calorimetry

CALORIMETRY
by
Wojciech Zielenkiewicz
Second Edition 2008
Institute of Physical Chemistry, Polish Academy of
Sciences, Kasprzaka 44/52, Warsaw, Poland, 2008.
Editor: Prof. dr hab. Janusz Lipkowski
Technical editor: Małgorzata Kowalewska-Jóźwik
Including 366 pages and 873 bibliographical
references.
ISBN 978-83-920719-6-9
All rights reserved
Cena: 100 zł
Przedmiotem książki jest podanie podstawowych informacji o rozwoju kalorymetrii i
jej
zastosowaniach.
Podano
podstawy
teoretyczne
kalorymetrii,
klasyfikację
kalorymetrów, przedstawiono stosowane metody i układy kalorymetryczne.
Wybór tematyki odzwierciedla zainteresowania autora, którego prace dotyczą
podstaw teoretycznych kalorymetrii, kalorymetrii roztworów, biomolekuł i związków
inkluzyjnych.
Spis treści:
Chapter 1. Outline of the history of calorimetry development.
Chapter 2. Heat transfer in calorimetry. Fourier Law and Fourier-Kirchhoff
Equation. Conduction, convection and radiation. Cooling and heating processes of
thermally passive body. Heat balance equation of simple body. Newton Law of
Cooling. The static-dynamic method.
Thermal-electric and thermal dynamic
analogy methods.
Chapter 3. Classification of calorimeters. Methods of determination of heat
effects. Calibration and test reactions.
Chapter 4. Adiabatic calorimeters. Adiabatic-isothermal calorimeters. Scanning
adiabatic calorimeters. Photoacoustic (quasi-adiabatic) calorimeters.
Chapter 5. Combustion calorimetry. Static and rotating oxygen calorimetric
bombs. Fluorine combustion bomb.
Chapter 6. Enthalpy of sublimation. Calorimetric and indirect methods.
Chapter 7. Solution calorimetry. Solution reaction calorimeters. Solute-solvent
interactions. H.F. solution calorimetry. High temperature solution calorimetry.
Determinations of heats of dilution and mixing. Isothermal displacement
calorimeters. Flow calorimeters. High-pressure, high temperature calorimeters.
Mixing calorimeters of liquids under cryogenic conditions.
Chapter 8. Isoperibol, nonadiabatic-nonisothermal calorimeters used for the
determination total heat effects and thermokinetics. The E. Calvet
microcalorimeter. Conduction microcalorimeters. Family of calorimeters with
considerable inertia. Determination of kinetic parameters. Fast reaction
calorimeters. Chips calorimeters. Photocalorimetry. Methods of determination of
heat effects and thermokinetics. Heat flux method and dynamic method. N-body
method. Numerical and analogue methods of reconstruction of thermokinetics.
Analysis of heat effects courses. Multi-body theory. Equations of dynamics.
Elaboration of the mathematical, dynamic model of calorimeter based on physical
parameters.
Chapter 9. Thermal analysis. Differential Thermal Analysis. Differential Scanning
Calorimetry (DSC). Temperature modulated calorimetry DSC (TMDSC).
Transistometry.
References
(873 references).
Informacja dla kupujących: cena 100,00 zł
Miejsca sprzedaży:
Główna Księgarnia Naukowa im. Bolesława Prusa, ul. Krakowskie Przedmieście 7,
00-068 Warszawa (vis-a-vis Uniwersytetu Warszawskiego), www.pwn.pl
Instytut Chemii Fizycznej PAN, ul. Kasprzaka 44/52, 01-224 Warszawa.
BANK PEKAO SA
Rachunek nr 26 1240 6003 1111 0000 4941 6172
Dopisek: Calorimetry
lub zamówić poprzez tel./fax.: 022-632 43 89; e-mail: [email protected]