UPDATE OF TECHNICAL REQUIREMENTS

Projekt współfinansowany ze środków Europejskiego Funduszu Rozwoju Regionalnego w ramach
Programu Operacyjnego Innowacyjna Gospodarka
Oświęcim, 04.02.2015
L.dz. 47/TZ/PM/2015
UPDATE OF TECHNICAL REQUIREMENTS
Conc: Inquiry / Contrator selection for DELIVERY AND INSTALLATION OF THE
TWO PIECES OF 5 l BATCH GLASS REACTORS WITH TOOLS, INSTRUMENTS
AND APPARATUS FOR THE S-SBR PLANT :
European Regional Development Fund under the operational Program Innovative Economy
Project no POIG.04.05.01-00-003/12
PROJECT: "Implementation of innovative technology of rubbers SSBR X3 production in Synthos
Dwory 7 spółka z ograniczoną odpowiedzialnością spółka jawna" POIG.04.05.01-00-003 / 12
„Wdrożenie innowacyjnej technologii wytwarzania kauczuków SSBR X3 w Synthos Dwory 7
spółka z ograniczoną odpowiedzialnością spółka jawna” POIG.04.05.01-00-003/12
CLIENT: SYNTHOS DWORY 7 –Spółka z ograniczoną odpowiedzialnością spółka jawna
The change concern Appendix no 2 – below new updated requirements
Other terms and conditions of the query 47/TZ/PM/2015 without changes
Appendix no 2. Technical requirements
5 l batch glass reactor no 1 ( 1 piece )
Wymagania / Requirements
Ciśnienie projektowe / design pressure
Temperatura projektowa / design temperature
Płaszcz grzewczo/chłodzący - Coats - heating /
cooling
Czujnik temperatury / temperature sensor
Pomiar ciśnienia / Pressure Measurement
Mieszadło z napędem / Driven stirrer
Przeznaczony do strefy Ex/ Suitable for Ex zone
Dokumentacja w j. polskim / Documentation in
Polish
Pokrywa do reaktora winna być wyposażona w 4
stożkowe szlify żeńskie 3 , stożkowe szlify 14 i
króciec do wprowadzania substancji stałych (
proszków) / Reactor cover should be equipped
with 4 NS tapered female jonts 32, and 2 NS
tapered female jonts 14 and a input for
introducing solids (powders)
Mieszadła/ stirrer
Uwagi / Comments
-1 do +1 bar
- do
C
Tak / YES
Tak /YES
Tak/YES
Tak/YES
Tak/YES
Tak/YES
Pt100
manometr
Zakres 0-500 obr/min - Range
0-500 rev / min
Strefa / Zone II 2B T3
Tak/ YES
Tak/YES
1 szt kotwicowe, 3 szt
łopatkowe, 3 szt wirnikowe Anchor 1 piece, 3-piece
paddle, 3-piece rotary
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Projekt współfinansowany ze środków Europejskiego Funduszu Rozwoju Regionalnego w ramach
Programu Operacyjnego Innowacyjna Gospodarka
Zestaw destylacyjny z chłodnicą zwrotną / The
distillation assembly with a reflux condenser
Podnoszona pokrywa na stelażu / Lifting lid on
the rack
Reaktor wyposażony w dolny króciec spustowy /
A reactor equipped with a bottom drain adapter
Tak/YES
Mieszadło mechaniczne wyposażone w suche
uszczelnienie. / Mechanical stirrer equipped with
a dry seal.
Tak/ YES
Reaktor powinien posiadać czujniki temperatury
umożliwiające kontrolę temperatury płaszcza i
mieszaniny reakcyjnej wewnątrz reaktora. / The
reactor should have temperature sensors to
enable control of the coat temperature and the
reaction mixture inside the reactor
Tak/ YES
Dodatkowy odbieralnik 2L /
Additional receiver 2L
Tak/YES
Tak/ YES
5 l batch glass reactor no 2 ( 1 piece )
Reason:
R&D investigations of emulsion polymerization at a laboratory scale to understand dependence
among reaction parameters, and provide customers with new polymer samples.
Parameters: All equipment must be compatible with EX zone.
Reactor:
Size: 5 liters (final working volume 70-80% from 5 liters)
Min/max pressure: 0,04/+2 bar
Min/max temperature: -5/ 1 °C
Material of Construction: Must be compatible with styrene, butadiene, organic solvents, amines,
water solutions of acids and bases (pH range from 3,5 to 12)
Agitator: Capable of mixing viscous polymer dispersion (up to 50 000 cPs) – may need to test –
230/400V, three phase 50 Hz, EEx e ii T4, max speed approximately 0-200 rpm, double helix impeller.
The thermocouple must be immersed in the reaction medium.
The agitator with a frame at the height min. 70% complete, and must be helical.
motor sufficient for highly viscous systems 50000cPs
operating system and vacuum system.
JULABO (cooling and warming system).
EX design.
Vessel: Borosilicate glass (or better) stirrer vessel 5 liter, max pressure at least 0,04/+2 bar, with
heating and cooling jacket, heating min. to 1 °C, cooling min. oC, bottom drain valve. Vessel body
is cylindrical.
Cover Plate: Has a center opening for agitator, and 5 openings:
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Projekt współfinansowany ze środków Europejskiego Funduszu Rozwoju Regionalnego w ramach
Programu Operacyjnego Innowacyjna Gospodarka
1. One for Vacuum vent line
2. One for temperature control
3. One for condenser
4. One for charging hopper or biurette
5. One for future growth – empty at this time
Bottom Exit Line: Manual ball valve, must have the ability to take samples of viscous latex through a
needle outlet fairly quickly. It has to be easy to clean, even when the undesirable coagulation process
takes place in the reactor.
Stand: Stainless steel construction
Accessories: heating and cooling system sufficient for 5l volume, temperature probes with sufficient
cable, additional parts for stirrer equipment, additional bottom drain valve, additional separating
valves, spare parts and tools sufficient to keep us running.
Condenser Line: Manual open/close valve, condenser with approx. 0.1 m2 (or more) exchange area,
manual open/close valve for venting.
Vacuum pump line
Must be capable of working with 0,04 bar absolute pressure. Consisting of condenser and vacuum
pump. All elements must be resistant to styrene, butadiene, amines, organic solvents and water
solutions of bases or acids (pH range from 3,5 to 12).
Waste vessel – 2,5 L could be made from glass resistant to low pressure (0,04 bar) (optional)
All lines must be easily detachable for ease of cleaning.
System:
Must be computer (automatic) operated:
-stirring
-temperature (Jacket and reactor interior)
- vacuum valve opening
-parameters such as: rpm, torque, temperatures (in jacket and reactor), should be displayed on the
screen.
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