Arch. Min. Sci., Vol. 52 (2007), No 3, p. 331–354
Transkrypt
Arch. Min. Sci., Vol. 52 (2007), No 3, p. 331–354
Arch. Min. Sci., Vol. 52 (2007), No 3, p. 331–354 331 JAN LIS*, PIOTR KIJEWSKI* METHODOLOGY OF TESTING THE STRENGTH AND DEFORMATIONAL PROPERTIES OF ROCKS FROM LGOM MINES UNDER TRIAXIAL STRESS CONDITIONS METODYKA BADAŃ WŁASNOŚCI WYTRZYMAŁOŚCIOWYCH I ODKSZTAŁCENIOWYCH SKAŁ Z KOPALŃ LGOM W TRÓJOSIOWYM STANIE NAPRĘŻEŃ The paper presents the laboratory equipment used in triaxial tests carried out at the Rock Mechanics Laboratory of the Mining Department, the KGHM CUPRUM Ltd Research & Development Centre. The equipment for triaxial tests at confining pressures of up to 250 MPa which allows for the determination of the strength and deformational properties of rocks is described. Using the results of the tests, the criteria for rock failure under compression, shear, tension and bending were determined. An attempt to monitor the propagation of cracks in rocks under hydrostatic pressure up to 60 MPa was also undertaken. Keywords: deformational properties, failure criterion, rock strength, triaxial laboratory tests W artykule przedstawiono wyposażenie pomiarowo-badawcze stosowane w trójosiowych badaniach skał prowadzonych w Pracowni Mechaniki Skał, Laboratorium Górnictwa i Mechaniki Górotworu KGHM CUPRUM. Badania te rozpoczęto w 1970 roku dla potrzeb budowy kopalń rud miedzi w nowo odkrytym złożu w obszarze monokliny przedsudeckiej. Badania są wykonywane w pełnym profilu górniczym, obejmującym skały złożowe i skały w najbliższym otoczeniu złoża (strop, spąg). Zakres prowadzonych badań w warunkach trójosiowego stanu naprężeń obejmował: • określenie wytrzymałościowych i odkształceniowych własności skał przy ściskaniu, ścinaniu, rozciąganiu i zginaniu w warunkach wszechstronnego ciśnienia; • wyznaczenie charakterystyk mechanicznych skał i określenie stałych sprężystości; • określenie wytrzymałości skał w złożonym stanie naprężenia, w którym składowe tego stanu mają różne wartości i znaki; • opracowanie, na podstawie wyników badań trójosiowych, warunków kruchego zniszczenia skał; • badania nad rozprzestrzenianiem się szczelin w materiale skalnym poddanym działaniu wszechstronnego ciśnienia. * KGHM CUPRUM LTD RESEARCH & DEVELOPMENT CENTRE, PL. JANA PAWŁA II, 50-136 WROCŁAW, POLAND 332 Badania wytrzymałości i deformacji skał w warunkach trójosiowego stanu naprężenia realizowane są według dwóch wariantów: 1. σ1 > σ2 = σ3 (wg tzw. schematu Kármána), tj. warunek, w którym na jednoosiowy stan naprężenia nakłada się hydrostatyczny stan ciśnień. 2. σ1 ≠ σ2 ≠ σ3 – warunek złożonego stanu naprężeń, w którym składowe tego stanu mają różne wartości i znaki. Dla realizacji przyjętego programu skonstruowano stanowisko badawcze, z prototypową aparaturą i urządzeniami, składające się z następujących elementów: • układu hydraulicznego zasilającego komory ciśnieniowe; • układu obciążającego z maszynami wytrzymałościowymi; • aparatury z wyposażeniem pomiarowym i rejestrującym; • zestawu komór badawczych (ciśnieniowych) o zróżnicowanych konstrukcjach stosownie do rodzaju prowadzonych badań. Badania skał w trójosiowym stanie naprężenia polegały na określeniu wytrzymałości badanej próbki skalnej przy minimum trzech różnych poziomach ciśnień okólnych, zależnych od wytrzymałości i zwięzłości skały. Uwzględniając zmienne właściwości skał występujących w profilu górniczym złoża rud miedzi LGOM badania prowadzone są przy następujących ciśnieniach okólnych: • 5, 10, 15, i 10; 20; 30 MPa - dla skał słabych, o niskiej zwięzłości; • 20, 40, 60 MPa - dla skał mocnych, zwięzłych i silnie zwięzłych. Do badań próbek skalnych przy ściskaniu służą trzy typy komór ciśnieniowych: 1. komora typu M-23 własnej konstrukcji do ciśnień w zakresie 0÷60 MPa (rys. 3.1); 2. komora tłoczkowa typu M-25 własnej konstrukcji do ciśnień w zakresie 0÷120 MPa (rys. 3.2); 3. komora firmy Walter+Bai produkcji szwajcarskiej do ciśnień w zakresie 0÷250 MPa (rys. 3.3). Wyniki badań wytrzymałościowych i odkształceniowych właściwości skał w trójosiowym stanie naprężeń są wykorzystywane w obliczeniach inżynierskich, przy projektowaniu obiektów górniczych oraz w modelowaniu procesów deformacji górotworu podczas prowadzenia eksploatacji złoża rud miedzi w kopalniach LGOM. Słowa kluczowe: badania trójosiowe, warunek kruchego zniszczenia, własności odkształceniowe, wytrzymałość 1. Introduction The intensification of rock-mass pressure symptoms in the vicinity of mine workings, which are determined by the behavior of rock under complex stress, occurs as a result of mining operations. In predicting the stresses and deformations induced in the rock mass, the physical and mechanical properties of rocks under triaxial stress conditions, particularly when the extraction is carried out at greater and greater depths play a crucial role. Mining the copper deposit in the Legnica-Głogów Copper District (LGOM), which started in 1967 in the Lubin mine and later in the Polkowice mine, required the identification of the geomechanical properties of rocks occurring in these unfamiliar mine strata. At first the tests determined the basic strength and deformational properties, but as early as in 1970, in the Laboratory of Rock Mechanics in Copper Research and De- 333 sign Office “Cuprum”, tests under complex stress condition were begun. The tests were carried out for a full mining profile including the ore deposit and the surrounding rocks, i.e. sandstones, carbonate rocks and sulphate rocks. The scope of tests under triaxial stress conditions included: • determination of the strength and deformational properties at compression, shear, tension and bending under hydrostatic pressure conditions; • determination of the mechanical characteristics of rocks and elasticity constants; • determination of rock strength under complex stress conditions, when the components of the stress state are of different values and signs; • elaboration of rock failure criteria based on the test results; • investigation of the propagation of cracks in rock material under hydrostatic pressure conditions. 2. Methods and measures for testing rock samples under triaxial stress conditions Tests of strength and deformations under triaxial stress conditions were carried out using two variants: 1. σ1 > σ2 = σ3 – axi-symmetric stress conditions, i.e. the conditions, in which hydrostatic pressure is superposed onto uniaxial stress (the co-called Kármán loading scheme); 2. σ1 ≠ σ2 ≠ σ3 – asymmetric or general triaxial stress conditions, i.e. the conditions where all three principal components of the stress tensor are different. The programme of the experiments included tests of the impact of pressure on rock strength and deformation under stress, shear, tension and bending conditions. To implement this programme, a test station with prototype testing apparatuses and devices was designed and built. It consists of the following systems: • hydraulic system feeding the pressure chambers; • loading system (testing machines); • instrumental system including measuring and recording equipment; • system with testing pressure chambers having a structure adequate for the type of tests (Fig. 1). 2 . 1 . Te s t s o f t h e s t r e n g t h a n d d e f o r m a t i o n a l p r o p e r t i e s o f r o c k s under axi-symmetric compressive stress conditions Tests of rock samples under triaxial compressive stress conditions consisted in determining the strength of the tested rock at a minimum of three different confining pressure levels, depending on the strength and compactness of the rock. Taking into consideration 334 the variable properties of rocks occurring in the mining profile of the copper deposit in the LGOM area, the tests were carried out at the following confining pressures: • 5, 10, 15, and 10, 20, 30 MPa – for weak rocks with low compactness; • 20, 40, 60 MPa – for strong, compact and highly compact rocks. According to the so-called Kármán scheme (σ1 > σ2 = σ3), the major principal stress σ1 in the sample is generated along its vertical axis, while minor principal stresses, induced by confining pressure (where σ2 = σ3 = p), operate in radial directions (Fig. 1). s1 s2 = s3 = p s1 s2 = s3 = p Fig. 1. Pattern of sample loading in the conventional triaxial compression test (the so-called Kármán scheme) Rys. 1. Schemat obciążania próbki w próbie na konwencjonalne trójosiowe ściskanie (tzw. schemat Kármána) A rock sample in an air-dry state is placed in a special rubber jacket to protect it against oil penetration and is enclosed in a leak-proof pressure chamber (Fig. 2) where axially symmetric stress conditions are induced in the sample. Confining pressure (p = σ2 = σ3) is applied to the sample by hydraulic oil while the vertical stress (σ1) is generated mechanically by testing machine at a constant rate of 1.0 MPa/s. The mechanical properties of the rocks tested under compressive conditions were determined using solid cylindrical samples having a diameter of 44 mm and a slenderness ratio of 1.0 (strength properties) and 2.0 (strength and deformational properties). Three types of pressure chambers for triaxial compression tests on rock samples were used: 1. M-23 chamber (designed by the authors) for 0÷60 MPa pressures (Fig. 3.1), 2. M-25 piston chamber (designed by the authors) for 0÷120 MPa pressures (Fig. 3.2), 3. Walter+Bai chamber (Swiss made) for 0÷250 MPa pressures (Fig. 3.3). 335 piston sample cylinder oil inlet cover sleeve Fig. 2. Scheme of a pressure chamber for triaxial compression tests Rys. 2. Schemat komory ciśnieniowej do badań trójosiowych przy ściskaniu Fig. 3. High-pressure triaxial chambers for compression tests on rocks samples Rys. 3. Wysokociśnieniowe komory trójosiowe do badań próbek skalnych na ściskanie Compressive stresses produced in the sample under triaxial loading conditions are as follows: s1 = P > s 2 = s3 = p Fo (1) 336 where: σ1 P Fo σ2 σ3 p — — — — — — vertical stress (major principal stress), vertical load, initial cross-sectional area of sample, intermediate principal stress, minor principal stress, confining pressure. Vertical stress σ1 reduced by hydrostatic pressure acting on the sample is called the differential stress or deviatoric stress (σ1 – σ3), and the differential stress at failure is called the differential compressive strength under triaxial stress conditions (σ1 – σ3)max: (s1 - s 3 )max = Pmax -p Fo (2) When represented by Mohr circles of principal stresses, the triaxial compression test results allow the failure criterion for the rock tested in the form of a Mohr envelope of the circles (Fig. 4) to be determined. In the simplest case, the Mohr envelope is a straight line described by the Coulomb equation: t = sn tan j + c (3) where: τ σn φ c — — — — ultimate shear stress, normal (compressive) stress, internal friction angle, cohesion. The state of stress in the sample is also described by principal stresses: σz, σφ, σr acting in the axial direction z, the perimeter (tangential) direction φ and the radial direction r, respectively. The plane perpendicular to the hydrostatic axis in the space of principal stresses is called the octahedral plane (σz + σφ + σr = const). In this plane the normal stress (σoct) operates: soct = sz + sr + sj 3 (4) as well as the shear (tangential) stress τoct: toct = 1 ( s z - sr ) 2 + (s z - sj ) 2 + ( sj - sr ) 2 3 (5) 337 Highly compact, fine-grained quartz sandstone c = 40.0 MPa; j = 32.3° Shear stress t, MPa 200 150 100 50 0 0 50 100 150 200 250 300 350 400 Normal stress sn , MPa Fig. 4. Coulomb-Mohr rock failure criterion under triaxial stress conditions Rys. 4. Kryterium zniszczenia skał wg Coulomba-Mohra w trójosiowym stanie naprężenia Taking into consideration the condition where σφ = σr = p, the following is obtained: soct = 2 p + sz 3 toct = 2 (soct - p) (6) (7) An example of conventional triaxial test results for dolomitic rocks is presented in Figure 5. This figure shows the dispersion of results and the average ultimate strength’s dependence on confining pressure. In order to determine the general criterion of rock failure, the compressive strength chart in the octahedral plane (τoct – σoct) is plotted in Figure 6 for a selected package of rock strata. This chart includes the trajectories of loading the sample until it fails. The strength trajectory was approximated by a straight line using the least squares method. The equation of this line is as follows: toct = 0.7225 soct + 38, MPa (8) This equation is valid for normal stresses: 55 MPa £ soct £ 175 MPa (9) When analysing changes in the differential compressive strength of roof rocks, it was confirmed that the rate of strength change decreases with a pressure increase within the 338 420 400 380 360 340 Max. differential stress (s1 – s 3)max, MPa 320 300 280 260 240 220 200 180 160 140 120 Fig. 5. Ultimate strength of dolomites under conventional triaxial compression conditions 100 80 60 0 10 20 30 40 50 60 Confining pressure p, MPa Rys. 5. Wytrzymałość graniczna dolomitów w warunkach konwencjonalnego trójosiowego ściskania range of applied pressures. Rock compressive strength at a pressure of p = 60 MPa is three times higher compared to the uniaxial strength. Rocks, which under uniaxial stress conditions have a high strength, also keep this feature under triaxial stress conditions. Observations of a sample fracturing pattern during the tests showed that rocks under uniaxial compression break into small fragments in a brittle manner with an audible acoustic effect. This is because the elastic volumetric strain energy accumulated in the sample during loading is released instantly, which is characteristic for rocks susceptible to bursting. The moment of sample disintegration was difficult to capture as the rupture occurred without any warning. In the case of homogeneous rocks with a low susceptibility to bursting, two chip-shaped cones were formed after failure. 339 180 sz 160 sr = sj = p Shear octahedral stress t oct, MPa 140 sz 120 p p p 100 p 80 60 40 20 0 20 40 60 80 100 120 140 160 180 Normal octahedral stress s oct, MPa Fig. 6. Failure criterion of dolomites in the octahedral plane under axi-symmetric triaxial stress conditions (σ1 > σ2 = σ3) Rys. 6. Kryterium zniszczenia dolomitów w płaszczyźnie oktaedrycznej w osiowo-symetrycznym trójosiowym stanie naprężenia (σ1 > σ2 = σ3) Samples tested under triaxial stress conditions failed without audible acoustic effects. The disintegration of samples after strength failure was not sudden but progressed slowly, and the rupture of the sample was signalled by an increase of pressure in the hydraulic system and a decrease in vertical load (a decrease in the load-bearing capacity of the sample). The higher the confining pressure, the lower the sample disintegration rate after the strength failure. The result of each test of the deformational properties of rocks are the mechanical characteristics of rocks in the form of stress-strain plots. These plots depict the mechanical behaviour of rocks under different confining pressures (Fig. 7). The modulus of deformation does not change substantially with a change of confining pressure. This is probably due to the diminishing influence of rock heterogeneity under triaxial stress conditions. Thus, it can be assumed that the slope of linear sections of σz – ε1 curves is independent of confining pressure; it is only the length of these sections that increases with an increase of pressure. 340 p=60 p=50 p=60 MPa p=50 300 Axial stress s z , MPa p=40 p=30 p=20 p=10 p=40 p=30 p=20 p=10 200 lateral strain p=0 p=0 150 axial strain 100 50 -4 -2 0 4 2 6 8 Strain e, 10–3 Fig. 7. Deformational characteristics of dolomites under triaxial compressive stress conditions Rys. 7. Charakterystyki odkształceniowe dolomitów w trójosiowym stanie naprężeń ściskających 2 . 2 . Te s t s o f t h e s t r e n g t h a n d d e f o r m a t i o n a l p r o p e r t i e s o f r o c k s at tension under triaxial stress conditions Tests of tensile strength were carried out using a pressure chamber of the M-17 type (Fig. 8). The chamber allows for the conditions of pure tension as well as conditions of compression and tension to be created. During such tests, deformation can be measured by using electric resistance strain gauges. Tension tests were performed on profiled (dogbone-shaped) samples with varying diameter in the middle part (d = 24÷32 mm) and a constant D = 44 mm diameter in the thick end parts. The samples were subjected to oil pressure in the M-17 chamber. Increasing hydrostatic pressure causes compression of a sample and at the same time tension by a force equal to the product of pressure and the difference between area in the thick part and in the middle part of sample. Combined lateral compression with axial tension causes a fracture of the sample. When the sample is extended by hydrostatic pressure (p), the axial stress is: s z = p (1 - D2 ) d2 (10) 341 Fig. 8. M-17 triaxial chamber for tension tests of rocks Rys. 8. Komora trójosiowa typu M-17 do badań skał na rozciąganie On the octahedral plane, stresses are equal to: – normal octahedral stress σoct soct = pæ D2 æ ç3 - 2 ç 3 çè d çè (11) toct = 2 D2 p 3 d2 (12) – shear octahedral stress τoct The octahedral stresses were used when determining the failure criterion for the rocks tested. In order to determine the plastic strain at failure δz under tensile conditions, the method of calculating the sample necking at the moment of failure developed by Bridgman was used. According to this method, the plastic strain at failure was calculated using the formula: d z = ln Fo F (13) where: Fo — initial cross-sectional area of sample at the middle part, F — cross-sectional area of the sample at the central middle part at the moment of failure. 342 e2 Axial stress s z , MPa Figure 9 presents the deformation characteristics for a limestone sample subjected to extension under hydrostatic pressure conditions. In addition, Figure 10 shows the plastic strain of the extended rock samples at the moment of failure in the pressure chamber. 8 e1 6 4 2 -200 0 200 400 600 Strain e, 10–6 Fig. 9. Deformation characteristics of limestone at extension under hydrostatic pressure conditions Rys. 9. Charakterystyka odkształceniowa wapienia przy rozciąganiu w warunkach wszechstronnego ciśnienia It was observed during the tests that rock samples undergo only slight deformation, while the deformations decrease in the plane that is perpendicular to the direction of tensile stresses. The rupture of the sample is initiated at mineral inclusions and structural discontinuities. Necking of the sample at the moment of failure is δ = 0.02÷0.05%. Such a small necking, as well as the orientation of the fracture surface evidences the brittle character of rock failure. The rock sample breaks mainly as the result of chipping off, thus in a different manner from a sample of a plastic material where failure occurs as the result of sample necking or due to the formation of slip planes oriented obliquely to the sample axis. 343 800 dz = lnF0 /F, 10 –6 sz 600 sr = p sr = p 400 sz 200 0 0 0.2 0.4 0.6 0.8 1.0 1.2 k = p/s z Fig. 10. Plastic strain of limestones at the moment of failure under hydrostatic pressure conditions Rys. 10. Graniczne odkształcenie plastyczne wapieni przy rozciąganiu w warunkach działania wszechstronnego ciśnienia 2 . 3 . Te s t s o f t h e s t r e n g t h a n d d e f o r m a t i o n a l p r o p e r t i e s o f r o c k s at shearing under triaxial stress conditions Testing the shear strength under triaxial stress conditions was performed using an M-16 chamber equipped with a special shearing device (Fig. 11). The Jaeger method that consists in forcing the slip of a rock disk along the cylindrical surface parallel to the shearing force was employed. Shear strength of rocks was determined using disk samples of 44 mm in diameter and 10 mm in thickness. The magnitude of shearing stress τ at the moment of rupture was calculated using the formula: tz = where: Ps p F d h — — — — — Ps - pF p dh (14) pressure of the punch on sample, hydrostatic pressure, cross-sectional area of the punch, punch diameter, sample thickness (height). The carbonate rocks tested showed a high shear strength. Hydrostatic pressure enhanced this strength significantly. At a hydrostatic pressure of 60 MPa the shear strength was about seven times higher compared to conditions where p = 0 (Fig. 12). 344 Fig. 11. M-16 triaxial chamber with equipment for shear tests of rocks Rys. 11. Komora trójosiowa M-16 z oprzyrządowaniem do badań skał na ścinanie 140 Shear strength t, MPa 120 100 80 60 40 20 Fig. 12. Shear strength of limestones under hydrostatic pressure conditions 0 0 20 40 60 Hydrostatic pressure p, MPa Rys. 12. Wytrzymałość wapieni na ścinanie w warunkach wszechstronnego ciśnienia 345 180 160 140 p=60 p=50 p=40 120 Shear strength t, MPa p=30 100 p=20 80 p=10 60 p 40 p p q q=p+4P/p (D 2–d 2) q Fig. 13. Deformation characteristics of limestones subjected to shear under hydrostatic pressure conditions 20 p=0 0 0 0.4 0.8 1.2 1.6 2.0 Relative movement of sheared disc Dh/h, % Rys. 13. Charakterystyki odkształceniowe wapieni poddanych ścinaniu w warunkach wszechstronnego ciśnienia During the shear tests, measurements of displacement (∆h) of the sheared disk were also done. The displacement was measured using an inductive sensor with accuracy up to 10–6. The results were used to draw the τ – ∆h/h characteristics. The resulting characteristics for carbonate rocks at different hydrostatic pressures are shown in Figure 13. These are straight lines of a slope that increases with an increase in hydrostatic pressure, meaning that the pressure inhibits the disk displacement. The value of the energy before the final rupture of the sample as well as the friction forces on the fracture surface can be determined based on the experimental characteristics τ – ∆h/h. The results of shear tests show that rocks have a high shear resistance in the plane perpendicular to bedding. At the same time, the shear strength is much greater than the tensile strength. 346 2 . 4 . Te s t s o f t h e s t r e n g t h a n d d e f o r m a t i o n a l p r o p e r t i e s o f r o c k s at bending under triaxial stress conditions In order to determine the properties of rocks at bending under triaxial stress conditions a special pressure chamber to test up to 60 MPa (Fig. 14) was constructed. Bending tests were carried out using beam-shaped samples with a rectangular cross-section of the dimensions 20 mm × 30 mm. The length of beams was 195÷250 mm. Beams were tested under bending conditions at hydrostatic pressures ranging from 0 to 60 MPa in a series of tests. Fig. 14. Triaxial chamber for testing rocks at bending under hydrostatic pressure Rys. 14. Komora trójosiowa do badania skał przy zginaniu w warunkach wszechstronnego ciśnienia During the tests, the measurements of beam deformation in the compressed and extended zones using electric resistance strain gauges were taken. An example of the deformation characteristics under bending conditions for a selected sample of anhydrite is presented in Figure 15. The chart shows σg − ε curves for the compressed and extended zones. They characterise the behaviour of rock during bending under given hydrostatic pressure conditions. When analysing the mechanical characteristics of rocks subjected to bending under triaxial stress conditions, an increase in the strength and deformability of the tested beams was observed (Fig. 16). In the extended zone the deformations of the beam were greater than in the compressed zone. At the initial stage of bending, the mechanical characteristics are the same for the compressed and extended zones and have the form of a straight line. After exceeding a certain value of the bending moment Mg = 0.6 Mg max, the characteristics become concave downward and a more rapid increase in strain occurs in the extended zone. The reason for this effect is presumably the growth of cracks in this zone. An important conclusion derived from these tests is that the values of Young’s modulus are the same for compression and tension in the direction perpendicular to bedding. 347 ec 60 er Bending stress s g, MPa 50 40 30 20 10 0 0 100 200 300 400 500 600 700 Deformation of beam in compressed e c and extended zone er, 10 –6 Fig. 15. Deformation characteristics at bending for a selected sample of anhydrite Rys. 15. Charakterystyka odkształceniowa przy zginaniu dla wybranej próbki anhydrytu 22 20 Critical bending moment Mg, kNm 18 16 14 12 10 8 p 6 p 4 2 0 0 10 20 30 40 50 60 70 Hydrostatic pressure p, MPa Fig. 16. Bending strength of anhydrite under hydrostatic pressure conditions Rys. 16. Wytrzymałość anhydrytu na zginanie warunkach wszechstronnego ciśnienia 348 2 . 5 . Te s t s o f t h e s t r e n g t h a n d d e f o r m a t i o n a l p r o p e r t i e s o f r o c k s u n d e r a s y m m e t r i c t r i a x i a l s t r e s s c o n d i t i o n s ( σ 1≠ σ 2≠ σ 3) An M-23 Kármán pressure chamber (Fig. 17) was used to test rocks under asymmetric triaxial stress conditions (σ1 ≠ σ2 ≠ σ3). This chamber was modified by introducing pressure heads instead of loading pistons. Fig. 17. Triaxial chamber with additional equipment for testing hollow cylindrical samples Rys. 17. Komora trójosiowa z dodatkowym wyposażeniem do badań próbek cylindrycznych Hollow cylindrical samples having an internal diameter of 21 mm, external diameter of 44 mm and slenderness index of 2.0 were used in the tests. A special feature of these samples is that vertical stress σz as well as the mean stress 1/3(σr + σφ + σz) and the sum (σr + σφ) are the same for all internal points of the cross-section of the sample. Distribution of stresses σr and σφ is, however, non-uniform in the radial direction. Due to this, the concentration of stresses in the sample was eliminated. The applied methodology of tests not only allowed the values of the principal stresses to be changed but also their direction. In traxial tests three schemes of sample loading were used: a) first, where σz = 0, σr ≠ σφ. The test results were used for plotting the strength characteristics of rocks under plane stress conditions for tension and compression. b) second, where σz = const., σr ≠ σφ. The results obtained allowed the strength characteristics of rocks on the octahedral plane (τoct, σoct) for average values of the stress σoct up to a 150 MPa maximum to be plotted. 349 c) third, where σr ≠ σφ ≠ σz. Mechanical parameters determined based on these tests characterise fracturing of rocks at high values of stress σoct, reaching up to 120 MPa. A complete strength characteristic of rocks under a triaxial stress state on the plane (τoct, σoct) presented in Figure 18 was determined using extension test results (profiled samples) and results of tests carried out using the hollow cylindrical samples. These Shear octahedral stress t oct, MPa 120 100 80 60 hollow cylindrical samples 40 dogbone-shaped samples 20 0 0 20 40 60 80 100 120 Normal octahedral stress s oct, MPa Fig. 18. Failure criterion for dolomites on the octahedral plane under asymmetric triaxial stress conditions (σ1 ≠ σ2 ≠ σ3) Rys. 18. Kryterium zniszczenia dolomitów w płaszczyźnie oktaedrycznej w asymetrycznym trójosiowym stanie naprężenia (σ1 ≠ σ2 ≠ σ3) characteristics have the form of two connected sections of intersecting straight lines described by the following equations: τoct = 1.1802 σoct + 3.7 for 1.7 MPa ≤ σoct ≤ 15 MPa (15) τoct = 0.7836 σoct + 10.3 for 15 MPa ≤ σoct ≤ 120 MPa (16) Results obtained on the hollow cylindrical samples showed a substantial difference in strength in comparison with those obtained using solid cylindrical samples tested according to the Kármán scheme. 350 2 . 6 . Te s t s o f c r a c k p r o p a g a t i o n i n r o c k s u n d e r t r i a x i a l s t r e s s conditions The aim of those tests was to evaluate the rocks susceptibility to sudden and uncontrolled rupture under triaxial stress conditions based on the measurement of the critical opening of a crack (a notch) preset in beam-shaped samples subjected to bending. The crack opening was measured using a specially designed sensor with flat clip springs and recorded automatically as a function of rock beam load at a constant hydrostatic pressure. The obtained charts allowed a determination of whether a lowenergy, brittle failure under unconfined conditions may change into high-energy failure under hydrostatic stress conditions. Samples for these tests had the shape of a beam with a rectangular cross-section of 30 mm × 40 mm and a length of 220 mm. In the centre of the beam a chevron notch 2 mm wide with an internal angle of 30° was made. The depth of the notch was 10 mm which was equal to 1/4 of the beam height. Triaxial stress conditions in the beam were generated in a triaxial chamber (Fig. 19) by using oil pressure ranging from 0 to 60 MPa. The bending load was applied to the beam at two locations using the four-point loading method. Using the existing measuring system with automatic recording of test results of the bent beams, a series of plots was obtained showing the relationship between beam load P and crack opening ∆f at different hydrostatic pressures. An example chart for a selected sample is presented in Figure 20. Fig. 19. Triaxial chamber for tests of crack propagation in beam-shaped samples of rock Rys. 19. Komora trójosiowa do badań rozprzestrzeniania się szczelin w próbkach-beleczkach skalnych 351 Bending load P, kN 6 4 p = 50 MPa 2 0 0 10 20 30 Crack opening Df, mm Fig. 20. Example chart of the relationship between load and crack opening in an anhydrite beam bent under hydrostatic pressure of p = 50 MPa Rys. 20. Przykładowy wykres zależności pomiędzy obciążeniem a rozwarciem szczeliny w zginanej belce z anhydrytu przy wszechstronnym ciśnieniu p = 50 MPa Hydrostatic pressure causes an increase in critical stresses and in the size of the crack opening (Fig. 21) exceeding which leads to an uncontrolled failure. High-energy brittle failure under unconfined conditions changes into even more violent failure with an increase of hydrostatic pressure. 352 30 Critical crack opening Df, mm 25 20 15 10 p p 5 p sensor 0 0 10 20 30 40 50 60 Hydrostatic pressure p, MPa Fig. 21. Critical opening of a crack in bent beams of anhydrite under hydrostatic pressure conditions Rys. 21. Krytyczne rozwarcie szczeliny w zginanych belkach z anhydrytu w warunkach wszechstronnego ciśnienia 3. Summary and final conclusions The designed and constructed station for testing the mechanical properties of rocks under triaxial stress conditions proved to be very useful for experiments carried out under confining pressure of 0÷60 MPa. The tests allowed for the determination of the impact of hydrostatic pressure on the strength and deformational properties of rocks from the copper ore deposit (Zechstein carbonate rocks in particular) occurring in the immediate and main roof of the orebody (Figs 22 and 23). 353 Fig. 22. Types of samples used for tests under triaxial stress conditions Rys. 22. Rodzaje próbek stosowanych w badaniach w trójosiowym stanie naprężenia Fig. 23. Fractured samples after tests under triaxial stress conditions Rys. 23. Zniszczone próbki po badaniach w trójosiowym stanie naprężenia Fig. 23. Fractured samples after tests under triaxial stress conditions Rys. 23. Zniszczone próbki po badaniach w trójosiowym stanie naprężenia Based on triaxial test results, the following conclusions can be drawn: 1. The compressive strength of rocks at a pressure of 60 MPa is three times higher in comparison with the uniaxial strength. Rocks, which under uniaxial stress conditions have high compressive strength, maintain this feature under triaxial stress conditions. The deformation moduli do not change significantly with a change of hydrostatic pressure. Critical deformations of the tested rocks are equal to 354 0.15÷0.25% under uniaxial compression conditions and 0.6÷1.0 under compression at a confining pressure of 60 MPa. It was also found that Poisson’s ratio does not substantially change its values with a confining pressure within the range of up to 60 MPa. 2. Tests of the shear strength of rocks showed high strength in the direction perpendicular to bedding. 3. The so-called true fracture strain or plastic strain at failure of rocks under tensile conditions is equal to 0.02÷0.5% on average. The direction of sample fracture that is perpendicular to the tensile load direction and a small value of sample necking at the moment of rupture is proof of brittle failure. 4. Test results of the strength and deformational properties of rocks under triaxial stress conditions are widely applied in engineering calculations, in the design of mine excavations and in numerical simulations of the mine strata deformation processes during mining. Received: 14 March 2007