glass transition temperature Tg = 500°C, – softening point DTM = 530°C. Fig. 3. The curve of viscosity for NC-21A. Rys. 3. Krzywa lepkoĞciowa dla szkáa NC-21A. Table 1. Oxide composition of borosilicate NC-21A glass. Tabela 1. Skáad tlenkowy borokrzemianowego szkáa NC-21A. Oxide composition of borosilicate NC-21A glass [wt%] SiO2 Al2O3 B2O3 Li2O Na2O K2O As2O3 55.0 1.0 26.0 3.0 9.5 5.5 0.8 Fig. 4. Spectral transmission of NC-21A glass. Rys. 4. Transmisja spektralna szkáa NC-21A. MATERIA£Y CERAMICZNE /CERAMIC MATERIALS/, 64, 1, (2012) 23 I. KUJAWA, R. BUCZYēSKI, D. PYSZ, T. MARTYNKIEN, H. THIENPONT The curve of viscosity for NC-21A is present in Fig. 3. The transmission of NC-21A glass is limited to the range 380–2700 nm (Fig. 4) with a moderate attenuation of 4–6 dB/m. For the preform fabrication, we use ellipse-like glass capillaries with axis aspect ratio of 0.33 and linear ¿lling factors of fx = 0.90 and fy = 0.75 ordered in a rectangular lattice. The core of the ¿bre is formed with 3 rectangular rods. During subpreform and ¿bre drawing, we use a low-speed drawing process to ensure homogenous heat distribution in the subpreform and a relatively low pulling temperature of 730 °C to preserve the ellipticity of the air holes. The drawing process is performed on a 6-m-long ¿bre drawing tower. We use a feeding speed of 1.5 mm/min, while the pulling speed is 0.6 m/min. Adjusting those drawing parameters is essential to obtaining elliptical holes. For our ¿nal ¿bre (Fig. 2), we intentionally chose a rectangular cross section, which allows easily identifying the main axis and avoiding twisting of the ¿bre in the measurement set-ups. 3. Measurement results The parameters characterizing a photonic crystal ¿bre with the global anisotropy are the phase birefringence B de¿ned as the difference between the propagation constants Ex and Ey of the two orthogonally polarized components HE11x and HE11y of the fundamental mode: B O Ex Ey 2S neff X neffY O Lb (1) and the group birefringence G de¿ned as: G B-O dB dO (2) B and G are different for PCFs, while they are almost the same for conventional ¿bres [8]. We used the spectral interferometric method with crossed polarizers to determine the group birefringence. The interferometer is shown in Fig. 5. Polarized supercontinuum light obtained with a highly nonlinear PCF pumped with a femtosecond Ti:Sapphire laser is launched into our ¿bre. A ¿rst polarizer is aligned so that both polarization modes were equally excited. At the output of our ¿bre, an analyzer is oriented at 90° with respect to the input polarizer. The output signal is registered using a spectrum analyzer and monitored with a CCD camera. The CCD camera allows verifying proper light coupling into the core of the PCF. The spectrum analyzer records the modulation of the intensity as a function of wavelength, which results Fig. 5. Group birefringence measurement set-up. Rys. 5. Ukáad pomiarowy. 24 MATERIA£Y CERAMICZNE /CERAMIC MATERIALS/, 64, 1, (2012) Fig. 6. The measured interferogram, which shows interference between polarization components in the PCF (1.2 m is cut-off wavelength for single mode regime). Rys. 6. Interferogram uwidaczniający interferencje skáadowych polaryzacji we wáóknie PCF (1,2 m jest dáugoĞcią odciĊcia). from the interference between the polarized components of the propagating mode. Maximum intensity occurs when: d'M dO r2S (3) where 'ij is the phase shift corresponding to successive fringes in the output spectrum represented by their maxima, and 'Ȝ is the distance between successive fringes. The group birefringence given by (2) can then be calculated as: G O2 d'M 2SL dO O2 'OL (4) where Ȝ is an average wavelength between two successive fringes, and L is the length of the measured ¿bre. A measurement interferogram is depicted in Fig. 6. Fig. 7. Values of group birefringence obtained from interferogram (Fig. 6) for two regimes: left: two-modal, and right: single mode. Rys. 7. WartoĞci dwójáomnoĞci grupowej uzyskane z interferogramu (Rys. 6) dla zakresu dwumodowego (krzywa po lewej) i jednodomowego (krzywa po prawej). BIREFRINGENCE OF GLASS-AIR PHOTONIC CRYSTAL FIBRE INDUCED BY ELLIPTICAL MICROHOLES OF CLADDING Using an image from the actual structure obtained with a Scanning Electron Microscope (SEM) we performed numerical analysis of the structure by means the ¿nite element method (FEM). Simulations show that 2 modes are guided in the ¿bre (1.2 m is cut-off wavelength for obtained structure). Moreover for the fundamental mode at the wavelength 1.5 m the phase birefringence reaches the value of 2.2·10-4 (calculated) and the group birefringence 3.0·10-4 (measured). Acknowledgements Fig. 8. Dispersion of NC-21A glass. Rys. 8. Dyspersja szkáa NC-21A. Measured values of a group birefringence obtained from the interferogram and an equation (4) are presented in Fig. 7. The group birefringence for the fundamental mode at the wavelength 1.5 Pm reaches the values of 3.0·10-4. Using in-house software based on the ¿nite element method (FEM), we calculated the phase birefringence using the actual structural parameters as obtained from the SEM photography (Fig. 2). In the simulation we took into account the material dispersion of NC-21A glass (Fig. 8). Calculations con¿rmed that 2 modes are guided in the structure. The phase (B) birefringence for the fundamental mode at the wavelength 1.5m was calculated, and reaches the values of 2.2·10-4. 4. Conclusions In this paper, we present a rectangular lattice photonic crystal ¿bre with elliptical like holes made of the high quality silicate glass NC-21A. The manufactured ¿bre has a lattice pitch ȁx = 1.35 m and ȁy = 2.25 m for main axes X and Y, respectively, and elliptical holes with ellipticity Ș = 0.76. The average ¿lling factors of 0.5 is obtained. The core of the ¿bre is rectangular with dimension 3.3 m x 5.4 m. This work was supported in part by Polish Ministry of Science and Information Society Technologies grant NN515244737, by the COST 299 action, and by an internal scienti¿c grant of ITME. Some of the numerical results were obtained using computer resources of the Interdisciplinary Centre for Mathematical and Computational Modelling (ICM), University of Warsaw. The authors of the paper would like to thank Dr R. StĊpieĔ (from ITME) for synthesis of NC-21A glass. References [1] Ortigosa-Blanch A., Knight J.C., Wadsworth W.J., Arriaga J., Mangan B.J., Birks T.A., Russell P. St. J.: Opt. Lett., 25, (2000), 1325. [2] Steel M.J., White T.P., Martijn de Sterke C., McPhedran R.C., Botten L.C.: Opt. Lett., 26, (2001), 488. [3] Wang L., Yang D.: Opt. Express, 15, 14, (2007), 8892-7. [4] Frazao O., Santos J., Araujo F., Ferreira L.: Laser Photonics Rev., 2, (2008), 449. [5] Martynkien T., Szpulak M., UrbaĔczyk W.: Appl. Opt., 44, (2005), 7780. [6] Bjarklev A., Broeng J., Bjarklev A.S.: Photonic Crystal Fibres (Kluwer Academic, Dordrecht, 2003) [7] Kujawa I., Pysz D., BuczyĔski R., Filipkowski A., StĊpieĔ R.: Electrical Review, 86, 10, (2010), 72. [8] Antkowiak M., KotyĔski R., Nasiáowski T., Lesiak P., Wójcik J., UrbaĔczyk W., Berghmans F., Thienpont H., J: Opt. A, Pure Appl. Opt., 7, (2005), 763. i Received 21 September 2011; accepted 15 December 2011 MATERIA£Y CERAMICZNE /CERAMIC MATERIALS/, 64, 1, (2012) 25